WPC  GM2sŮ>yvD-pHiw׎IVpBS59j;!Fʒ=2GY(:4GOp0Js~z^uYxmcO[]y(]V@*\JR.cq$ Vcpx8DY Y2i^P!hΩڼ5Jw T ߭Qwh;S?.[ױsGU>F"ֹGrZoFd-w&1YP@ffХF8BWˑ6wD!9&dp~C0qL*C^k7\,%z}?n QHmJɕ R'Jea`nRKu_h Unvah//TR'Q uwM;. tixέEaIxD,&h,t4q0YwhLa5mY>SQ"JMsį^f5kps# JUc@U % 0( f a  4  w@ ND F mH U:_ U}@ @ o5 "UR:U Nfa"faU:(U >bfaU@ U@U@<R|   B h h h h  h hfaf1a333333333333333333 B-GGGGGGGGGGGGGGGGG Bttttttt A 0D.. D+r 0K B* D3HP LaserJet 4P/4MPHPPCL5E,,,,,,0!),h  Z (CG Times RegularX($TABLE A nD$ar3|xL  C D E F aG H UI EJ K L U,cAZ"Arial Regular*[X Z(CG Times Regular WPC{{/ / !/  ƚT  & +/U$&@`ObRb??b7`^A`BBb`bA`1`!bb!R?bбuҰj|h¼q///R"/ @O@1/"@@@ b!A !!! / Oab B@@AOOO@`B111/" A ` ""@_bBb___`BBBB@#2?/ "@@rrr?bb``<@A@@@@`AP`b`A@"AA% bAbAbA5AA"""+"Y@@B!AB@B@@pA@Ra`b_``qtA2BB?5ŸҿA@@AA5B@"@ AA@A@@BO45 - "-f$1;6   W ( !vQ0 2DpJzUXAXkVFv nm   - "-,$ ?4$?1$ \ O    L FL # O# E D   "--" M"?# """ !# l#l      {! (! "R$$ "  "-%" $$RL)$ #L)$%)$L#  "- $/ $ # "%" # 0# # #u $- $/ #  #) # #%# "D # c# #r #) --  X X *\  `:Tms Rmn 8ptRmn-8 25inOne!( Z6Times New Roman RegularMTABLE A  X X MTABLE A' `"CG Times 12pt3_ Z &Tms Rmn RegularTable_A(LR  x (CG Times Regular*)L  Z(CG Times Regular)   Z (CG Times Regular 0 '  , JOHNSONLMHM d,.Table_ATable_A)Hairline dP Pd`\_^ I&mage <=8C HKKKK(3$ !  'dxd( $ Figure  1  Level 1Level 2Level 3Level 4Level 5&0 d dffff'dxd !  _7XXdd7XXXX    METHODS98 P  STATUSOFSTATIONARYSOURCEMETHODSFORAIR_TOXICS_ pY<,(`~0 1 `E1mp (#(#         (#(# @@"#XXXX~#LarryD.Johnson P($' NationalExposureResearchLaboratoryOfficeofResearchandDevelopmentU.S.EnvironmentalProtectionAgencyResearchTrianglePark,NC27711 XXXX  -@),   9ZXXCOMMENTSANDSUGGESTIONS   XX9ZThefollowinginformationisincludedtogivetheuserofthisdocumentperspectiveontheinformationcontainedthereinandtoaidindecisionsregardingitsuse.1.0  Thestatustablecontainsasummaryofthemethodstypeandstatusforstacksampling   andanalysisofeachofthe189air_toxics_Ԁlistedinthe1990CleanAirActAmendments.Thetableanditsattachmentshavenodirectregulatorystanding,and f  thereforedonotconstituteapprovaloftheuseofthemethodstosatisfyregulatory V   requirements.Suchapprovalmustalwaysbeobtainedfromtheregulatoryagencyor F  groupinvolvedintheindividualproject.Hopefullythiscompilationwillaidboththeregulatorandtheregulatedcommunityinmakingplanningdecisionsforair_toxics_sourcetesting. (#(# 2.0  Methods98isaMay1998updateandexpansionofthe12/14/89versionofthestatus 6 table,whichwasoriginallyproducedprimarilyfrommemoryoropinionwiththeuseofonlyaveryfewreferencetexts.Anintermediatepartialupdatewasproducedin1994,butwasnotcirculatedwidely.AlargeamountoffieldevaluationdatahasbeenproducedbyEPAanditscontractorssince1989,andanattempthasbeenmadetoutilizeallofitinMethods98.The1998statustable,therefore,isbasedmuchmoreonfieldandlab.testinformationthanwereitspredecessors.NoattempthasbeenmadetoperformacomprehensiveliteraturesurveyandtoincludefieldtestinformationfromsourcesoutsideEPA.Itistheauthorsopinion,however,thatverylittledatafromoutsidesourcesexiststhatwouldmeetthecriterianeededforusefulinclusioninthistable.ThescopeofMethods98hasbeenexpandedinordertogivetheusereasyaccesstothepapersandreportswhichcontaintheinformationbehindtheStatusTableentries,andcompilationtablesareincludedwhichcontainmuchofthefieldandlab.data.FootnotesforeachcolumnonthecompilationtablesleadthereadertoacorrespondingitemontheReferenceList.Thereferencelistcontainsatleastonesource,usuallyareportandapaper,foralloftherecentlygenerateddataandforsomeoftheolderstudies.Theinformationintheattachedtablesandthereferencedpapersismorecompact,andisusuallymucheasiertousethanthatinthereports.Thereportsprovidemuchmoredetail.Some,butnotall,oftheStatusTableentriesincludesuggestedreferences.OtherreferencesmaybeidentifiedbyscanningtheReferenceListforappropriatetopics. (#(# 3.0  Methodssuchas0010(MM5),0030(_VOST_Ԁsampling),5041/8260(_VOST_Ԁanalysis), &"% and8270(GC/MS)arefromtheSW846MethodsManualusedby_OSW_ԀandtheRegionsfor_RCRA_Ԁrelatedwork.Method5,Method15,andMethod106areexamplesofFederalRegisterMethodshistoricallyrelatedto_OAQPS_Ԁairprograms.Someofthemethodshavebeenpromulgatedbybothgroupsunderdifferentmethodnumbers.Methodsandotherusefulmaterialcanbeobtainedfromsourcesgivenlaterinthisdocument.TheSW846methodslistedarethemostrecentversions,forexample8270Cand5041A.Inthefuture,laterversionsofthesamemethodshouldfunctionjustaswell,orbetter.Inmostcases,dataobtainedwithearlierversionsofthesame .V*- methodwillalsobesound,butnewtestsshouldalwaysutilizethemostrecentrenderingoftheprocedure.Methodssuchas_XHCN_Ԁand_XACN_ԀareOfficeofResearchandDevelopmentproducedmethodswhichhavebeenclearedforpublication,butwhichhavenotyetbeenpromulgatedbyoneoftheprogramoffices.Copiesofthe Xmethodsareincludedinthecorrespondingresearchreportslistedinthereferences. (#(# 40  Thesamplingmethodslistedaregenerallyintendedforrelativelylowconcentrationsof P  materialsinstackgases.Alternatemethodsmaybenecessaryforprocessstreamsorfluegaseswithnocontroldevices.Notallmethodsthatmightbeeffectiveareincludedonthetable.The_Tedlar_ԀbagversionofM18wouldprobablybeeffectiveforthesamecompoundsthat0040sampledwell,providedthatthesourcedidnotemit P  _sorptive_Ԁparticulatematteror_condensable_Ԁwatervapor,andthatsorptionlossesinthelineswereminimal.TheperformanceofthesorbenttubeversionofMethod18wouldbelesseasytopredict,andwouldhavelittlerelationto0040performance. (#(# 5.0  Priorityhasbeengiveninthistabletomethodssuchas0010(a.k.aModifiedMethod  Five,a.k.a._SemiVOST_)orMethod29/Method0060(a.k.a.theMultipleMetalsTrain)whichhavethemostpotentialfordeterminationofmanycompoundsormetalssimultaneously.Alternatesinglepollutantmethodsareoftengiveninthecommentscolumn.ExclusionofamethodfromtheStatusTabledoesnotnecessarilyimplythatitwillnotperformadequately. (#(# 6.0  Manyofthecompoundsonthislistarealsoon_RCRA_ԀAppendix8butlistedundera P differentname.Incaseswherecommon,alternateidentitieshavebeenidentified,thesearegiveninthecommentscolumn.Noattempthasbeenmadetolistallalternate 0p chemicalnames.Insomecases,twoinconsistentchemicalnamesoraninconsistentpairingofanamewitha_CAS_Ԁnumberhasbeengivenonthe_CAAA_Ԁlist.CasessuchasthesehavebeennotedintheStatusTable,andthe_CAS_Ԁnumberhasbeenassumedtobetheprimaryreference(i.e.thecorrect_CAS_Ԁnumberforthecompoundintendedtobe 0 regulated).Theauthorhasnoidea,whatever,whatthelegalramificationsareofsuchmistakesinthe_CAAA_. (#(# 7.0  Ingeneralthecompoundsthathaveidenticallistingsinthesamplingcolumnandinthe "! analysiscolumncanbedeterminedsimultaneously.SomeoftheanalysesmayrequiremorethanoneGCor_HPLC_Ԁruntoaccomplishthisend. (#(# 9.0  Unlessotherwisestated,metalsmethodsproducetotalCr,totalPb,etc.Metals r&"% oxidationstateorcompound_speciation_Ԁisalwaysdifficult,oftenimpossible,andrequiresspecialS&A. (#(# 10.0  EventhoughmuchlessfielddataisavailableforMethod0031thanforMethod0030, 2*r&) theformershouldalwaysperformatleastaswellasthelatter,andoftentimesbetter.Thelimitedcomparisondatagenerally,butnotalways,supportsthisposition.Theauthorbelievesthat0031canalwaysbesuccessfullysubstitutedforM0030,and -B), usuallyshouldbechosenfornewprojects.-2*-(#(# Ї11.0  Thefieldandlab.recoverytableshavenotbeenincludedforallcompoundsorall  methodsontheStatusTable,butthereshouldbeatleastonereferenceintheReferenceListtosupporteach for llistinginthetable.The mand slistingsaremoreconjectural,andmayormaynothavedirectsupportinthereferences. (#(# 12.0  Only_CAAA_Ԁ_toxics_ԀareincludedontheStatusTable,butdataforafewadditional p compoundsmaybefoundontheresultstables. (#(# 13.0  PoorperformanceofoneofthebasicmethodssuchasM0010isoftenaresultof @  reactivityofthetargetcompound.Therelativelynonreactivecompoundswillconsistentlyshowgoodrecoveries,thehighlyreactivecompoundswillconsistentlyexhibitverypoorrecoveries,butthemarginallyreactivecompoundsmayshowvariabilityasafunctionofthereactivityofthestackgasmatrixbeingsampled._Cloroprene_,forexample,yieldedfieldtestresultsoff2andf4alongwithl1lab.recoveries._Caprolactam_Ԁactuallyshowedf1,f4,andl1results.Whensamplingcompoundswithahistoryofmixedperformance,itisprobablyagoodideatospikethesorbentresin(forsorbentmethods)withanisotopicallylabeledrecoverystandardbeforesampling.Carbonorchlorinelabelsaretheleastlikelytoexchangetoanothercompound.Method23usesaformofthistechnique,asdoesM0040. (#(# 14.0  LaboratoryrecoveriesarenotusuallyshownontheSummaryTableunlessfieldresults  werepoor,orthelab.resultsareatoddswiththefieldresults.Thecodedoesnotindicatehowmanyfieldresultsofagivencategorywereobtained,seethecompilationtablesorthereferencedocumentsforthattypeofinformation.