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Superfund Analytical Services / Contract Laboratory Program (CLP)


Multi-Media, Multi-Concentration Dioxins and Furans Analysis, DLM02.2 (a Non-Routine Analytical Service)

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The Statement of Work (SOW) for Multi-Media, Multi-Concentration Dioxins and Furans Analysis (DLM02.2) describes the analytical method for chlorinated dibenzo-p-dioxins and chlorinated dibenzofurans (CDDs/CDFs) analyses. This SOW is based on the EPA Office of Water Method 1613B and defines the means by which 2,3,7,8-substituted CDDs/CDFs are isolated, detected, quantitatively measured, and reported [including the Electronic Data Deliverable (EDD) format]. DLM02.2 includes extraction procedures for water, soil, sediment, sludge, tissue (non-human), ash, and oil/oily matrix samples, and employs High Resolution Gas Chromatography/High Resolution Mass Spectrometry (HRGC/HRMS) to analyze the samples. For an overview of changes from the last version of this SOW, please refer to the Summary of Changes from DLM02.1 (July 2009) to DLM02.2 (December 2009) (PDF) (1p 103K).

View a handout providing an at-a-glance look at DLM02.2 (PDF) (2pp, 313K)

DLM02.2 in PDF Format

DLM02.2 Exhibits A-C (PDF) (60 pp, 473K) - Summary of Requirements; Reporting and Deliverables Requirements; and Target Compound List with Contract Required Quantitation Limits

DLM02.2 Exhibit D (PDF) (72 pp, 1.2 MB) - Analytical Methods

DLM02.2 Exhibits E-H (PDF) (82 pp, 276K) - Quality Assurance/Quality Control Procedures and Requirements; Chain of Custody, Document Control, and Written Standard Operating Procedures; Glossary of Terms; and Data Dictionary and Format for Data Deliverables in Computer Readable Format

DLM02.2 Forms in Microsoft Word Format

Dioxin and Furan Forms in Microsoft Word Format (DOC) (16 pp, 624K)

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