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I. 1. A. a.(1)(a) i) a)S ($0 ($0 0 (($0 0 0   A_ekqwDocumentDocument StyleI.1.A.a.(1)(a)i)a)jo4Tech InitInitialize Technical StyleS #  1 .1 .1 .1 .1 .1 .1 .1 S CuyTechnicalTechnical Document Style11.11.1.11.1.1.11.1.1.1.11.1.1.1.1.11.1.1.1.1.1.11.1.1.1.1.1.1.1x?t2PleadingHeader for numbered pleading paper %  &t(  XXXXX?0''*dE*??0''*dE*?HH1HH2HH3HH4HH5HH6HH7HH8HH910111213141516171819202122232425262728  .+(2t$ 5!  '     0 .   -(2t$ 5!   dTable_A&0 d d d  CRight ParRight-Aligned Paragraph NumbersI.A.1.a.(1)(a)i)a)3|x<6X9`("Courier 10cpiXx6X@8;X@< 9(*Courier 10cpiBoldXx B;X($<( 9Z &Courier Regularj%$(3y$ 5!   f hy'  6XlXXX DXX 5!  +r^XpP hp x (#%'0*,.8135@8:<H?ACXr  l7lXdd7@ PERFORMANCESPECIFICATION5SPECIFICATIONSANDTEST Z @0 0 PROCEDURESFORTRSCONTINUOUSEMISSION@ MONITORINGSYSTEMSINSTATIONARYSOURCES  " * DXXXpP X*1.0ScopeandApplication.    1.1Analytes.*q-. ddd Xdd Xdd X(#(#q,P dd",P dd"+  //" d  p/Analyte ./!  / .CASNo. J009!   p / (JTotalReducedSulfur(TRS) 200!X 00 2NA1'%v   (  00 1~ 1.2Applicability.ThisspecificationisforevaluatingtheapplicabilityofTRScontinuousemissionmonitoringsystems(CEMS)atthetimeofinstallationorsoonafterandwheneverspecifiedinanapplicablesubpartoftheregulations.TheCEMSmayincludeoxygenmonitorswhicharesubjecttoPerformanceSpecification3(PS3). 1.3Thedefinitions,performancespecification,testprocedures,calculationsanddataanalysisproceduresfordeterminingcalibrationdrifts(CD)andrelativeaccuracy(RA)ofPS2,Sections3.0,8.0,and12.0,respectively,applytothisspecification.2.0SummaryofPerformanceSpecification. %>$  TheCDandRAtestsareconductedtodetermineconformanceoftheCEMStothespecification.l3.0Definitions. *$*  SameasinSection3.0ofPS2. ,N&, 4.0Interferences.[Reserved] Z 5.0Safety.   Thisperformancespecificationmayinvolvehazardousmaterials,operations,andequipment.Thisperformancespecificationmaynotaddressallofthesafetyproblemsassociatedwithitsuse.Itistheresponsibilityoftheusertoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicableregulatorylimitationspriortoperformingthisperformancespecification.TheCEMSusersmanualshouldbeconsultedforspecificprecautionstobetakenwithregardtotheanalyticalprocedures.6.0EquipmentandSupplies. l  SameasSection6.0ofPS2.7.0ReagentsandStandards. N  SameasSection7.0ofPS2.  8.0SampleCollection,Preservation,Storage,andTransport. "4   8.1RelativeAccuracyTestProcedure.SamplingStrategyforreferencemethod(RM)Tests,NumberofRMTests,andCorrelationofRMandCEMSDataarethesameas PS2,Sections8.4.3,8.4.4,and8.4.5,respectively. )8#(  NOTE: ForMethod16,asampleismadeupofatleast Z threeseparateinjectsequallyspaceovertime.ForMethod16A,asampleiscollectedforatleast1hour.  8.2ReferenceMethods.Unlessotherwisespecifiedintheapplicablesubpartoftheregulations,Method16,Method16A,16BorotherapprovedalternativeistheRMforTRS.9.0QualityControl.[Reserved]   10.0CalibrationandStandardization.[Reserved] `  11.0AnalyticalProcedure. ~$  Samplecollectionandanalysisareconcurrentforthisperformancespecification(seeSection8.0).Refertothereferencemethodforspecificanalyticalprocedures.12.0CalculationsandDataAnalysis. 4  SameasSection12.0ofPS2.13.0MethodPerformance.   13.1CalibrationDrift.TheCEMSdetectorcalibrationmustnotdriftordeviatefromthereferencevalueofthecalibrationgasbymorethat5percentoftheestablishedspanvaluefor6outof7testdays.Thiscorrespondsto1.5ppmdriftforSubpartBBsourceswherethespanvalueis30ppm.IftheCEMSincludespollutant anddiluentmonitors,theCDmustbedeterminedseparately r+%* foreachintermsofconcentrations(seePS3forthediluentspecifications).  13.2RelativeAccuracy.TheRAoftheCEMSmustbenogreaterthan20percentwhentheaverageRMvalueisusedtocalculateRAor10percentwhentheapplicableemissionstandardisusedtocalculateRA.14.0PollutionPrevention.[Reserved]   15.0WasteManagement.[Reserved] \  16.0AlternativeProcedures.[Reserved] z  17.0References. >  1.DepartmentofCommerce.ExperimentalStatistics,NationalBureauofStandards,Handbook91.1963.Paragraphs33.1.4,p.331. 2.AGuidetotheDesign,MaintenanceandOperationofTRSMonitoringSystems.NationalCouncilforAirandStreamImprovementTechnicalBulletinNo.89.September1977. 3.ObservationofFieldPerformanceofTRSMonitorsonaKraftRecoveryFurnace.NationalCouncilforAirandStreamImprovementTechnicalBulletinNo.91.January1978.18.0Tables,Diagrams,Flowcharts,andValidationData. )D#(  SameasSection18.0ofPS2.