#XXXX#P(#(# 15.0  Anumberofthe_CAAA_ԀcompoundswereeliminatedfromfurthertestingwithMethods 0p 0030and0010whentheyfailedinitiallaboratorystudies.Thiswasusuallyananalyticalproblemratherthanasamplingdeficiency.Inthemajorstudieswhichproducedthedatainthecompilationtables,noeffortwasmadetoutilizealternateanalysismethods.Insomecases,potentialalternateshavebeensuggestedintheStatusTable.Method0010willcollectanyorganiccompoundwithaboilingpointabove100C.Ifthecompoundisnotalteredbychemicalreactionduringsampling,fieldrecovery,transportorstorage,thenidentificationofasuccessful_quantification_Ԁschemebecomesamatteroffindingeffectiveextractionanddeterminativeanalyticalmethods.Theresearcherinvestigatingaproblemofthisnature,shouldfindReferences32,33,42,56,57,and58especiallyhelpful. (#(#   %!$ XXXX     9ZXXSTATUSANDRECOVERYTABLECODEDEFINITIONS#XX9Z.#   .  R0  %Recoveryofspikedstandard.(#(# C0  Method301biascorrectionfactor(#(# 0  Anunderlinedmethodisnotrecommendedforthelistedairtoxic. (#(# ?0  Effectivenessofthemethodfo> r> ? > > ? thelistedairtoxicisquestionable@ orshowedmixed f  results.@  (#(# f10  DataareavailablefromatleastoneMethod301fieldtestwhere143%R76.9% 6v  (equivalentto0.70C1.30)andthe_RSD_ԀofRwas50%.&f (#(# f20  DataareavailablefromatleastoneMethod301fieldtestwhere150%R50% F  (equivalentto0.67C2.00)andthe_RSD_ԀofRwas50%.6(#(# f30  DataareavailablefromatleastonefieldtestnotfullyqualifyingasMethod301where  150%R50%(equivalentto0.67C2.00)andthe_RSD_ԀofRwas50%.Someof  therecoverydatamaybebetterthantheminimumshown,andthetestmayonlyhavefailedtomeetminimumreplicatecriteriaforfullMethod301statisticalanalysis. (#(# f40  DataareavailablefromatleastoneMethod301fieldtestwhereR50%orR150%  orthe_RSD_ԀofRwas50%.v(#(# f50  DataareavailablefromatleastonefieldtestnotfullyqualifyingasMethod301where V R50%orR150%orthe_RSD_ԀofRwas50%.F(#(# l10  Laboratorytestdataareavailablewherefullscalesamplingequipment,dynamic &f spiking,andastacksimulatorwereutilized.The_RSD_ԀofRwas50%,and143%R V 76.9%(equivalentto0.70C1.30).ThisisessentiallyasuccessfulMethod301test  F inthelaboratory. (#(# l20  Laboratorytestdataareavailablewherefullscalesamplingequipment,dynamic "! spiking,andastacksimulatorwereutilized.The_RSD_ԀofRwas50%,and150%R # " 50%(equivalentto0.67C2.00).$ #(#(# l30  Laboratorytestdataareavailablewherefullscalesamplingequipment,dynamic &"% spiking,andastacksimulatorwereutilized.R50%orR150%orthe_RSD_ԀofR '#& was50%orunknown.v($'(#(# l40  Otherlaboratorytestdataareavailable,where143%R76.9%(equivalentto V*&) 0.70C1.30)andthe_RSD_ԀofR50%orunknown.Thedatafromtestsinthis F+'* categorymaybeinsufficienttoyieldacredible_RSD_. (#(# l50  Otherlaboratorytestdataareavailable,where150%R50%(equivalentto .V*- 0.67C2.00)andthe_RSD_ԀofR50%orunknown.Thedatafromtestsinthis  categorymaybeinsufficienttoyieldacredible_RSD_. (#(# l60  Otherlaboratorytestdataareavailable,whereR50%orR150%orthe_RSD_ԀofR  was50%orunknown.Thedatafromtestsinthiscategorymaybeinsufficientto  yieldacredible_RSD_. (#(# l70  Laboratorytestsshowednoresponsein_VOST_Ԁanalyticalsystem(5041A&8260B). P  SeeReferences5,7,11,and16. (#(# l80  Laboratorytestsshowedweakresponsein_VOST_Ԁanalyticalsystem(5041A&8260B).  `  SeeReferences5,7,11,and16.Specialattentionormodificationnecessaryforreliableoperation. (#(# #XXXX.#s0  Shouldwork.Forsamplingmethods,noconfirmatoryfieldorlaboratorydatahasbeen   identified,butthestructureofthecompoundoritssimilaritytovalidatedcompoundsmakestheprognosisoptimistic. (#(# m0  Mightwork.Thisdesignationusuallyimpliesthatthetechniquegivenshouldworkif  thecompoundsurvivesthesamplingandanalysisprocess,butthatwehavestrongreservationsaboutitsabilitytodoso.Thisstatusisusuallylinkedwithreactivity/instability.Manycompoundsarestableenoughtoanalyze,butwillnottolerateprolongedexposuretowater,NO2,orothermaterialsduringsampling.`(#(# n0  Noknownadequatemethod.Thisalwaysmeansweknowofnoreliablemethodfor @ thispollutant.Weusuallyhaveidentifiedanumberofunreliablemethodsforthepollutant. Ifnegativedataareavailable,thesamplingmethodwillbeunderlined . `(#(# sp0  Suspectedproblems.Thesuspectedproblemisgiveninthecomments,andisoften D relatedtoreactivity. (#(# _kp_0  Knownproblems.Thisissimilartothesuspectedproblemexceptthatourfearshave   beenconfirmedbydata.XXXX Ifdataindicatequestionableorinconsistentperformance, !  thesamplingmethodwillbefollowedbyaquestionmark. #XXXXTF# "!(#(# *w%ddd Xdd Xdd X(#(#w,9dd ,dd ,9dd ,Xdd ,dd , dd +  +fff  +X2HXXXXXXX2Hǯ XX_CAS_ԀNo. ;ff*$dfff ;ChemicalName ;ff*$dff ;Sampling $d Method ;ff*ff ;S. $d Code ;ff*ff ;Analysis $d Method =fff*ff =Comments 0&$$d   fff 075-07-0  4  Acetaldehyde 7- 4  &@0011&@70011 7-+4  &@0011 &@ 7f1  4  8315A  4 Simultaneousaldehydespossible.Refs.23,40  4 60-35-5  &f _Acetamide_ 5+ &f  $@10$@50010 5+)&f  $@10 $@ 5_m,sp_ 7- &f `@8032`@78032 7-+&f `@8032 `@ 7Maybereactive  &f 75-05-8  X _Acetonitrile_  X _XACN_  X f1  X 8015B8033  X SeeRefs.24&26.#  ǯH#ǯ     X 98-86-2    _Acetophenone_ ;1   j@00100011j@;00100011 ;1/( h j@00100011 j@ ;f1f1  ( h! 35428270C#  ǯfN#ǯ     " 8315A#  ǯO#ǯ     ( h# SeeReferences23&40for0011.  ( h% 53-96-3  Z & 2-_Acetylaminofluorene_  Z ' 0010?  Z ( f2f4l1  Z ) 35428270C#  ǯP#ǯ     Z *   Z + 107-02-8   , _Acrolein_   - 0011?_PFBHA_  * j / f2,_kp_l4  * j 1 8315AGC/_MSorECD_  * j 3 Stabilityproblems,evenin_DNPH_Seereferences45&50for_PFBHA_Ԁapproach.  * j 5 79-06-1  \ 6 _Acrylamide_ 7- \ 7 $@0010$@70010 7-+\ 8 $@0010 $@ 7m,sp  \ 9 GC/MSor8316  : ; Polar,watersoluble.PoorGC,needswork.  \ < 79-10-7  ,l = AcrylicAcid  ,l > 0010sorbent   @ _m,sp_l4   B 8316GC/_FID_   D SuspectpolymerizationmaybeproblemRef50&54,prototypeneedstobe_isokinetic_.   F 107-13-1  <G Acrylonitrile  <H _XACN_00300031  J ssl8  L 8015B8033#  ǯ6Q#ǯ   5041A8260B#  ǯV#ǯ     N SeeRefs.24&26.Purgespoorly,needsspecialattention.  P 107-05-1   Q AllylChloride   R 0030_kp_  S 0031_kp_ jT 0040  HU f4l1f4f1  HX 5041A8260B#  ǯV#ǯ     Y 5041A8260B#  ǯX#ǯ    jZ 8260B#  ǯX#ǯ     H[ 0030recoveriesgoodinlab.,30%fromfieldtest(suspectreactivity)  j] 92-67-1  :z^ 4-_Aminobiphenyl_  :z_ 0010acidliquid  a m,sps  c GC/MS_HPLC_/_PDA_  e Ref50&51.#  ǯUY#ǯ     g 62-53-3   Jh Aniline   Ji 0010?_kp_acidliquid  k f2f4l2l4  m 35428270C_HPLC_/_PDA_#  ǯ[#ǯ     o Extractionandreactivityproblems.Ref50&51,prototypeneedstobe_isokinetic_.#  ǯ_\#ǯ     q 90-04-0  r o-_Anisidine_  s 0010_kp_ t acidliquid  xu f4l2s  xw 35428270C#  ǯ&]#ǯ    x _HPLC_/_PDA_  xy Ref50&51,prototypeneedstobe_isokinetic_#  ǯa^#ǯ   .#  ǯa_#ǯ     x{ 1332-21-4  | Asbestos  } -  ~ -   microscopy   SeparateS&A   71-43-2   Benzene ;1   PA00300040 PA;00300040 ;1/z  PA00300040  PA ;f1f1  z 5041A#  ǯ_#ǯ   8260B#  ǯda#ǯ     8260B#  ǯa#ǯ     z MakesurethattheTenaxisclean.   92-87-5   _Benzidine_   0010?_kp_acidliquid  J f2f4l3s  J 35428270C#  ǯb#ǯ     _HPLC_/_PDA_  J Mayreactduringsampling.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ_c#ǯ   .#  ǯyd#ǯ     J 98-07-7  |  _Benzotrichloride_ 5+ |   $@10$@50010 5+)|   $@10 $@ 5f2  |  35428270C#  ǯd#ǯ     |    |  100-44-7  ! BenzylChloride 5+ !  $@10$@50010 5+)!  $@10 $@ 5f1f2  ! 35428270C#  ǯe#ǯ     !   ! 92-52-4  "  _Biphenyl_ 5+ "   $@10$@50010 5+)"   $@10 $@ 5f1  "  35428270C#  ǯg#ǯ     "    "  117-81-7  $R  _Bis_(2-_ethylhexyl_)phthalate 5+ $R   $@10$@50010 5+)$R   $@10 $@ 5f2f4l1  $R  35428270C#  ǯWh#ǯ     $R  a.k.a._DEHP_  $R  542-88-1  D%! _Bis_(_chloromethyl_)ether  D%! n,_kp_Ԁ0010 D%! _kp_Ԁ0030  %"" f4l1l7  %"" 35428270C#  ǯi#ǯ     D%! Reactsquicklywithwater  D%! 75-25-2  'T# _Bromoform_ 5+ 'T#  $@10$@50010 5+)'T#  $@10 $@ 5f1f2  'T# 35428270C#  ǯk#ǯ     'T#   'T# 106-99-0  F($ 1,3-Butadiene  F($ 0040?_kp_  F($ f4  F($ 8260B#  ǯl#ǯ     F($ Reactive,borderlineresults.  F($ 156-62-7  x)% Calciumcyanamide  x)% 0010M5  *V& s  x)% ?  x)% Shouldbeabletocollectsaltasparticulate.Analysisisproblematic,lowsolubilitywithoutdecomposition.  *& 105-60-2  +&( _Caprolactam_  +&( 0010?  +&( f1f4l1  +&( 35428270C#  ǯm#ǯ     +&( Mixedresults,suspecthydrolysis.  +&( 133-06-2  -X) _Captan_ 5+ -X)  $@10$@50010 5+)-X)  $@10 $@ 5m  -X) 35428270C#  ǯ.p#ǯ    -X) _HPLC_  -) Canbereactive.  -X) 63-25-2  .(+ Carbaryl  .(+ 0010?  .(+ f1f4l1  .(+ 35428270C#  ǯq#ǯ     .(+ Mixedresults.  .(+ 75-15-0  d CarbonDisulfide  d 0030?  d f2f4l2  d 5041A#  ǯr#ǯ   8260B#  ǯs#ǯ     d Mixedresults.  d 463-58-1  & CarbonTetrachloride  & 0030/0031  &  f1  &  5041A8260B#  ǯs#ǯ     &    &  463-58-1  X  CarbonylSulfide  X M150040  f s  X GC/_FPD_CG/_FPD_  f   X 120-80-9  (  _Catechol_ 7- (  $@0010$@70010 7-+(  $@0010 $@ 7m  (  35428270C#  ǯt#ǯ     (  CarefulpHcontrolduringextractionmandatory.Recoverymaybedifficult.   6 133-90-4   h _Chloramben_   h acidliquid   h l4   h _HPLC_/_PDA_   h  Ref50&51,prototypeneedstobe_isokinetic_#  ǯ&w#ǯ      h! 57-74-9  * " Chlordane 5+ * #  $@10$@50010 5+)* $  $@10 $@ 5f1  * % 35428270C#  ǯy#ǯ     * &   * ' 7782-50-5  \( Chlorine  \) M26/26A00500051  j + f1  \, 90569057  \- Halogens&halo-acidscanbedonesimultaneously  j / 79-11-8  , 0 _Chloroacetic_ԀAcid  , 1 n,sp  , 2 n  , 3 _HPLC_  , 4   , 5 532-27-4  ^ 6 2-_Chloroacetophenone_ 5+ ^ 7  $@10$@50010 5+)^ 8  $@10 $@ 5f1f2  ^ 9 35428270C#  ǯ"z#ǯ     ^ :   ^ ; 108-90-7   < _Chlorobenzene_   = 00100030?0031?  <@ f1f2f1f1  <C 35428270C5041A8260B#  ǯ,}#ǯ    . E 5041B8260B#  ǯS~#ǯ     <F Aboverecommendedbplimitfor0030/0031,andfor0040.  . H 510-15-6  nI _Chlorobenzilate_ 5+ nJ  $@10$@50010 5+)nK  $@10 $@ 5f1f3f4  nL 35428270C#  ǯ~#ǯ     nM   nN 67-66-3  0O Chloroform ?5 0P #ZA 003000310040#ZA?003000310040 ?53lS #ZA 003000310040 #ZA ?f1f1s  lV 5041A8260B#  ǯ7#ǯ    0W 5041A8260B#  ǯ|#ǯ    >X 8260B#  ǯށ#ǯ     lY   0Z 107-30-2  [ _Chloromethyl_ԀMethylEther  \ n_kp_Ԁ0030  ] l7  ^ 5041A8260B#  ǯ:#ǯ     _ Maydecomposedurings&a  ` 126-99-8  @a Chloroprene  @b 0030?0031  nd f2f4l1f1  nf 5041A8260B#  ǯ}#ǯ    @g 5041A8260B#  ǯ#ǯ     nh Recoveriesgoodinlab.,mixedinfield.Suspectreactivity.  nj 1319-77-3  k _Cresols_/_Cresylic_ԀAcid  l Є  m -  n -  o Determineasindividual_cresols_Ԁbymethodsfollowing.  >q 95-48-7  pr o-Cresol  ps 0010_NaOH_  ~u f1f2f1  ~w 35428270C_HPLC_#  ǯ#ǯ     ~y _NaOH_Ԁ_impinger_Ԁcollectionforemissionsinthe20100_ppm_Ԁrange.#  ǯ#ǯ   ԀRefs.46,64,&65.  ~{ 108-39-4  @| m-Cresol  @} 0010_NaOH_  N f2f1  N 35428270C#  ǯ~#ǯ    @ _HPLC_#  ǯ#ǯ     N _NaOH_Ԁ_impinger_Ԁcollectionforemissionsinthe20100_ppm_Ԁrange.#  ǯ#ǯ   ԀRefs.46,64,&65.#  ǯ#ǯ     N 106-44-5  ! p-Cresol  ! 0010_NaOH_  ! f2f1  ! 35428270C#  ǯL#ǯ    ! _HPLC_#  ǯ?#ǯ     ! _NaOH_Ԁ_impinger_Ԁcollectionforemissionsinthe20100_ppm_Ԁrange.#  ǯ#ǯ   ԀRefs.46,64,&65.#  ǯ#ǯ     ! 98-82-8  "P _Cumene_ 7- "P $@0010$@70010 7-+"P $@0010 $@ 7f1  "P 35428270C#  ǯ#ǯ     "P   "P 94-75-7  $ 2,4-d 5+ $  $@10$@50010 5+)$  $@10 $@ 5s  $ 8151A,8321A  $   $ 3547-04-4  D% _DDE_ 5+ D%  $@10$@50010 5+)D%  $@10 $@ 5f1  D% 35428270C#  ǯ2#ǯ     D% _CAS_Ԁ#3547-04-4ison_CAAA_,Thelargevolumepesticideis72-55-9.Thetwoaresimilar(almostcongeners)andshouldbehave &  comparably.  '! 334-88-3  P(" _Diazomethane_  P(" n,_kp_  P(" -  P(" -  P(" Veryreactive.Derivativemethodshouldbedeveloped.  (^# 132-64-9   *$ _Dibenzofurans_ 5+  *$  $@10$@50010 5+) *$  $@10 $@ 5f1   *$ 35428270C#  ǯI#ǯ      *$ For_PCDF_,useMethod0023AorMethod23   *$ 84-74-2  R+% 1,2-_Dibromo_-3-_Chloro_Ԅpropane 5+ +`&  $@10$@50010 5+)R+%  $@10 $@ 5f1f4  R+% 35428270C#  ǯ~#ǯ     R+%   R+% 84-74-2  "-' _Dibutylphthalate_ 5+ "-'  $@10$@50010 5+)"-'  $@10 $@ 5f1f4  "-' 35428270C#  ǯ<#ǯ     "-' Commoncontaminant  "-' 106-46-7  T.( 1,4-_Dichlorobenzene_(p) 5+ T.(  $@10$@50010 5+)T.(  $@10 $@ 5f1f2  T.( 35428270C#  ǯ#ǯ     T.(   T.( 91-94-1  d  3,3-_Dichlorobenzidene_  d 0010 d acidliquid   f4f5s   35428270C#  ǯ#ǯ    d _HPLC_/_PDA_   Reactive,nogoodwith0010.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ4#ǯ   .#  ǯP#ǯ       111-44-4  4  _Dichloroethyl_ԀEther 5+ 4   $@10$@50010 5+)4   $@10 $@ 5f1f2  4 35428270C#  ǯ#ǯ     4 Sameas_bis_(2-_chloroethyl_)ether  4 542-75-6  f 1,3-_Dichloropropene_  f 0030/00310010    f1f2f1f2    5041A8260B#  ǯ͜#ǯ    f 35428270C#  ǯK#ǯ       Mixedresults.Maybesourcesensitive.  f 62-73-7   6 _Dichlorvos_ 7-  6 $@0010$@70010 7-+ 6 $@0010 $@ 7f1f2   6 35428270C#  ǯ#ǯ      6    6 111-42-2   h  _Diethanolamine_   h! n,_kp_acidliquid   # -s   % 8270  h& _HPLC_Ԁshould   ' ThemethodofRef.50&51shouldcollectOKifmade_isokinetic_.Nobenzenering,soalternatedetectormaybeneeded  4 * 91667  f+ _N,N_-_Diethyl_Ԁaniline  f, 0010acidliquid  t . f1f2s  t 0 35428270C#  ǯ#ǯ    f1 _HPLC_/_PDA_  t 2 Compoundconfusedwith_Dimethylaniline_Ԁon_CAAA_,wrong_CAS_Ԁnumberlisted.Ref.50&51,prototypeneedstobe_isokinetic_#  ǯ#ǯ   .#  ǯǤ#ǯ      5 64-67-5  D 6 _Diethyl_ԀSulfate  D 7 n,_kp_  D 8 -  D 9 -  D : ProbablyspecialS&A.a.k.a.sulfuricacid,_diethyl_Ԁester  r < 119-90-4   = 3-3-_Dimethoxybenzidine_   > _kp_Ԁ0010  ? acidliquid  B @ f4l3s  B B 35428270C#  ǯ #ǯ     C _HPLC_/_PDA_  B D Likelyreactive.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ#ǯ   .#  ǯ#ǯ     B F 60-11-7  tG _Dimethyl__Aminoazobenzene_  I 0010?acidliquid  K f4l1s  M 35428270C#  ǯר#ǯ    tN _HPLC_/_PDA_  O Suspectreactivity.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ#ǯ   .#  ǯ#ǯ     Q 121697  DR _N,N_Ԅ_dimethylaniline_  DS 0010acidliquid  RU f2l1l4  RW 35428270C_HPLC_/_PDA_#  ǯY#ǯ     RY Incorrectlycalled_diethylaniline_Ԁon_CAAA_Ref50&51,prototypeneedstobe_isokinetic_#  ǯʬ#ǯ     R[ 119-93-7  \ 3,3-_Dimethyl_Ԁ_Benzidine_  ] 0010?_kp_acidliquid  "_ f1f4l3l4  "a 35428270C#  ǯ֭#ǯ    b _HPLC_/_PDA_  "c Mixedresultsprobablyduetoreactivity.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ&#ǯ     "e 79-44-7  Tf _Dimethyl_Ԁ_Carbamoyl_Chloride 5+ h  $@10$@50010 5+)Ti  $@10 $@ 5m,sp  Tj 8321A  Tk   Tl 68-12-2  $m _Dimethyl_Ԁ_Formamide_ 5+ $n  $@10$@50010 5+)$o  $@10 $@ 5m,sp  $p 8260B,8141A  $q   $r 57-14-7  Vs 1,1-_Dimethyl_Ԁ_Hydrazine_  Vt 0030?  Vu _kp_Ԁl7  Vv   Vw Stabilityproblems.Probablyneeds_derivatization_Ԁmethod.  y 131-11-3  &z _Dimethyl_ԀPhthalate 5+ &{  $@10$@50010 5+)&|  $@10 $@ 5f1  &} 35428270C#  ǯO#ǯ     &~ Commoncontaminant  & 77-78-1  X _Dimethyl_ԀSulfate  X special  X s  X special  X   X 534-52-1  ! 4,6-_Dinitro_-o-Cresol,andsalts 5+ !(  $@10$@50010 5+)!  $@10 $@ 5f1f2l3  ! 35428270C#  ǯ<#ǯ     ! Badlabresultsarepuzzling.Thistestwasforthecresolonly,notsalts.  !( 51-28-5  "Z 2,4-_Dinitrophenol_  "Z 0010?  "Z f1f4l3  "Z 35428270C#  ǯm#ǯ     "Z Mixedresults,verygoodtoverybad.  "Z 121-14-2  $ 2,4-_Dinitrotoluene_ 5+ $  $@10$@50010 5+)$  $@10 $@ 5f1  $ 35428270C#  ǯƸ#ǯ     $   $ 123-39-11  N% 1,4-_Dioxane_ ;1 N% k@00100030k@;00100030 ;1/%\  k@00100030 k@ ;f1l7  %\  35428270C#  ǯ5#ǯ     N% a.k.a.1,4_Diethyleneoxide_.Easilylostduringextractionandconcentration.Labeledlab.recoverystandardismandatory.  &  122-66-7  '," 1,2-_Diphenylhydrazine_  '," 0010acidliquid  Z(" ms  Z(" GC/MS_HPLC_/_PDA_  Z(" Reactive.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ#ǯ   .#  ǯ#ǯ     Z(" 106-89-8  )# _Epichlorohydrin_  )# 0010_kp_ )# 0030_kp_  **$ f2f4l3l7  **$ 35428270C#  ǯ7#ǯ     )# Mostlypoorwith0010,worsewith0030.Newmethodneeded.  **$ 106-88-7  \+% 1,2-_Epoxybutane_ 5+ \+%  >@30>@50030 5+)\+%  >@30 >@ 5_m,sp_  \+% 5040,(_GCMS_)  \+% Suspectreactivityproblems  \+% 140-88-5  ,& EthylAcrylate  ,& _kp_Ԁ0030?0010sorbent  -:( l8_m,sp_l4  -:( GC/MSGC/_FID_  -:( PolymerizeseasilyRef50&54.#  ǯ#ǯ     -:( 100-41-4  .l) EthylBenzene 5+ .l)  $@10$@50010 5+).l)  $@10 $@ 5f1  .l) 35428270C#  ǯ#ǯ     .l)   .l) 51-79-6  d EthylCarbamate  d 0010?  d f1f4l2  d 35428270C#  ǯ#ǯ     d a.k.a.urethane  d 75-00-3  & EthylChloride(_Chloroethane_)  4  0030?_kp_0031?_kp_  4  f2f4l1f4  4  5041A8260B5041A8260B#  ǯ#ǯ     4 Lowbp,0031shouldhavedonebetter.  & 106-93-4  f Ethylene_Dibromide_Ԁ  f 00100030?0031?  2  f1f2f1f4l1f1  2  35428270C#  ǯK#ǯ    f 5041A8260B#  ǯ#ǯ      5041A8260B#  ǯ#ǯ     2  a.k.a._dibromoethane_#  ǯX#ǯ   .Aboverecommendedbp f for0030/0031.    107-06-2  d  Ethylene_Dichloride_Ԁ ;1 d  OA00300031OA;00300031 ;1/ r! OA00300031 OA ;f1f2f1   r# 5041A8260B#  ǯ#ǯ    d $ 5041A8260B#  ǯk#ǯ      r% a.k.a.1,2_dichloroethane_  d & 107-21-1  4 ' EthyleneGlycol 5+ 4 (  $@10$@50010 5+)4 )  $@10 $@ 5s  4 * 8015B,8430  4 +   4 , 151-56-4  f- Ethylene_Imine_Ԁ(_Aziridine_)  f. n_kp_Ԁ0030  f/ l7  f0   f1 Watersoluble&polymerizes  f2 75-21-8   3 EthyleneOxide   4 _tedlar_Ԁbag_CARB_Ԁ431  6 6 f3   7 GC/MSGC/_FID_  6 9 Reactivitycancauseproblemsinsomematrices  6 ; 96-45-7  h < EthyleneThiourea 5+ h =  $@10$@50010 5+)h >  $@10 $@ 5m  h ? _HPLC_/UV8325  v A Reactiveandwatersoluble.SeeRef.56&57for_HPLC_/UV.  v C 75-34-3  8 D 1,1_dichloroethane_(misnamed_Ethylidene__Dichloride_Ԁon_CAAA_) ?5 H #ZA 003000310040#ZA?003000310040 ?53tK #ZA 003000310040 #ZA ?f1f2f1f1  tN 5041A8260B#  ǯ#ǯ    8 O 5041A8260B8260B#  ǯ#ǯ     tQ 75343isreally1,1_dichloroethane_._Ethylidene_Ԁ_dichloride_Ԁis75354  FS 50-00-0  DT Formaldehyde 7- DU &@0011&@70011 7-+DV &@0011 &@ 7f1  DW 8315A  DX Simultaneousaldehydespossible,ref.23&40  DY 76-44-8  vZ _Heptachlor_ 5+ v[  $@10$@50010 5+)v\  $@10 $@ 5f1f4l1  v] 35428270C#  ǯ#ǯ     v^   v_ 118-74-1  ` _Hexachlorobenzene_ 5+ a  $@10$@50010 5+)b  $@10 $@ 5f1f2f4  Fd 35428270C#  ǯ#ǯ     e Recoveryincreasedgreatlywitheachfieldtest.Lastonewas82.6%  Fg 87-68-3  xh _Hexachlorobutadiene_ 5+ xi  $@10$@50010 5+)xj  $@10 $@ 5f1f2  xk 35428270C#  ǯc#ǯ     xl   xm 77-47-4  n _Hexachlorocyclopentadiene_ 5+ o  $@10$@50010 5+)p  $@10 $@ 5f2f4  q 35428270C#  ǯ#ǯ     r Goodtomediocrefieldtests,poorinthelab.  s 67-72-1  Lt _Hexachloroethane_ 5+ Lu  $@10$@50010 5+)Lv  $@10 $@ 5f1  Lw 35428270C#  ǯG#ǯ     Lx   Ly 822-06-0  ~z _Hexamethylene_-1,6-_diisocyanate_  | M2071  ~} f1  ~~ M2072  ~ Reactive,a.k.a.1,6_diisocyanatohexane_a.k.a._HDI_   680-31-9  N _Hexamethylphosphoramide_ 5+ N  $@10$@50010 5+)N  $@10 $@ 5f4l3  N 35428270C#  ǯ#ǯ     N Suspectreactivity  N 110-54-3  ! Hexane ;1 !  