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Lake Michigan Mass Balance

About the Project About the Data Summary Results

Original LMMB Codes: Analytical Remarks Codes (Result Qualifiers)

Please report the 3-letter lab remark codes from this list as appropriate for each sample.

CODENAMEDEFINITION
ALCaldol condensation The indicated compound is suspected by the analyst of being a product of an aldol condensation reaction.
ALTalternate measurementThe subject parameter was determined using an alternate measurement method. Value is believed to be accurate but could be suspect.
BDLbelow detectable limitsThere was not sufficient concentration of the parameter in the sample to exceed the lower method detection limit in force at the time the analysis was performed. Numeric results field, if present, is an approximate value. Also see MDL.
BLQbetween instrument detection limit and limit of quantificationResult was above instrument detection limit but below limit of quantification.
CANcanceledThe analysis of this parameter was canceled and not performed.
CBCcannot be calculatedThe calculated analysis result cannot be calculated because an operand value is qualified.
CLCcalculated resultCalculated result
CNTnon-acceptable colony countsResults based on colony counts outside acceptable range.
CONconfirmedThe subject parameter has been confirmed using an auxiliary analytical technique as specified in the analytical method.
EERentry errorThe recorded value is known to be incorrect but the correct value cannot be determined to enter a correction.
EHTexceeded holding timeSample or extract was held longer than stated time before analysis; results may be estimated.
ESTestimated valuePresent above detection limit but not quantified within expected limits of precision.
FBKfound in blankThe subject parameter had a measurable value above the established QC limit when a blank was analyzed using the same equipment and analytical method. Therefore, the reported value may be erroneous.
FBSfailed blank sampleThe blank sample did not meet the established measurement quality criterion. Blank concentration > MDL.
FDBfailed dry blankLaboratory procedural or dry blank failed acceptance criteria
FDCfailed drift checkThe drift check sample did not meet the established measurement quality criterion.
FDLfailed lab duplicateLab duplicate sample failed to meet the established measurement quality criterion.
FFDfailed field duplicateField duplicate exceeded stated relative percent difference.
FFRfailed field blankField blank failed acceptance criteria
FFSfailed field spikeField spike recoveries failed acceptance criteria
FFTfailed trip blankTrip blank failed acceptance criteria
FISfailed internal standardInternal standard failed acceptance criteria
FLCfailed linearity checkThe linearity check sample did not meet the established measurement quality criterion.
FLSfailed laboratory spikeLaboratory spike recoveries failed acceptance criteria
FMSfailed matrix spike criteriaRecovery of matrix spike was outside of stated limits
FPCfailed performanceLaboratory performance check failed acceptance criteria
FPSfield preliminary screeningA preliminary screening of the sample for the subject parameter was conducted. The result of the screening indicated that it would not be useful to determine the concentration of the parameter.
FQCfailed quality controlThe analysis result is not reliable because quality control criteria were exceeded when the analysis was conducted. Numeric field, if present, is estimated value.
FRSfailed referenceInternal laboratory reference sample failed acceptance criteria.
FSFfailed surrogate spikeSurrogate spike recoveries for ICP MS of Y, Ho, or Yb failed acceptance criteria
FSLfailed blankSpiked laboratory blank or larboratory procedural blank failed acceptance criteria
FSRfailed SRMStandard Reference Materials failed acceptance criteria.
FSSfailed surrogateSurrogate recovery failed acceptance criteria
GTLgreater than upper detection limitActual value is known to be greater than value of the upper detection limit
INTinterference suspectedAnalyst believes this result to be an interference and not the analyte listed.
ISPimproper sample preservation Due to improper preservation of the sample, it was rendered not suitable for analysis.
LAClaboratory accidentThere was an accident in the laboratory that either destroyed the sample or rendered it not suitable for analysis.
LISlaboratory internal standardFor organic analysis, internal standards added to a sample to be used for quantitation.
LLSless than lower standardThe analysis value is less than the lower quality control standard.
LTCless than criteria of detectionValue reported is less than the criteria of detection (which may differ from instrument detection limits).
LTLless than lower detection limitActual value is known to be less than value given for the lower detection limit
MDLbelow Ultra MDLValue was below the Ultra method detection limit.
MSL"EMSL" detection limitsInstrument detection limits were computed using a "T" test on two or more calibration samples.
NAInot analyzed due to interferenceBecause of uncontrollable interference the analysis for the subject parameter was not conducted.
NAPNot ApplicableNot applicable (not to be used in any field except Laboratory remark codes)
NARno analysis resultThere is no analysis result required for this subject parameter.
NSQnot sufficient quantityThere was not sufficient quantity of the sample to conduct an analysis to determine the concentration of the subject parameter.
PNQpresent but not quantifiedThe subject parameter was present in the sample but no quantifiable result could be determined.
PREpresumptive presencePresumptive evidence of presence of material; tentative identification.
PTSpeak too smallPeak is too small to apply relative percent difference criteria for duplicates
REJrejectedThe analysis results have been rejected for an unspecified reason by the laboratory. For any results where a mean is being determined, this data was not utilized in the calculation of the mean.
REQreque for re-analysisThe analysis is not approved and must be re-analyzed using a different method.
RETreturn(ed) for re-analysisThe analysis result is not approved by laboratory management and reanalysis is required by the bench analyst with no change in the method.
REXre-preparedThe indicated analysis results were generated from a re-preparation (extraction) of the same sample.
RINre-analyzedThe indicated analysis results were generated form a re-analysis (injection) of the same sample extract or aliquot.
SFFfailed field spike blankField spike blank (SFB) recoveries are either below 70% or above 125%
TDSRPD Criteria ExceededDuplicate values less than 5 times the method detection limit and RPD criteria exceeded. (Too darn small) See FDL also.
TIEtentatively identified-estimated valueThe subject parameter was not in the contract-defined list of parameters to be analyzed for; however the value has been estimated.
UNDanalyte not detectedAnalysis was performed but analyte not detected above noise.
 
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