PA00300040 PA;00300040 ;1/!  PA00300040  PA ;f1f1  ! 5041A#  ǯy#ǯ   8260B#  ǯ#ǯ    ! 8260B#  ǯ#ǯ     !   ! 302-01-2  "P _Hydrazine_ 7- "P $@0010$@70010 7-+"P $@0010 $@ 7_kp_  "P GC/MS  "P Watersoluble&unstable,probablyrequiresspecialS&A  ~# 7647-01-0  $  HydrochloricAcid  $  M26/26A00500051  N% f1  $  90569057  $  Halogens&halo-acidscanbedonesimultaneously  N% 7664-39-3  &  HydrogenFluoride  &  M26/26A  &  l4 7- &  @9057@79057 7-+&  @9057 @ 7Methods13A,13B,14#  ǯ\#ǯ   Ԁfortotalfluoride  &  123-31-9  '"" _Hydroquinone_ 5+ '""  $@10$@50010 5+)'""  $@10 $@ 5_m,sp_  '"" GC/MS  '"" Reactive,solubilityproblems.  '"" 78-59-1  (T# _Isophorone_ ;1 (T# j@00100011j@;00100011 ;1/)# j@00100011 j@ ;f1f1  )# 35428270C#  ǯ#ǯ    (T# 8315A#  ǯw#ǯ     )#   (T# 58-89-9  *$% Lindane(allisomers) 5+ *$%  $@10$@50010 5+)*$%  $@10 $@ 5f1  *$% 35428270C#  ǯ#ǯ     *$% a.k.a._hexachlorocyclohexane_  *$% 108-31-6  +V& MaleicAnhydride 5+ +V&  $@10$@50010 5+)+V&  $@10 $@ 5_s,kp_  +V& _HPLC_  +V& Reactswithwater,must_quantitate_Ԁtheacid&reportasparentcompound  ,& 67-56-1  -&( Methanol  -&( 0030?M308MST  .b) _m,sp_f1f1  .b) 5041A#  ǯ#ǯ   8260B#  ǯ#ǯ    -&( GC/_FID_GC/_FID_  .b) Highlywatersoluble,maypurgepoorlySeeReferences59,60,&61forevaluationofM308andMST.  .b) 72-43-5  d _Methoxychlor_ 5+ d  $@10$@50010 5+)d  $@10 $@ 5f2  d 35428270C#  ǯ#ǯ     d   d 74-83-9  & MethylBromide  & 0030?_kp_0031?_kp_0040?_kp_  b  f2f4f4  b 5041A8260B5041A8260B#  ǯ#ǯ    4 8260B#  ǯ#ǯ     b a.k.a._bromomethane_.0030barelymetf2,0031shouldbebetter,butwasworse.Lowbp.0040resultshigh.  b 74-87-3    MethylChloride(_Chloromethane_)  2  0030_kp_   0031_kp_ 2  0040   @ f4f4f1   @ 5041A8260B5041B8260B#  ǯ#ǯ    2  8260B#  ǯ#ǯ      @  ArtifactproblemswithTenax.   ! 71-55-6   r" MethylChloroform   r# 0030/00310040   % f1f1   ' 5041A8260B#  ǯz#ǯ   8260B#  ǯ#ǯ      ) a.k.a.1,1,1-_trichloroethane_   r* 78-93-3   B+ MethylEthylKetone(2-_Butanone_)  p- 0011  B. 0030?_PFHBA_  ~ 0 f4l8l4  ~ 3 8315A5041A8260BGC/_MSorECD_  ~ 6 Watersolubilitycausesproblemswith5041Apurge.SeeReferences45&50for_PFBHA_approach.#  ǯ#ǯ     ~ 9 60-34-4  @ : Methyl_Hydrazine_ 5+ @ ;  >@30>@50030 5+)@ <  >@30 >@ 5_kp_ 7- @ = @5040@75040 7-+@ > @5040 @ 7Reactive,probablyrequiresspecialS&A  @ ? 74-88-4  r @ Methyliodide  r A 0030/0031  r B f1  r C 5041A8260B#  ǯ8#ǯ     r D a.k.a._Iodomethane_#  ǯ#ǯ     r E 108-10-1   F Methyl_Isobutyl_ԀKetone(_Hexone_)  B H 00100011 B J _PFBHA__kp_Ԁ0030?#  ǯ #ǯ     ~L f1f4l4l8  ~P 35428270C#  ǯz#ǯ     Q 8315AGC/_MSorECD_  PS Seereferences45&50for_PFBHA_Ԁapproach,23&40for_DNPH_Ԁ(0011).#  ǯ#ǯ     B U 624-83-9   V MethylIsocyanate   W M2071#  ǯ#ǯ      X f1   Y M2072#  ǯ#ǯ      Z a.k.a.isocyanicacid,methylester,a.k.a.MI.SeeRef.18.  N\ 80-61-6  ] MethylMethacrylate  ^ 0010_kp_Ԁ0030?sorbent  ,a _m,sp_l8l4  ,d 5040,(GC/MS)GC/_FID_  ,g MaypolymerizeRef50&54.#  ǯ/#ǯ     ,j 1634-04-4  ^k Methyl_Tert_ԀButylEther  ^l _kp_Ԁ0030?  ^m l8  ^n   ^o a.k.a._tert_.butylmethylether  ^p 101-14-4   q 4,4-Methylene_Bis_(2-_chloroaniline_)  .s 0010acidliquid  .u _m,sp_s  .w GC/MS_HPLC_/_PDA_  .y Suspectreactivityproblemsduringsampling.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ#ǯ   .#  ǯU#ǯ     .{ 75-09-2  `| MethyleneChloride(_dichloromethane_)  ~ 0030/00310040   f1f1   5041A8260B8260B#  ǯ#ǯ      a.k.a._dichloromethane_  ` 101-68-8  0 Methylene_Diphenyl__Diisocyanate_  ^ M2071#  ǯ#ǯ     0 f1  0 M2072#  ǯ#ǯ     0 Reactive,SeeRef.18.#  ǯ_#ǯ   Ԁa.k.a._MDI,a.k.a._ 0 4,4'-_Bis_(_carbonylamino_)_diphenylmethane_.#  ǯ#ǯ     ^ 101-77-9    4,4-_Methylenedianiline_    0010acidliquid  .! m,sps  .! GC/MS_HPLC_/_PDA_  .! Reactive?Ref50&51,prototypeneedstobe_isokinetic_#  ǯ#ǯ   .#  ǯ#ǯ     .! 91-20-3  `" Naphthalene 5+ `"  $@10$@50010 5+)`"  $@10 $@ 5f1  `" 35428270C#  ǯ#ǯ     `"   `" 98-95-3  # Nitrobenzene 5+ #  $@10$@50010 5+)#  $@10 $@ 5f1  # 35428270C#  ǯ#ǯ     #   # 92-93-3  $4 4-_Nitrobiphenyl_ 5+ $4  $@10$@50010 5+)$4  $@10 $@ 5f1  $4 35428270C#  ǯ #ǯ     $4   $4 100-02-7  %f  4-_Nitrophenol_ 5+ %f   $@10$@50010 5+)%f   $@10 $@ 5f1f2l3  %f  35428270C#  ǯO #ǯ     %f  Badlabresultsarepuzzling.  %f  79-46-9  ('! 2-_Nitropropane_ 9/ ('! k@100030k@90010,0030 9/-('! k@100030 k@ 9s  ('! GC/MS  ('!   ('! 684-93-5  Z(" N-_Nitroso_-N-_Methylurea_ 5+ Z("  $@10$@50010 5+)Z("  $@10 $@ 5_m,sp_  Z(" _HPLC_  Z(" Unstable  Z(" 62-75-9  )# N-_Nitrosodimethylamine_ 5+ )#  $@10$@50010 5+))#  $@10 $@ 5f1  )# 35428270C#  ǯ #ǯ     )#   )# 59-89-2  *.% N-_Nitrosomorpholine_ 5+ *.%  $@10$@50010 5+)*.%  $@10 $@ 5f1  *.% 35428270C#  ǯ}#ǯ     *.%   *.% 56-38-2  +`& Parathion 5+ +`&  $@10$@50010 5+)+`&  $@10 $@ 5f1f2  +`& 35428270C#  ǯ#ǯ     +`&   +`& 82-68-8  "-' _Pentachloronitrobenzene_ 5+ "-'  $@10$@50010 5+)"-'  $@10 $@ 5f1f3f4  "-' GC/MS  "-'   "-' 87-86-5  T.( _Pentachlorophenol_ 5+ T.(  $@10$@50010 5+)T.(  $@10 $@ 5f1f3f4  T.( 35428270C#  ǯ#ǯ     T.(   T.( 108-95-2  d  Phenol  d 0010_NaOH_   f1f2f1   35428270C_HPLC_#  ǯA#ǯ      _NaOH_Ԁ_impinger_Ԁcollectionforemissionsinthe20100_ppm_Ԁrange.Refs.46,64,&65.#  ǯ#ǯ       106-50-3  4  p-_Phenylenediamine_  4  0010acidliquid  b _m,sp_s  b GC/MS_HPLC_/_PDA_  b Reactive,polar,watersoluble.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ#ǯ   .#  ǯv#ǯ     b 75-44-5    Phosgene    _XPHS_    l1    GC/MS    Reactive,mustbe_derivatized_Ԁascollected.SeeRefs.52&53.  2  7803-51-2  d  Phosphine  d  M290060  d  s  d  601060207000   r! YieldstotalPvalue  d " 7723-14-0  4 # Phosphorus  4 $ M290060#  ǯ#ǯ     4 % s  4 & 601060207000#  ǯ'#ǯ      B( _Yelds_ԀtotalPvalue  4 ) 85-44-9  t * Phthalicanhydride  t + 00100010_kp_   - sf4l3   / _HPLC_35428270C#  ǯ#ǯ      1 Reactswithwater,must_quantitate_Ԁtheacid&reportasparentcompound   3 1336-36-3  D 4 _Polychlorinated_Ԁ_Biphenyls_(_Aroclors_)  r 6 0010_CARB_Ԁ428  r 8 s  D 9 3542GC/MS_CARB_Ԁ428#  ǯ#ǯ     r ; Combustiondestroys_Aroclor_Ԁpatterns.Determineisomergroupsorindividuals.  r = 1120-71-4   > 1,3-Propane_Sultone_ 5+  ?  $@10$@50010 5+) @  $@10 $@ 5m   A GC/MS   B Polarandreactive.   C 57-57-8  FD Beta-_Propiolactone_ 5+ FE  $@10$@50010 5+)FF  $@10 $@ 5_m,sp_  FG GC/MS  FH Maybetooreactive  FI 123-38-6  xJ _Propionaldehyde_ 7- xK &@0011&@70011 7-+xL &@0011 &@ 7f1  xM 8315A  xN Simultaneousaldehydespossible.Ref.23&40  xO 114-26-1  :P _Propoxur_ 5+ :Q  $@10$@50010 5+):R  $@10 $@ 5f1f2  :S 35428270C#  ǯ+#ǯ     :T a.k.a._Baygon_  :U 78-87-5  lV Propylene_Dichloride_ ;1 lW OA00300031OA;00300031 ;1/ zY OA00300031 OA ;f1f2f1   z[ 5041A8260B#  ǯW$#ǯ    l\ 5041A8260B#  ǯ%#ǯ      z] a.k.a.1,2_dichloropropane_  l^ 75-56-9  <_ PropyleneOxide  <` _kp_0030 <a 0040  Jb l7m,sp  Jd   <e Reactive,watersoluble,a.k.a.1,2propyleneoxide  Jg 75-55-8   |h 1,2-_Propylenimine_   |i n_kp_Ԁ0030   |j l7   |k    |l Maybereactive   |m 91-25-5  >n _Quinoline_  >o 0010acidliquid  Lq f1l4  Ls 35428270C#  ǯI&#ǯ    >t _HPLC_/_PDA_  Lu Ref50&51,prototypeneedstobe_isokinetic_#  ǯ)#ǯ     Lw 106-51-4  ~x _Quinone_  ~y 0010 ~z 0011?  { f4l3kpf2,kp  } 35428270C#  ǯ*#ǯ    ~~ 8315A   Maybe_reactive,a.k.a._1,4-_benzoquinone,a.k.a._Ԁp-_benzoquinone_   100-42-5  N Styrene  N 0010?  N f1f4l1  N 35428270C#  ǯ+#ǯ     N Lowf4resultspuzzling.Reactivity?  N 96-09-3  ! StyreneOxide  ! 0010_kp_  ! f4l3  ! 35428270C#  ǯL-#ǯ     ! Reactive.a.k.a.1,2_epoxyethylbenzene_  ! 1746-01-6  B" 2,3,7,8-_Tetrachlorodibenzo_Լ-p-Dioxin  "P M230023A  "P f1  B" M238290  "P Specialcareneededduringrecoveryandanalysis.  "P 79-34-5  $ 1,1,2,2-_Tetrachloroethane_ 5+ $  $@10$@50010 5+)$  $@10 $@ 5f1  $ 35428270C#  ǯ.#ǯ     $   $ 127-18-4  D% _Tetrachloroethylene_Ԁ  D% 00100030/0031#  ǯ%1#ǯ     %R  f2f1f2  %R  35428270C#  ǯ2#ǯ    D% 5041A8260B#  ǯ2#ǯ     %R  a.k.a._tetrachloroethene_,.a.k.a_perchloroethylene_  %R  7550-45-0  '! TitaniumTetrachloride  '! M290060  '! s  '! 60106020#  ǯ2#ǯ    '! 7000#  ǯG4#ǯ     '"" Fortotaltitanium  '! 108-88-3  (T# Toluene ?5 (T# A 001000300040A?001000300040 ?53 *$ A 001000300040 A ?fif2f1f1   *$ 35428270C5041A#  ǯ4#ǯ   8260B#  ǯ6#ǯ    )# 8260B#  ǯH6#ǯ      *$   (T# 95-80-7  R+% 2,4-TolueneDiamine  R+% 0010acidliquid  +`& _m,sp_l4  +`& GC/MS_HPLC_/_PDA_  +`& ReactiveRef50&51,prototypeneedstobe_isokinetic_#  ǯ6#ǯ   .  +`& 584-84-9  "-' 2,4-Toluene_Diisocyanate_  "-' M2071  "-' f1  "-' M2072  "-' Reactswith_water,a.k.a._Ԁ_TDI_  "-' 95-53-4  T.( o-_Toluidine_  T.( 0010?acidliquid  .b) f2f4l1l4  .b) 35428270C#  ǯl8#ǯ    T.( _HPLC_/_PDA_  .b) Mixedresults,maybereactive.Ref50&51,prototypeneedstobe_isokinetic_#  ǯ:#ǯ   .  .b) 8001-35-2  d _Toxaphene_Ԁ(Chlorinated_Camphene_) 5+   $@10$@50010 5+)d  $@10 $@ 5s  d GC/MS,8250  d   d 120-82-1  4 1,2,4-_Trichlorobenzene_ 5+ 4   $@10$@50010 5+)4   $@10 $@ 5f1f2  4  35428270C#  ǯ;#ǯ     4    4  79-00-5  f 1,1,2-_Trichloroethane_  f 00100030/00310040  2  f1f2f1f1  2  35428270C#  ǯ(>#ǯ    f 5041A8260B8260B#  ǯL?#ǯ     2    f 79-01-6  d  Trichloroethylene  d  0030/0031  d  f1  d  5041A8260B#  ǯ?#ǯ     d  a.k.a._trichloroethene_  d  95-95-4     2,4,5-_Trichlorophenol_ 5+  !  $@10$@50010 5+) "  $@10 $@ 5f1   # 35428270C#  ǯ@#ǯ      $    % 88-06-2   8& 2,4,6-_Trichlorophenol_ 5+  8'  $@10$@50010 5+) 8(  $@10 $@ 5f1f2   8) 35428270C#  ǯ$B#ǯ      8*    8+ 121-44-8  j , _Triethylamine_  j - n_kp_Ԁ0030 j . acidliquid   / l7s   1 _HPLC_Ԁshould   3 a.k.a._N,N_-_diethylethanimine_.Suspectreactivity.#  ǯsC#ǯ   ԀThemethodofRef.50&51should  5 collectOK.Nobenzenering,soalternatedetectormaybeneeded#  ǯnE#ǯ     D 7 1582-09-8  v 8 _Trifluralin_  v 9 0010 v : acidliquid   ; f4l2kpm,_kp_   = 35428270C_HPLC_/_PDA_#  ǯ(F#ǯ      ? Suspectreactivity,a.k.a._Treflan_Ref50&51,prototypeneedstobe_isokinetic_#  ǯG#ǯ   .  A #  ǯH#ǯ   Analysismethodneedsmodification.  B B 540-84-1  tC 2,2,4-_Trimethylpentane_ ;1 tD  PA00300040 PA;00300040 ;1/F  PA00300040  PA ;f2f1  H 5041A8260B#  ǯH#ǯ    tI 8260B#  ǯ_J#ǯ     J a.k.a._isooctane_  tK 108-05-4  DL VinylAcetate  DM _kp_Ԁ0030?sorbent  RO l8l4  RQ GC/_FID_  RS Ref50&54.#  ǯJ#ǯ     RU 593-60-2  V VinylBromide  W 0030?_kp_0031?_kp_0040M106  ^[ f2f4l1f4f1  P^ 5041A8260B#  ǯ 60106020#  ǯj#ǯ    F? 7000  t@   FA Є  B _Polycyclic_ԀOrganicMatter  C 0010_CARB_Ԁ429  DE f3  F 35428270C#  ǯYk#ǯ    G _CARB_Ԁ429#  ǯl#ǯ     DH Individualcompoundsaredetermined,nottotalPOM,moreorlesssynonymouswith_pna_,_pah_,pac.  RK Є  L _Radionuclides_Ԁ(includingradon)  "N M111M114M115  PQ   R   S   T Є  U SeleniumCompounds  V M290060#  ǯ$m#ǯ     W f1  X 60107000#  ǯ@o#ǯ     Y #  ǯo# Z   PZ A ,A X2HX  A hA XHhXC XXX2HTRP'3 Letter Landscape3' '3 Letter Landscape3'TResultsforMethod0010_halogenated_Ԁcompoundslaboratorystudyandfivefieldtests. h *,r%-d d9dd dd 9dd Xdd dd dd %H81H81, d ,ttd ,tt ,$td%,td%,htd ,htd ,htd ,t ,htd ,t +  D%3 R lddDCompound e%V:*".%dd ddeFirstField V _Testa_ W%H,@"%dd ddWSecondField_Testb_ W%H,@"%dd ddWThirdField V  _Testc_ W%H,@ "%dd ddWLaboratory_Testd_ W%H,@ "%dd ddW_Margeson_,etal. V  TwoField_Testse_ lf]7@" l  %dd Lddl L%%%;#*fdd ddL#  XXCTp# Percent v Recovery R%%%A)"%%%dd ddRPercent v _RSD_ R%%%A)"%%%dd ddRPercent v Recovery R%%%A)"%%%dd ddRPercent v _RSD_ R%%%A)"%%%dd ddRPercent v Recovery# x#  R%%%A)"%%%dd ddRPercent v _RSD_# r{#  R%%%A)"%%%dd ddRPercent v Recovery R%%%A)"%%%dd ddRPercent v _RSD_# E|#XC X  R%%%A)"%%%dd ddR#  XXC}# Percent v Recovery# "~#XC X  R%%%A) "%%%dd ddR#  XXC~# Percent v! _RSD_# #XC X  SAF4"" L  %%%dd LS#  XXC#  _bis_(_chloromethyl_)ether DAA5v#A # D0.0 MAA>3v$U # AA M0.0 9AA*v%UAA 90.0 0AA!v&UAA 00.0 RAACv'AA 333333B@36.4333333B@R36.4 }AAnAv(U 333333B@36.4 333333B@AA 33333sF@44.933333sF@}44.9 [AALAv)U 33333sF@44.9 33333sF@AA [80.7 9AA*v*UAA 923.2 9AA*v+UAA 9Ј <AA-v,UAA <Ј IA<*v-U L AA <I_Epichlorohydrin_ 0AA!z.A 06.0 9AA*z/UAA 9128.1 0AA!z0UAA 013.4 'AAz1AA '44.2 RAACz2AA @M@58.5@M@R58.5 }AAnAz3U @M@58.5 @M@AA C@39.7C@}39.7 [AALAz4U C@39.7 C@AA [187.0 9AA*z5UAA 911.7 9AA*z6UAA 9Ј <AA-z7UAA <Ј IA<*z8U < AA <I_cis_Ԅ1,3_Dichloropropene_ 0AA!~9A 049.1 9AA*~:UAA 937.5 0AA!~;UAA 050.3 'AA~<AA '48.3 RAAC~=AA 33333sR@73.833333sR@R73.8 }AAnA~>U 33333sR@73.8 33333sR@AA 9@25.19@}25.1 [AALA~?U 9@25.1 9@AA [51.9 9AA*~@UAA 912.9 9AA*~AUAA 9Ј <AA-~BUAA <Ј IA<*~CU < AA <Itrans1,3_Dichloropropene_ PAAA DA  J@52J@P52.0 YAAJ? EU  J@52 J@AA Y35.2 0AA! FUAA 079.8 'AA GAA '63.4 RAAC HAA S@79.4S@R79.4 }AAnA IU S@79.4 S@AA fffff5@21.9fffff5@}21.9 [AALA JU fffff5@21.9 fffff5@AA [29.3 9AA* KUAA 913.1 9AA* LUAA 9Ј <AA- MUAA <Ј IA<* NU < AA <I1,1,2_Trichloroethane_ RAAC  OA 333333L@56.4333333L@R56.4 [AALA  PU 333333L@56.4 333333L@AA [37.7 RAAC  QUAA fffff&N@60.3fffff&N@R60.3 IAA:8  R fffff&N@60.3 fffff&N@AA I38.2 RAAC  SAA 33333S@79.833333S@R79.8 }AAnA  TU 33333S@79.8 33333S@AA 1@17.61@}17.6 [AALA  UU 1@17.6 1@AA [84.4 9AA*  VUAA 913.5 9AA*  WUAA 9Ј <AA-  XUAA <Ј IA<*  YU < AA <I1,2_Dibromoethane_ RAAC " ZA 33333sM@58.933333sM@R58.9 [AALA " [U 33333sM@58.9 33333sM@AA [36.9 RAAC " \UAA @O@62.5@O@R62.5 IAA:8 " ] @O@62.5 @O@AA I40.4 RAAC " ^AA 33333SU@85.333333SU@R85.3 }AAnA " _U 33333SU@85.3 33333SU@AA ffffff3@19.4ffffff3@}19.4 [AALA " `U ffffff3@19.4 ffffff3@AA [83.9 9AA* " aUAA 912.7 9AA* " bUAA 9Ј <AA- " cUAA <Ј IA<* " dU < AA <I_Tetrachloroethene_ RAAC & eA J@53.2J@R53.2 [AALA & fU J@53.2 J@AA [37.2 RAAC & gUAA 33333H@49.433333H@R49.4 IAA:8 & h 33333H@49.4 33333H@AA I52.5 RAAC & iAA 33333sR@73.833333sR@R73.8 }AAnA & jU 33333sR@73.8 33333sR@AA 33333>@30.733333>@}30.7 [AALA & kU 33333>@30.7 33333>@AA [78.7 9AA* & lUAA 917.6 9AA* & mUAA 9Ј <AA- & nUAA <Ј IA<* & oU < AA <I_Chlorobenzene_ RAAC * pA fffff&O@62.3fffff&O@R62.3 [AALA * qU fffff&O@62.3 fffff&O@AA [43.2 RAAC * rUAA fffffFP@65.1fffffFP@R65.1 IAA:8 * s fffffFP@65.1 fffffFP@AA I40.7 RAAC * tAA S@76.4S@R76.4 }AAnA * uU S@76.4 S@AA 3333332@18.23333332@}18.2 [AALA * vU 3333332@18.2 3333332@AA [86.2 9AA* * wUAA 911.9 9AA* * xUAA 986/86 <AA- * yUAA <22/14 IA<* * zU < AA <I_Bromoform_ RAAC. {A fffffM@59.8fffffM@R59.8 [AALA. |U fffffM@59.8 fffffM@AA [37.6 RAAC. }UAA 33333SQ@69.333333SQ@R69.3 IAA:8. ~ 33333SQ@69.3 33333SQ@AA I35.7 RAAC. AA U@87.0U@R87.0 }AAnA. U U@87.0 U@AA L1@17.3L1@}17.3 [AALA. U L1@17.3 L1@AA [123.0 9AA*. UAA 914.2 9AA*. UAA 9Ј <AA-. UAA <Ј IA<*. U < AA <I1,1,2,2_Tetrachloroethane_ RAAC2A P@64.0P@R64.0 [AALA2U P@64.0 P@AA [35.3 RAAC2UAA yR@73.9yR@R73.9 IAA:82 yR@73.9 yR@AA I34.5 RAAC2AA lT@81.7lT@R81.7 }AAnA2U lT@81.7 lT@AA 2@18.52@}18.5 [AALA2U 2@18.5 2@AA [79.7 9AA*2UAA 910.5 [AAL2UAA `T@81.5`T@[81.5 AAqA2U `T@81.5 `T@AA 33333s@@32.933333s@@32.9 kA^L2U 33333s@@32.9 < 33333s@@AA <k_Dichloroethyl_Ԁether RAAC6A 33333sN@60.933333sN@R60.9 [AALA6U 33333sN@60.9 33333sN@AA [34.7 RAAC6UAA @S@77.0@S@R77.0 IAA:86 @S@77.0 @S@AA I34.3 RAAC6AA 33333T@80.333333T@R80.3 }AAnA6U 33333T@80.3 33333T@AA ffffff1@17.4ffffff1@}17.4 [AALA6U ffffff1@17.4 ffffff1@AA [82.5 9AA*6UAA 910.5 9AA*6UAA 9Ј <AA-6UAA <Ј IA<*6U < AA <I1,4_Dichlorobenzene_ RAAC:A L@56.2L@R56.2 [AALA:U L@56.2 L@AA [35.2 RAAC:UAA `R@73.5`R@R73.5 IAA:8: `R@73.5 `R@AA I35.7 RAAC:AA  U@84.2 U@R84.2 }AAnA:U  U@84.2  U@AA /@15.9/@}15.9 [AALA:U /@15.9 /@AA [78.7 9AA*:UAA 912.5 9AA*:UAA 9Ј <AA-:UAA <Ј IA<*:U < AA <IBenzylchloride RAAC>A P@67.4P@R67.4 [AALA>U P@67.4 P@AA [33.4 RAAC>UAA yR@73.9yR@R73.9 IAA:8> yR@73.9 yR@AA I34.9 RAAC>AA fffffT@82.1fffffT@R82.1 }AAnA>U fffffT@82.1 fffffT@AA fffff4@20.9fffff4@}20.9 [AALA>U fffff4@20.9 fffff4@AA [77.9 9AA*>UAA 911.7 9AA*>UAA 9Ј <AA->UAA <Ј IA<*>U < AA <I_Hexachloroethane_ RAACBA R@74.0R@R74.0 [AALABU R@74.0 R@AA [36.9 RAACBUAA Q@70.9Q@R70.9 IAA:8B Q@70.9 Q@AA I35.6 RAACBAA fffffT@83.6fffffT@R83.6 }AAnABU fffffT@83.6 fffffT@AA /@15.5/@}15.5 [AALABU /@15.5 /@AA [84.6 9AA*BUAA 913.3 9AA*BUAA 9Ј <AA-BUAA <Ј IA<*BU < AA <I1,2_Dibromo_Ԅ3_chloropropane_ RAACFA ffffffF@44.8ffffffF@R44.8 [AALAFU ffffffF@44.8 ffffffF@AA [36.0 RAACFUAA 33333sR@73.833333sR@R73.8 IAA:8F 33333sR@73.8 33333sR@AA I35.7 RAACFAA 33333U@84.333333U@R84.3 }AAnAFU 33333U@84.3 33333U@AA 0@16.80@}16.8 [AALAFU 0@16.8 0@AA [69.8 9AA*FUAA 911.4 9AA*FUAA 9Ј <AA-FUAA <Ј IA<*FU < AA <I1,2,4_Trichlorobenzene_ RAACJA M@59.5M@R59.5 [AALAJU M@59.5 M@AA [35.7 RAACJUAA fffffS@76.1fffffS@R76.1 IAA:8J fffffS@76.1 fffffS@AA I34.5 RAACJAA 33333U@86.833333U@R86.8 }AAnAJU 33333U@86.8 33333U@AA ffffff,@14.2ffffff,@}14.2 [AALAJU ffffff,@14.2 ffffff,@AA [67.7 9AA*JUAA 913.3 9AA*JUAA 9Ј <AA-JUAA <Ј IA<*JU < AA <I_Hexachlorobutadiene_ RAACNA YP@65.4YP@R65.4 [AALANU YP@65.4 YP@AA [43.1 RAACNUAA fffffFS@77.1fffffFS@R77.1 IAA:8N fffffFS@77.1 fffffFS@AA I34.3 RAACNAA ,U@84.7,U@R84.7 }AAnANU ,U@84.7 ,U@AA 0@16.60@}16.6 [AALANU 0@16.6 0@AA [68.1 9AA*NUAA 914.0 9AA*NUAA 9Ј <AA-NUAA <Ј IA<*NU < AA <I_Benzotrichloride_ RAACRA  N@60.1 N@R60.1 [AALARU  N@60.1  N@AA [36.5 RAACRUAA R@72.4R@R72.4 IAA:8R R@72.4 R@AA I38.0 RAACRAA R@75.2R@R75.2 }AAnARU R@75.2 R@AA 4@20.54@}20.5 [AALARU 4@20.5 4@AA [85.7 9AA*RUAA 916.8 9AA*RUAA 9Ј <AA-RUAA <Ј IA<*RU < AA <I2_Chloroacetophenone_ RAACVA L@56.0L@R56.0 [AALAVU L@56.0 L@AA [40.7 RAACVUAA S@79.5S@R79.5 IAA:8V S@79.5 S@AA I32.7 RAACVAA fffffP@66.1fffffP@R66.1 }AAnAVU fffffP@66.1 fffffP@AA LF@44.6LF@}44.6 [AALAVU LF@44.6 LF@AA [89.1 9AA*VUAA 911.7 9AA*VUAA 9Ј <AA-VUAA <Ј IA<*VU < AA <I_Hexachlorocyclopentadiene_ 0AA!ZA 042.3 9AA*ZUAA 961.8 RAACZUAA M@59.6M@R59.6 IAA:8Z M@59.6 M@AA I37.7 RAACZAA  Q@68.5 Q@R68.5 }AAnAZU  Q@68.5  Q@AA ̌A@35.1̌A@}35.1 [AALAZU ̌A@35.1 ̌A@AA [975.5 9AA*ZUAA 924.8 9AA*ZUAA 9Ј <AA-ZUAA <Ј IA<*ZU < AA <I2,4,6_Trichlorophenol_ RAAC^A fffffH@49.8fffffH@R49.8 [AALA^U fffffH@49.8 fffffH@AA [47.0 RAAC^UAA R@75.4R@R75.4 IAA:8^ R@75.4 R@AA I35.2 RAAC^AA fffffFS@77.1fffffFS@R77.1 }AAnA^U fffffFS@77.1 fffffFS@AA /@15.8/@}15.8 [AALA^U /@15.8 /@AA [72.8 9AA*^UAA 926.2 9AA*^UAA 9Ј <AA-^UAA <Ј IA<*^ U < AA <I2,4,5_Trichlorophenol_ RAACb A YO@62.7YO@R62.7 [AALAb U YO@62.7 YO@AA [35.3 RAACb UAA fffff&S@76.6fffff&S@R76.6 IAA:8b  fffff&S@76.6 fffff&S@AA I34.5 RAACbAA ,T@80.7,T@R80.7 }AAnAbU ,T@80.7 ,T@AA 0@16.10@}16.1 [AALAbU 0@16.1 0@AA [76.1 9AA*bUAA 923.8 9AA*bUAA 9Ј <AA-bUAA <Ј IA<*bU < AA <I_Hexachlorobenzene_ 0AA!fA 044.6 9AA*fUAA 933.9 RAACfUAA @L@56.5@L@R56.5 IAA:8f @L@56.5 @L@AA I31.0 RAACfAA fffffT@82.6fffffT@R82.6 }AAnAfU fffffT@82.6 fffffT@AA ffffff)@12.7ffffff)@}12.7 [AALAfU ffffff)@12.7 ffffff)@AA [73.3 9AA*fUAA 910.0 9AA*fUAA 9Ј <AA-fUAA <Ј IA<*fU < AA <I_Pentachlorophenol_ 0AA!j A 042.4 9AA*j!UAA 941.5 RAACj"UAA fffff&N@60.3fffff&N@R60.3 IAA:8j# fffff&N@60.3 fffff&N@AA I25.6 RAACj$AA 33333P@64.333333P@R64.3 }AAnAj%U 33333P@64.3 33333P@AA H@49.2H@}49.2 [AALAj&U H@49.2 H@AA [57.5 9AA*j'UAA 960.3 ZAAKj(UAA _@124_@Z124 AAp@j)U _@124 _@AA fffff&G@46.3fffff&G@46.3 kA^Lj*U fffff&G@46.3 < fffff&G@AA <k_Pentachloronitrobenzene_ 0AA!n+A 043.4 9AA*n,UAA 937.9 RAACn-UAA @M@58.5@M@R58.5 IAA:8n. @M@58.5 @M@AA I28.9 RAACn/AA U@87.5U@R87.5 }AAnAn0U U@87.5 U@AA /@15.8/@}15.8 [AALAn1U /@15.8 /@AA [79.2 9AA*n2UAA 910.1 9AA*n3UAA 9Ј <AA-n4UAA <Ј IA<*n5U < AA <I_Chlorobenzilate_ 0AA!r6A 040.7 9AA*r7UAA 950.6 RAACr8UAA fffffN@61.8fffffN@R61.8 IAA:8r9 fffffN@61.8 fffffN@AA I33.1 RAACr:AA S@78.0S@R78.0 }AAnAr;U S@78.0 S@AA 1@17.01@}17.0 [AALAr<U 1@17.0 1@AA [131.6 9AA*r=UAA 932.0 9AA*r>UAA 9Ј <AA-r?UAA <Ј EA8*r@U < AA < E3,3'_Dichlorobenzidine_ 3AA$ vA A 34.4 <AA- vBUAA <164.9 3AA$ vCUAA 30.6 *AA vDAA *264.6 UAAF vEAA $@10.0$@U10.0 AAqA vFU $@10.0 $@AA 33333S@78.833333S@78.8 ^AAOA vGU 33333S@78.8 33333S@AA ^1352.4 <AA- vHUAA <43.4 <AA- vIUAA <Ј <AA- vJUAA  <Ј:0. vKU <0    AA :# p#]aMeanof12replicatequadtrainruns.Coalfiredpowerplant.Fromreferences8&9. !n K bMeanof4replicatequadtrainruns.Organicchemicalmanufacturingfacility.Fromreferences9,10&30.cMeanof10replicatequadtrainruns.Organicagriculturalchemicalmanufacturingfacility.Fromreferences10&17. f#!M dMeanof7replicatequadtrainruns.Fullscalesamplingtrain,dynamicspike,stacksimulator.Fromreference9. .$"N e#9]2#^9Meanof1339replicatequadtrainruns,withdynamicspiking.Twohazardouswasteincinerators.Fromreference#^M# #  #  Ԁ4.# F## #  $#O Q   XX QCResultsforMethod0010_nonhalogenated_Ԁorganiccompounds,laboratorystudyandfourfieldtests. h *r%d d d ttd tt $td%td%htd htd htd t htd t ,r%-H81H81, d ,Htd",tt",$td%,td%,htd",t",htd",t"+  D%3 X lddDCompound e%V:<"0z%dd ddeFirstField \ _Testa_ W%H,L"%dd ddWSecondField_Testb_ W%H,L"%dd ddWLaboratory \  _Testc_ W%H,L "%dd ddW_Margeson_,etal. \  TwoField_Testsd_ lf]7> " l  %dd Lddl L%%%;#. fdd ddL#Q XX$#( QPercent z Recovery R%%%A)"%%%dd ddRPercent z _RSD_ R%%%A)"%%%dd ddRPercent z Recovery R%%%A)"%%%dd ddRPercent z _RSD_#Q (#( Q R%%%A)"%%%dd ddRPercent z Recovery R%%%A)"%%%dd ddRPercent z _RSD_#Q (#XX Q R%%%A)"%%%dd ddR#Q XX#( QPercent z Recovery#Q (#XX Q R%%%A)"%%%dd ddR#Q XX#( QPercent z _RSD_#Q (#XX Q @64" L  %%%dd @#Q XX#L* Q_di_Ԅnbutylphthalate :A+ 0  G@46G@:46 gAX60  G@46 G@A  K@54K@g54 qAb60   K@54 K@A Z@107Z@q107 zAk@0!U Z@107 Z@A  ,@14,@z14 qAb?0"U  ,@14 ,@A ]@118]@q118 hAY70# ]@118 ]@A  $@10$@h10 GA860$  $@10 $@A G 'A0%A ' %A0&A %_bis_(2_ethylhexyl_)phthalate GAA8'A  H@48H@G48 gAAX6(  H@48 H@AA  7@237@g23 pAAa6)  7@23 7@AA  @P@65@P@p65 yAAj?*U  @P@65 @P@AA  @W@93@W@y93 qAAb?+U  @W@93 @W@AA [@110[@q110 hAAY7, [@110 [@AA  @@32@@h32 GAA86-  @@32 @@AA G 'AA.AA ' %A/AA %m/pcresol GAA8P 0A  @Q@69@Q@G69 gAAX6P 1  @Q@69 @Q@AA  ,@14,@g14 pAAa6P 2  ,@14 ,@AA  @P@65@P@p65 yAAj?P 3U  @P@65 @P@AA  H@49H@y49 qAAb?P 4U  H@49 H@AA @Z@105@Z@q105 gAAX7P 5 @Z@105 @Z@AA  @5@g5 FAA75P 6  @5 @AA F 'AAP 7AA ' %AP 8AA %_dimethyl_Ԁphthalate GAA8 D 9A  T@82T@G82 gAAX6 D :  T@82 T@AA  1@171@g17 qAAb6 D ;  1@17 1@AA ^@123^@q123 yAAj@ D <U ^@123 ^@AA  @7@y7 pAAa> D =U  @7 @AA @Z@105@Z@p105 gAAX7 D > @Z@105 @Z@AA  "@9"@g9 FAA75 D ?  "@9 "@AA F 'AA D @AA ' %A D AAA %phenol GAA8 BA  @V@89@V@G89 fAAW6 C  @V@89 @V@AA  "@9"@f9 oAA`5 D  "@9 "@AA  L@56L@o56 yAAj? EU  L@56 L@AA  6@226@y22 pAAa? FU  6@22 6@AA  X@96X@p96 fAAW6 G  X@96 X@AA  @7@f7 fAAW5 H  @7 @AA  X@96X@f96 gAAX6 I  X@96 X@AA  ,@14,@g14 EA86 J  ,@14 ,@AA Eocresol GAA8d KA  V@90V@G90 gAAX6d L  V@90 V@AA  .@15.@g15 pAAa6d M  .@15 .@AA  Q@71Q@p71 yAAj?d NU  Q@71 Q@AA  A@34A@y34 qAAb?d OU  A@34 A@AA Y@100Y@q100 gAAX7d P Y@100 Y@AA  @5@g5 FAA75d Q  @5 @AA F 'AAd RAA ' %Ad SAA %2,4_dinitrophenol_ HAA9XTA [@111[@H111 hAAY7XU [@111 [@AA  ?@31?@h31 pAAa6XV  ?@31 ?@AA  8@248@p24 yAAj?XWU  8@24 8@AA  U@87U@y87 oAA`?XXU  U@87 U@AA  @5@o5 gAAX5XY  @5 @AA `c@155`c@g155 HAA97XZ `c@155 `c@AA H 'AAX[AA ' %AX\AA %4_nitrophenol_ HAA9]A \@114\@H114 hAAY7^ \@114 \@AA  ?@31?@h31 pAAa6_  ?@31 ?@AA  M@59M@p59 yAAj?`U  M@59 M@AA  2@182@y18 pAAa?aU  2@18 2@AA  C@38C@p38 gAAX6b  C@38 C@AA  @@33@@g33 GAA86c  @@33 @@AA G 'AAdAA ' %AeAA %4,6_dinitro_Ԅocresol HAA9xfA ^@122^@H122 hAAY7xg ^@122 ^@AA  ,@14,@h14 pAAa6xh  ,@14 ,@AA  J@53J@p53 yAAj?xiU  J@53 J@AA  A@34A@y34 pAAa?xjU  A@34 A@AA  F@44F@p44 gAAX6xk  F@44 F@AA  F@44F@g44 GAA86xl  F@44 F@AA G 'AAxmAA ' %AxnAA %_quinone_ FAA7loA  @2@F2 gAAX5lp  @2 @AA `{@438`{@g438 LAA=7lq `{@438 `{@AA Lnottested JAA;lrAA  <@28<@J28 gAAX6ls  <@28 <@AA  @X@97@X@g97 GAA86lt  @X@97 @X@AA G 'AAluAA ' %AlvAA %_hexamethylphosphoramide_ GAA80wA  ,@14,@G14 hAAY60x  ,@14 ,@AA ]@118]@h118 LAA=70y ]@118 ]@AA Lnottested#Q *Lџ#L* QԈ JAA;0zAA  H@49H@J49 gAAX60{  H@49 H@AA  R@74R@g74 GAA860|  R@74 R@AA G 'AA0}AA ' %A0~AA %_trifluralin_ GAA8$A  ;@27;@G27 gAAX6$  ;@27 ;@AA  D@41D@g41 KAA<6$  D@41 D@AA Knottested#Q *L-#L* QԈ KAA<$AA b@149b@K149 hAAY7$ b@149 b@AA  &@11&@h11 GAA86$  &@11 &@AA G 'AA$AA ' %A$AA %_dimethylaminoazo_Ԅbenzene GAA8A  ?@31?@G31 gAAX6  ?@31 ?@AA  I@51I@g51 pAAa6  I@51 I@AA  1@171@p17 yAAj?U  1@17 1@AA  P@67P@y67 qAAb?U  P@67 P@AA Z@106Z@q106 hAAY7 Z@106 Z@AA  0@160@h16 GAA86  0@16 0@AA G 'AAAA ' %AAA %3,3'_dimethoxybenzidine_ GAA8DA  B@37B@G37 gAAX6D  B@37 B@AA  C@38C@g38 oAA`6D  C@38 C@AA  @6@o6 yAAj>DU  @6 @AA  `@129 `@y129 qAAb@DU  `@129  `@AA  4@204@q20 gAAX6D  4@20 4@AA  I@50I@g50 GAA86D  I@50 I@AA G 'AADAA ' %ADAA %o_anisidine_ GAA88A  C@39C@G39 gAAX68  C@39 C@AA  C@39C@g39 oAA`68  C@39 C@AA  @4@o4 yAAj>8U  @4 @AA b@149b@y149 qAAb@8U b@149 b@AA  P@67P@q67 gAAX68  P@67 P@AA  1@171@g17 GAA868  1@17 1@AA G 'AA8AA ' %A8AA %o_toluidine_ GAA8A  L@56L@G56 gAAX6  L@56 L@AA  >@30>@g30 pAAa6  >@30 >@AA  8@248@p24 yAAj?U  8@24 8@AA  Q@70Q@y70 pAAa?U  Q@70 Q@AA  T@80T@p80 gAAX6  T@80 T@AA  6@226@g22 GAA86  6@22 6@AA G 'AAAA ' %AAA %_benzidine_ GAA8XA  @P@65@P@G65 hAAY6X  @P@65 @P@AA ]@119]@h119 pAAa7X ]@119 ]@AA   @8 @p8 xAAi>XU   @8  @AA  W@95W@x95 oAA`?XU  W@95 W@AA   @8 @o8 fAAW5X   @8  @AA  @T@81@T@f81 GAA86X  @T@81 @T@AA G 'AAXAA ' %AXAA %_N,N_,_dimethylaniline_ GAA8LA  P@67P@G67 gAAX6L  P@67 P@AA  8@248@g24 pAAa6L  8@24 8@AA  K@54K@p54 yAAj?LU  K@54 K@AA  ?@31?@y31 pAAa?LU  ?@31 ?@AA  @X@97@X@p97 gAAX6L  @X@97 @X@AA  (@12(@g12 GAA86L  (@12 (@AA G 'AALAA ' %ALAA %aniline GAA8 A  Q@70Q@G70 gAAX6   Q@70 Q@AA  8@248@g24 pAAa6   8@24 8@AA  A@35A@p35 yAAj? U  A@35 A@AA  F@45F@y45 pAAa? U  F@45 F@AA  P@67P@p67 gAAX6   P@67 P@AA  &@11&@g11 GAA86   &@11 &@AA G 'AA AA ' %A AA %4,4'methylene_bis_(2_chloroaniline_) GAA8l! A  @V@89@V@G89 gAAX6l!   @V@89 @V@AA  B@36B@g36 pAAa6l!   B@36 B@AA  9@259@p25 yAAj?l! U  9@25 9@AA  H@49H@y49 pAAa?l! U  H@49 H@AA  R@75R@p75 gAAX6l!   R@75 R@AA  ;@27;@g27 GAA86l!   ;@27 ;@AA G 'AAl! AA ' %Al! AA %3,3'_dimethylbenzidine_ GAA8"`!A  W@92W@G92 gAAX6"`!  W@92 W@AA  F@44F@g44 oAA`6"`!  F@44 F@AA  @6@o6 yAAj>"`!U  @6 @AA  `@129 `@y129 qAAb@"`!U  `@129  `@AA  <@28<@q28 gAAX6"`!  <@28 <@AA  I@51I@g51 GAA86"`!  I@51 I@AA G 'AA"`!AA ' %A"`!AA %_N,N,diethylaniline_ GAA8$$"A  W@95W@G95 gAAX6$$"  W@95 W@AA  3@193@g19 pAAa6$$"  3@19 3@AA  K@54K@p54 yAAj?$$"U  K@54 K@AA  ?@31?@y31 qAAb?$$"U  ?@31 ?@AA Z@104Z@q104 hAAY7$$" Z@104 Z@AA  0@160@h16 GAA86$$"  0@16 0@AA G 'AA$$"AA ' %A$$"AA %carbaryl GAA8%$A  X@99X@G99 gAAX6%$  X@99 X@AA  3@193@g19 qAAb6%$  3@19 3@AA @_@125@_@q125 zAAk@%$U @_@125 @_@AA  I@51I@z51 pAAa?%$U  I@51 I@AA  W@94W@p94 gAAX6%$  W@94 W@AA  6@226@g22 GAA86%$  6@22 6@AA G 'AA%$AA ' %A%$AA %ethylcarbamate HAA9dA Y@103Y@H103 hAAY7d Y@103 Y@AA  ,@14,@h14 pAAa6d  ,@14 ,@AA  ;@27;@p27 yAAj?dU  ;@27 ;@AA  @@33@@y33 pAAa?dU  @@33 @@AA  @Q@69@Q@p69 gAAX6d  @Q@69 @Q@AA  5@215@g21 GAA86d  5@21 5@AA G 'AAdAA ' %Ad AA %_caprolactam_ HAA9 A \@114\@H114 hAAY7  \@114 \@AA  (@12(@h12 pAAa6   (@12 (@AA  6@226@p22 zAAk? U  6@22 6@AA Z@107Z@z107 qAAb@U Z@107 Z@AA  V@91V@q91 gAAX6  V@91 V@AA  2@182@g18 GAA86  2@18 2@AA G 'AAAA ' %AAA %N_nitrosomorpholine_ HAA9` A ]@116]@H116 hAAY7`  ]@116 ]@AA  (@12(@h12 pAAa6`   (@12 (@AA  @T@81@T@p81 yAAj?` U  @T@81 @T@AA  :@26:@y26 pAAa?` U  :@26 :@AA  @U@85@U@p85 gAAX6`   @U@85 @U@AA  7@237@g23 GAA86`   7@23 7@AA G 'AA` AA ' %A` AA %N_nitrosodimethylamine_ HAA9 xA @]@117@]@H117 hAAY7 x @]@117 @]@AA  *@13*@h13 pAAa6 x  *@13 *@AA  @T@81@T@p81 yAAj? xU  @T@81 @T@AA  ;@27;@y27 pAAa? x U  ;@27 ;@AA  X@96X@p96 fAAW6 x!  X@96 X@AA  "@9"@f9 FAA75 x"  "@9 "@AA F 'AA x#AA ' %A x$AA %_propoxur_ HAA9 %A ^@123^@H123 hAAY7 & ^@123 ^@AA  (@12(@h12 pAAa6 '  (@12 (@AA  R@75R@p75 yAAj? (U  R@75 R@AA  N@61N@y61 pAAa? )U  N@61 N@AA  @X@97@X@p97 gAAX6 *  @X@97 @X@AA  4@204@g20 GAA86 +  4@20 4@AA G 'AA ,AA ' %A -AA %2_acetylaminofluorene_ HAA9t 0.A `b@147`b@H147 hAAY7t 0/ `b@147 `b@AA  7@237@h23 pAAa6t 00  7@23 7@AA  H@49H@p49 yAAj?t 01U  H@49 H@AA  F@45F@y45 qAAb?t 02U  F@45 F@AA Z@106Z@q106 hAAY7t 03 Z@106 Z@AA  1@171@h17 GAA86t 04  1@17 1@AA G 'AAt 05AA ' %At 06AA %styreneoxide HAA97A ?0.5?H0.5 jAA[78 ?0.5 ?AA $@1481$@j1481 VAAG89 $@1481 $@AA Vnottested SAAD":UAA  H@49H@S49 gAAX6;  H@49 H@AA  P@66P@g66 GAA86<  P@66 P@AA G 'AA=AA ' %A>AA %phthalicanhydride FAA7, ?A  @5@F5 gAAX5, @  @5 @AA b@144b@g144 UAAF7, A b@144 b@AA Unottested RAAC", BUAA  @2@R2 gAAX5, C  @2 @AA a@136a@g136 HAA97, D a@136 a@AA H 'AA, EAA ' %A, FAA %_methoxychlor_ GAA8D GA  @R@73@R@G73 gAAX6D H  @R@73 @R@AA  3@193@g19 pAAa6D I  3@19 3@AA  R@75R@p75 yAAj?D JU  R@75 R@AA  I@51I@y51 pAAa?D KU  I@51 I@AA  @R@73@R@p73 gAAX6D L  @R@73 @R@AA  >@30>@g30 GAA86D M  >@30 >@AA G 'AAD NAA ' %AD OAA %toluene GAA8 PA  S@76S@G76 gAAX6 Q  S@76 S@AA  &@11&@g11 pAAa6 R  &@11 &@AA  @X@97@X@p97 yAAj? SU  @X@97 @X@AA  &@11&@y11 qAAb? TU  &@11 &@AA @u@340@u@q340 hAAY7 U @u@340 @u@AA  F@45F@h45 GAA86 V  F@45 F@AA G75/85 'AA WAA '26/15 %A XAA %m/pxylene GAA8@ YA  S@79S@G79 gAAX6@ Z  S@79 S@AA  (@12(@g12 pAAa6@ [  (@12 (@AA  S@79S@p79 yAAj?@ \U  S@79 S@AA  (@12(@y12 qAAb?@ ]U  (@12 (@AA Z@104Z@q104 gAAX7@ ^ Z@104 Z@AA  "@9"@g9 FAA75@ _  "@9 "@AA F 'AA@ `AA ' %A@ aAA %_quinoline_ GAA8XbA  T@80T@G80 gAAX6Xc  T@80 T@AA  3@193@g19 pAAa6Xd  3@19 3@AA  T@82T@p82 yAAj?XeU  T@82 T@AA  >@30>@y30 pAAa?XfU  >@30 >@AA  X@99X@p99 fAAW6Xg  X@99 X@AA   @8 @f8 FAA75Xh   @8  @AA F 'AAXiAA ' %AXjAA %styrene GAA8kA  U@84U@G84 gAAX6l  U@84 U@AA  $@10$@g10 pAAa6m  $@10 $@AA  C@39C@p39 yAAj?nU  C@39 C@AA  @T@81@T@y81 qAAb?oU  @T@81 @T@AA Z@104Z@q104 gAAX7p Z@104 Z@AA   @8 @g8 FAA75q   @8  @AA F 'AArAA ' %AsAA %oxylene GAA8TtA  @U@85@U@G85 gAAX6Tu  @U@85 @U@AA  &@11&@g11 pAAa6Tv  &@11 &@AA  @X@97@X@p97 xAAi?TwU  @X@97 @X@AA  "@9"@x9 pAAa>TxU  "@9 "@AA Y@103Y@p103 gAAX7Ty Y@103 Y@AA   @8 @g8 fAAW5Tz   @8  @AA  X@99X@f99 fAAW6T{  X@99 X@AA   @8 @f8 DA75T|   @8  @AA D1,4_dioxane_ GAA8l}A  U@87U@G87 gAAX6l~  U@87 U@AA  &@11&@g11 pAAa6l  &@11 &@AA  S@79S@p79 yAAj?lU  S@79 S@AA  5@215@y21 pAAa?lU  5@21 5@AA  W@92W@p92 fAAW6l  W@92 W@AA   @8 @f8 fAAW5l   @8  @AA  U@86U@f86 gAAX6l  U@86 U@AA  1@171@g17 EA86l  1@17 1@AA E_cumene_ GAA8 A  V@88V@G88 gAAX6   V@88 V@AA  &@11&@g11 pAAa6   &@11 &@AA  W@95W@p95 xAAi? U  W@95 W@AA  "@9"@x9 pAAa> U  "@9 "@AA Y@102Y@p102 gAAX7  Y@102 Y@AA  "@9"@g9 FAA75   "@9 "@AA F 'AA AA ' %A AA %_ethylbenzene_ GAA8h$A  @V@89@V@G89#Q *L#XX Q gAAX6h$  @V@89 @V@AA  (@12(@g#Q XXrq#L* Q12#Q *Lr#XX Q pAAa6h$  (@12 (@AA  @W@93@W@p#Q XX_r#L* Q93#Q *Ls#XX QԈ xAAi?h$U  @W@93 @W@AA  "@9"@x#Q XXUs#L* Q9#Q *Lt#XX QԈ oAA`>h$U  "@9 "@AA  W@94W@o#Q XXSt#L* Q94 gAAX6h$  W@94 W@AA  $@10$@g10 GAA86h$  $@10 $@AA G 'AAh$AA ' %Ah$AA %parathion GAA8A  @V@89@V@G89 gAAX6  @V@89 @V@AA  <@28<@g28 pAAa6  <@28 <@AA  S@76S@p76 yAAj?U  S@76 S@AA  <@28<@y28 pAAa?U  <@28 <@AA  X@96X@p96 gAAX6  X@96 X@AA  &@11&@g11 GAA86  &@11 &@AA G 'AAAA ' %AAA %_isophorone_ GAA8 A  @W@93@W@G93 gAAX6   @W@93 @W@AA  (@12(@g12 pAAa6   (@12 (@AA  X@96X@p96 yAAj? U  X@96 X@AA  *@13*@y13 qAAb? U  *@13 *@AA Z@106Z@q106 hAAY7  Z@106 Z@AA  *@13*@h13 GAA86   *@13 *@AA G 'AA AA ' %A AA %_acetophenone_ GAA8| 8A  X@96X@G96 gAAX6| 8  X@96 X@AA  (@12(@g12 pAAa6| 8  (@12 (@AA  X@98X@p98 yAAj?| 8U  X@98 X@AA  *@13*@y13 qAAb?| 8U  *@13 *@AA `@132`@q132 hAAY7| 8 `@132 `@AA  (@12(@h12 GAA86| 8  (@12 (@AA G 'AA| 8AA ' %A| 8AA %naphthalene GAA8!A  X@96X@G96 gAAX6!  X@96 X@AA  &@11&@g11 pAAa6!  &@11 &@AA  W@94W@p94 yAAj?!U  W@94 W@AA  $@10$@y10 qAAb?!U  $@10 $@AA Z@107Z@q107 gAAX7! Z@107 Z@AA   @8 @g8 gAAX5!   @8  @AA Z@106Z@g106 hAAY7! Z@106 Z@AA  0@160@h16 EA86!  0@16 0@AA E_dibenzofuran_ HAA94#A Y@100Y@H100 hAAY74# Y@100 Y@AA  (@12(@h12 qAAb64#  (@12 (@AA Y@103Y@q103 zAAk@4#U Y@103 Y@AA  (@12(@z12 qAAb?4#U  (@12 (@AA [@110[@q110 hAAY74# [@110 [@AA  &@11&@h11 GAA864#  &@11 &@AA G 'AA4#AA ' %A4#AA %_dichlorvos_ HAA9$LA @Y@101@Y@H101 hAAY7$L @Y@101 @Y@AA  2@182@h18 pAAa6$L  2@18 2@AA  L@57L@p57 yAAj?$LU  L@57 L@AA  ;@27;@y27 pAAa?$LU  ;@27 ;@AA  Q@68Q@p68 gAAX6$L  Q@68 Q@AA  >@30>@g30 GAA86$L  >@30 >@AA G 'AA$LAA ' %A$LAA %CX,Xh  G CX,Xh  G _DDE_ HAA9dA Y@102Y@H 102 hAAY7d Y@102 Y@AA  .@15.@h15 pAAa6d  .@15 .@AA  @W@93@W@p93 yAAj?dU  @W@93 @W@AA  8@248@y24 qAAb?dU  8@24 8@AA ^@120^@q120 hAAY7d ^@120 ^@AA  $@10$@h10 GAA86d  $@10 $@AA G 'AAdAA ' %Ad AA %4_nitrobiphenyl_ HAA9 A Y@102Y@H102 hAAY7  Y@102 Y@AA  ,@14,@h14 qAAb6   ,@14 ,@AA Z@104Z@q104 zAAk@ U Z@104 Z@AA  $@10$@z10 qAAb?U  $@10 $@AA Z@104Z@q104 hAAY7 Z@104 Z@AA  (@12(@h12 GAA86  (@12 (@AA G 'AAAA ' %AAA %_heptachlor_ HAA9P A Y@103Y@H103 hAAY7P  Y@103 Y@AA  (@12(@h12 pAAa6P   (@12 (@AA  A@35A@p35 zAAk?P U  A@35 A@AA Z@107Z@z107 qAAb@P U Z@107 Z@AA  W@95W@q95 fAAW6P   W@95 W@AA  "@9"@f9 FAA75P   "@9 "@AA F 'AAP AA ' %AP AA %_biphenyl_ HAA9 xA Y@103Y@H103 hAAY7 x Y@103 Y@AA  (@12(@h12 qAAb6 x  (@12 (@AA @Z@105@Z@q105 zAAk@ xU @Z@105 @Z@AA  (@12(@z12 qAAb? x U  (@12 (@AA Z@106Z@q106 gAAX7 x! Z@106 Z@AA  "@9"@g9 FAA75 x"  "@9 "@AA F 'AA x#AA ' %A x$AA %lindane HAA9 %A Z@104Z@H104 hAAY7 & Z@104 Z@AA  (@12(@h12 qAAb6 '  (@12 (@AA Z@104Z@q104 yAAj@ (U Z@104 Z@AA   @8 @y8 pAAa> )U   @8  @AA Z@107Z@p107 gAAX7 * Z@107 Z@AA  "@9"@g9 FAA75 +  "@9 "@AA F 'AA ,AA ' %A -AA %nitrobenzene HAA9d0.A @[@109@[@H109 hAAY7d0/ @[@109 @[@AA  (@12(@h12 qAAb6d00  (@12 (@AA Y@100Y@q100 zAAk@d01U Y@100 Y@AA  $@10$@z10 pAAa?d02U  $@10 $@AA  @X@97@X@p97 fAAW6d03  @X@97 @X@AA  "@9"@f9 gAAX5d04  "@9 "@AA @]@117@]@g117 hAAY7d05 @]@117 @]@AA  1@171@h17 EA86d06  1@17 1@AA E2,4_dinitrotoluene_ HAA97A @[@109@[@H109 hAAY78 @[@109 @[@AA  (@12(@h12 qAAb69  (@12 (@AA Y@102Y@q102 zAAk@:U Y@102 Y@AA  5@215@z21 qAAb?;U  5@21 5@AA [@110[@q110 hAAY7< [@110 [@AA  8@248@h24 GAA86=  8@24 8@AA G 'AA>AA ' %A?AA %methyl_isobutyl_Ԁketone HAA9 @A \@112\@H112 hAAY7 A \@112 \@AA  &@11&@h11 qAAb6 B  &@11 &@AA @Y@101@Y@q101 zAAk@ CU @Y@101 @Y@AA  &@11&@z11 qAAb? DU  &@11 &@AA Y@103Y@q103 gAAX7 E Y@103 Y@AA  "@9"@g9 FAA75 F  "@9 "@AA F 'AA GAA ' %A HAA %chlordane HAA9xD IA a@142a@H142 hAAY7xD J a@142 a@AA  0@160@h16 pAAa6xD K  0@16 0@AA  @U@85@U@p85 yAAj?xD LU  @U@85 @U@AA  9@259@y25 pAAa?xD MU  9@25 9@AA  @W@93@W@p93 gAAX6xD N  @W@93 @W@AA  ,@14,@g14 GAA86xD O  ,@14 ,@AA G 'AAxD PAA ' %AxD QAA %pyridine +AA RA +nottested 7AA( SAA 7nottested 7AA(" TUAA 7nottested *AA UAA *82/71 'AA VAA '24/18& W 9 AA &#Q *Lu#L* QaMeanof1020replicatequadtrainruns,withdynamicspiking.Coalfiredpowerplant.Fromreferences15&16.b#Q *L+#L* QԀMeanof819replicatequadtrainruns,withdynamicspiking.Chemicalmanufacturingfacilitywasteburner.Fromreferences13&14. \(Y c#Q *L#L* QMeanof614replicatequadtrainruns,withdynamicspiking.Sourcesimulator.Fromreferences11&16. $Z dMeanof1339replicatequadtrainruns,withdynamicspiking.Twohazardouswasteincinerators.Fromreference4.#Q *Lɪ##  Q#  [ F XXF X2HX  F XXF XY,XXX2HResultsforMethod0030_halogenated_Ԁcompoundslaboratorystudyandfourfieldtests.  *d :d d Htd"tt"$td%td%htd"t"htd"t"r%H81H81,xd ,9td ,tt ,9td%,tt%,9td%,tt%,dd%,t%,dd%,t%+  6ff'  dd6 Qf%B)Z"ffdd ddQFirstField_Testa_ Xf%%E,D|"f%dd ddXSecondField_Testb_ Xf%%E,D|"f%%dd ddXThirdField_Testc_ Xf%E,D|"f%%dd ddXLaboratory_Studiesd_ [ffH,D| "f%dd dd[_Fuerst_,etal. Z  Field_Teste_ cfT2D| " ffdd ddcCompound M%%>)"fdd ddM# ,XXY`# Percent  Recovery Q%%%>)\"%%dd ddQPercent  _RSD_ K%>)\"%%%dd ddKPercentRecovery Q%%%>)\"%dd ddQPercent_RSD_ K%>)\"%%%dd ddKPercent  Recovery# |#  Q%%%>)\"%dd ddQPercent  _RSD_# ĵ#  K%>)\"%%%dd ddKPercent  Recovery Q%%%>)\"%dd ddQPercent  _RSD_# #XY,X  K%>)\"%%%dd ddK# ,XXYݷ# Percent  Recovery# m#XY,X  Q%%f>)\ "%dd ddQ# ,XXYָ# Percent ! _RSD_# l#XY,X  R%fC4\""  %%fdd R# ,XXY#^- MethylChloride(_Chloromethane_) 0%A!J#%f 0937 9%A*J$U%A 953.8 9%A*J%U%A 9243 0%A!J&U%A 062.8 0%A!J'%A 0255.3 9%A*J(U%A 958.1 9%A*J)U%A 9101.2 0%A!J*U%A 08.10 0%A!J+%A 0Ј 4%Af!J,U%A 4Ј ?Af0!J-  %Af x?_Ethylidene_Ԁ_Dichloride_Ԁ(1,1_Dichloroethane_) RAACBz.Af R@75.7R@R75.7 [AALABz/U R@75.7 R@AA [13.7 RAACBz0UAA ̌T@82.2̌T@R82.2 IAA:8Bz1 ̌T@82.2 ̌T@AA I23.3 0AA!Bz2AA 086.0 9AA*Bz3UAA 913.2 0AA!Bz4UAA 0108.8 'AABz5AA '3.97 'AABz6AA 'Ј +AAfBz7AA +Ј ?Af0!Bz8 x AAf x?_Chlorobenzene_ RAACr 9Af  V@88.2 V@R88.2 [AALAr :U  V@88.2  V@AA [22.0 RAACr ;UAA LT@81.2LT@R81.2 IAA:8r < LT@81.2 LT@AA I22.1 0AA!r =AA 084.8 9AA*r >UAA 927.9 0AA!r ?UAA 094.2 'AAr @AA '14.56 'AAr AAA 'Ј +AAfr BAA +Ј ?Af0!r C x AAf x?VinylChloride SAAD DAf [@110.4[@S110.4 \AAMB EU [@110.4 [@AA \27.3 0AA! FUAA 041.8 'AA GAA '44.6 0AA! HAA 037.3 9AA* IUAA 939.5 0AA! JUAA 090.4 'AA KAA '12.01 'AA LAA 'Ј +AAf MAA +Ј ?Af0! N x AAf x?_Vinylidene_ԀChloride(1,1_Dichloroethylene_) PAAA OAf  V@88V@P88.0 YAAJ? PU  V@88 V@AA Y31.3 0AA! QUAA 077.8 'AA RAA '24.2 0AA! SAA 077.8 9AA* TUAA 925.1 0AA! UUAA 0123.0 'AA VAA '4.56 'AA WAA 'Ј +AAf XAA +Ј ?Af0! Y x AAf x?Chloroform RAAC : ZAf 33333sT@81.833333sT@R81.8 [AALA : [U 33333sT@81.8 33333sT@AA [14.8 RAAC : \UAA 33333V@91.333333V@R91.3 IAA:8 : ] 33333V@91.3 33333V@AA I24.6 0AA! : ^AA 095.3 9AA* : _UAA 914.3 0AA! : `UAA 0117.4 'AA : aAA '4.92 HAA9 : bAA _@127_@H127 lAAfY7 : c _@127 _@AA  (@12(@l12 _AfPA : d  (@12 x (@AAf x_Propylene_Dichloride_Ԁ(1,2_Dichloropropane_) RAAC2j eAf P@67.2P@R67.2 [AALA2j fU P@67.2 P@AA [9.6 QAAB2j gUAA @^@121@^@Q121 HAA972j h @^@121 @^@AA H24.8 0AA!2j iAA 0117.7 9AA*2j jUAA 930.0 0AA!2j kUAA 098.0 'AA2j lAA '9.52 'AA2j mAA 'Ј +AAf2j nAA +Ј ?Af0!2j o x AAf x?MethylBromide(_Bromomethane_) RAACbpAf J@53.7J@R53.7 [AALAbqU J@53.7 J@AA [20.2 RAACbrUAA ffffffK@54.8ffffffK@R54.8 IAA:8bs ffffffK@54.8 ffffffK@AA I26.2 0AA!btAA 052.8 9AA*buUAA 927.8 0AA!bvUAA 097.4 'AAbwAA '9.78 'AAbxAA 'Ј +AAfbyAA +Ј ?Af0!bz x AAf x?EthylChloride(_Chloroethane_) RAAC{Af fffff&I@50.3fffff&I@R50.3 [AALA|U fffff&I@50.3 fffff&I@AA [28.7 0AA!}UAA 033.7 'AA~AA '36.9 0AA!AA 031.4 9AA*UAA 937.6 0AA!UAA 095.8 'AAAA '11.2 'AAAA 'Ј +AAfAA +Ј ?Af0! x AAf x?MethyleneChloride RAACAf lS@77.7lS@R77.7 [AALAU lS@77.7 lS@AA [27.1 0AA!UAA 089.9 'AAAA '14.3 0AA!AA 090.8 9AA*UAA 911.7 0AA!UAA 0101.6 'AAAA '2.84 'AAAA 'Ј +AAfAA +Ј ?Af0! x AAf x?MethylChloroform(1,1,1_Trichloroethane_) QAAB*Af [@110[@Q110 ZAAK@*U [@110 [@AA Z43.5 RAAC*UAA fffffV@91.1fffffV@R91.1 IAA:8* fffffV@91.1 fffffV@AA I31.1 0AA!*AA 096.8 9AA**UAA 919.4 0AA!*UAA 0103.4 'AA*AA '12.28 'AA*AA 'Ј +AAf*AA +Ј ?Af0!* x AAf x?CarbonTetrachloride QAAB"ZAf Z@107Z@Q107 ZAAK@"ZU Z@107 Z@AA Z47.2 0AA!"ZUAA 081.2 'AA"ZAA '23.6 0AA!"ZAA 085.7 9AA*"ZUAA 913.8 0AA!"ZUAA 0108.4 'AA"ZAA '14.97 HAA9"ZAA [@108[@H108 kAAfX7"Z [@108 [@AA   @8 @k8 ^AfO@"Z   @8 x  @AAf x^Ethylene_Dichloride_Ԁ(1,2_Dichloroethane_) RAACRAf fffff&S@76.6fffff&S@R76.6 [AALARU fffff&S@76.6 fffff&S@AA [33.0 RAACRUAA 33333R@72.333333R@R72.3 IAA:8R 33333R@72.3 33333R@AA I37.5 0AA!RAA 078.6 9AA*RUAA 927.7 0AA!RUAA 095.8 'AARAA '6.19 'AARAA 'Ј +AAfRAA +Ј ?Af0!R x AAf x?Trichloroethylene QAABAf _@126_@Q126 ZAAK@U _@126 _@AA Z15.6 0AA!UAA 0119 'AAAA '26.2 0AA!AA 0124.0 9AA*UAA 916.8 0AA!UAA 0110.0 'AAAA '6.88 'AAAA 'Ј +AAfAA +Ј ?Af0! x AAf x?_cis_Ԅ1,3_Dichloropropene_ QAABAf  a@137 a@Q137 ZAAK@U  a@137  a@AA Z26.0 RAACUAA S@79.5S@R79.5 IAA:8 S@79.5 S@AA I27.6 0AA!AA 083.5 9AA*UAA 916.1 0AA!UAA 0109.0 'AAAA '14.59 'AAAA 'Ј +AAfAA +Ј ?Af0! x AAf x?trans1,3_Dichloropropene_ QAABAf `@135`@Q135 ZAAK@U `@135 `@AA Z38.1 0AA!UAA 052.3 'AAAA '35.4 0AA!AA 047.9 9AA*UAA 935.0 0AA!UAA 096.6 'AAAA '18.00 'AAAA 'Ј +AAfAA +Ј ?Af0! x AAf x?1,1,2_Trichloroethane_ PAAAJAf  X@98X@P98.0 YAAJ?JU  X@98 X@AA Y22.1 RAACJUAA S@79.7S@R79.7 IAA:8J S@79.7 S@AA I27.2 0AA!JAA 081.4 9AA*JUAA 914.4 0AA!JUAA 0106.4 'AAJAA '13.71 'AAJAA 'Ј +AAfJAA +Ј ?Af0!J x AAf x?_Tetrachloroethene_ RAACBzAf lX@97.7lX@R97.7 [AALABzU lX@97.7 lX@AA [21.9 RAACBzUAA  N@60.1 N@R60.1 IAA:8Bz  N@60.1  N@AA I27.9 0AA!BzAA 057.5 9AA*BzUAA 912.5 0AA!BzUAA 0111.6 'AABzAA '6.72 HAA9BzAA ^@122^@H122 kAAfX7Bz ^@122 ^@AA   @8 @k8 ^AfO@Bz   @8 x  @AAf x^MethylIodide(_Iodomethane_) 0AA!rAf 072.8 9AA*rUAA 937.6 0AA!rUAA 079.5 'AArAA '63.1 0AA!rAA 077.8 9AA*rUAA 920.4 0AA!rUAA 0108.4 'AArAA '5.28 'AArAA 'Ј +AAfrAA +Ј ?Af0!r x AAf x?AllylChloride(3_Chloropropene_) 0AA!Af 029.9 9AA*UAA 919.5 0AA!UAA 035.6 'AAAA '33.3 0AA!AA 036.4 9AA*UAA 929.6 0AA!UAA 0127.2 'AAAA '5.43 'AAAA 'Ј +AAfAA +Ј ?Af0! x AAf x?Ethylene_Dibromide_Ԁ(1,2_Dibromoethane_)G % # G 0AA! Af 034.9 9AA* UAA 931.6 RAAC UAA fffffS@79.6fffffS@R79.6 IAA:8  fffffS@79.6 fffffS@AA I37.4 0AA! AA 081.6 9AA* UAA 931.0 0AA! UAA 097.0 'AA AA '14.86 'AA AA 'Ј +AAf AA +Ј ?Af0!   x AAf x?Chloroprene 0AA! : Af 040.1 9AA* : UAA 922.4 0AA! : UAA 072.4 'AA : AA '23.0 0AA! :AA 076.4 9AA* :UAA 912.3 0AA! :UAA 0104.2 'AA :AA '4.31 'AA :AA 'Ј +AAf :AA +Ј ;Af,! : x AAf x;VinylBromide RAAC2!j Af YN@60.7YN@R60.7 [AALA2!j U YN@60.7 YN@AA [34.3 0AA!2!j UAA 029.8 'AA2!j AA '29.7 0AA!2!j AA 028.4 9AA*2!j UAA 930.9 0AA!2!j UAA 0110.8 'AA2!j AA '9.30 'AA2!j AA 'Ј +AAf2!j AA +# -^#  Ԉ 8Aff'!2!j  x0  AAf x8D #  #^- D _Trichlorofluoromethane_Ԁ(Freon11) 6AAf%"! Aff 6nottested 9AAf(""!!UAAf 9nottested 9AAf("!"AAf 9nottested 9AAf(""!#UAAf 9nottested LAAf;"!$AAf  @W@93@W@L93D # -^##D D   D kAAffX6"!%  @W@93 @W@AAf  $@10$@kE #  #^- E 10E # -^#E E   E LB@"!&  $@10 x0  $@AAff L#  %##  #9  aMeanofsixreplicatequadtrainruns,withdynamicspiking.Coalfiredpowerplant.Fromreferences8&9. #"& bMeanofeightreplicatequadtrainruns,withdynamicspiking.Organicchemicalmanufacturingfacility.Fromreferences9&31.cMeanofsixreplicatequadtrainruns,withdynamicspiking.Organicchemicalmanufacturingfacility.Fromreferences9,27,28&29.dMeanoffivereplicatequadtrainruns.Fullscalesamplingtrain,dynamicspike,stacksimulator.Fromreferences7&9.*.9 d%$) e#9.*$#Meanof1116replicatequadtrainruns,withdynamicspiking.HazardousWaste_Combustor_.Fromreference25.# 9#  &:%* Q   XX QC  ResultsforMethod0030_nonhalogenated_Ԁorganiccompounds,laboratorystudyandB fourB C threeC fieldtests.  *r%d dxd 9td tt 9td%tt%9td%tt%dd%t%dd%t%H81H81, d ,9td",tt",td%,td%,htd",t",htd",t"+  D%3  lddDCompound e%V:<"$%dd ddeFirstField $\ _Testa_ W%H,L"%dd ddWSecondField_Testb_ W%H,L"%dd ddWLaboratory $\  _Testc_ W%H,L "%dd ddW_Fuerst_,etal. $\  Field_Testd_ lf]7N " l  %dd Lddl L%%%;#> fdd ddL#Q XXd#( QPercent R  Recovery R%%%A)("%%%dd ddRPercent R _RSD_ R%%%A)("%%%dd ddRPercent R Recovery R%%%A)("%%%dd ddRPercent R _RSD_#Q (% #( Q R%%%A)("%%%dd ddRPercent R Recovery R%%%A)("%%%dd ddRPercent R _RSD_#Q (# #XX Q R%%%A)("%%%dd ddR#Q XXl#( QPercent R Recovery#Q (#XX Q R%%%A)("%%%dd ddR#Q XXf#( QPercent R _RSD_#Q (#XX Q @64(" L  %%%dd @#Q XX{#L* Q2,2,4_trimethylpentane_ <A- @ ̌O@63.1̌O@<63.1 kA\8@ ̌O@63.1 ̌O@A L2@18.3L2@k18.3 tAe8@ L2@18.3 L2@A R@75.9R@t75.9 }AnA@ U R@75.9 R@A 33333;@27.733333;@}27.7 RACA@!U 33333;@27.7 33333;@A R69/83 JA;@"A @@36170@@J13/11 JA;9@# @@36170 @@A J 'A@$A ' %A@%A %carbondisulfide IAA:d&A fffffO@63.8fffffO@I63.8 kAA\8d' fffffO@63.8 fffffO@AA 7@23.67@k23.6 tAAe8d( 7@23.6 7@AA E@42.0E@t42.0 }AAnAd)U E@42.0 E@AA 33333;@27.733333;@}27.7 RAACAd*U 33333;@27.7 33333;@AA R54/60#Q *L#L* Q 'AAd+AA '21/15 'AAd,AA ' 'AAd-AA ' %Ad.AA %nhexane IAA:/A S@79.2S@I79.2 kAA\80 S@79.2 S@AA 6@22.66@k22.6 tAAe81 6@22.6 6@AA 9W@92.99W@t92.9 }AAnA2U 9W@92.9 9W@AA 7@23.57@}23.5 RAACA3U 7@23.5 7@AA R88/105 JAA;4AA @36167@J13/8 JAA;95 @36167 @AA J 'AA6AA ' %A7AA %benzene JAA; T 8A 33333Z@106.333333Z@J106.3 lAA]9 T 9 33333Z@106.3 33333Z@AA 9@25.69@l25.6 uAAf8 T : 9@25.6 9@AA fffffY@100.1fffffY@u100.1 ~AAoB T ;U fffffY@100.1 fffffY@AA 7@23.67@~23.6 RAACA T <U 7@23.6 7@AA R66/99 JAA; T =AA @35981@J7/6 kAA\9 T > @35981 @AA Z@106Z@k106 gAAX7 T ? Z@106 Z@AA  @6@g6 DA75 T @  @6 @AA Dtoluene IAA:x AA yS@77.9yS@I77.9 kAA\8x B yS@77.9 yS@AA 1@17.51@k17.5 tAAe8x C 1@17.5 1@AA 33333X@98.833333X@t98.8 }AAnAx DU 33333X@98.8 33333X@AA L>@30.3L>@}30.3 RAACAx EU L>@30.3 L>@AA R60/* 'AAx FAA '21/* 'AAx GAA ' 'AAx HAA '#Q *Ly#XX Q&x I  AA &#Q XXd #L* QaMeanof9replicatequadtrainruns,withdynamicspiking.Coalfiredpowerplant.Fromreferences16&34.b#Q *L #L* QԀMeanof11replicatequadtrainruns,withdynamicspiking.Chemicalmanufacturingfacilitywasteburner.Fromreferences14&35. (` K c#Q *Lф!#L* QMeanof10replicatequadtrainruns,withdynamicspikingattwoconcentrationlevels.Sourcesimulator.Fromreferences11&16. (L dMeanof16replicatequadtrainruns,withdynamicspiking.Hazardouswaste_combustor_.Fromreference25.#Q *Ld"#L* Q M *Invalidresultsduetolaboratorycontamination.#*LE## ##  N XHXX2HX   X0XXX2HTRY3' LetterP'3 Letter Landscape3' Letter '3 Letter LandscapeTResultsforMethod0031fieldtestandMethod0040fieldtest.   *./ d d d 9td"tt"td%td%htd"t"htd"t"r%(#(#,, d ,td@,Htd@,td@,Ht@+  ?ff0  dd?Compound bf%S:(x"2ffdd ddbMethod0031 Xf%fE,H"f%dd ddXMethod0040 TJ7H"  f%fdd CT 0%%! \ dd0MeanPercent_Recoverya_ M%%>)  "%%dd ddMPercent_RSD_ M%%>)  "%%dd ddMMeanPercent_Recoveryb_ Q%%f>) "%%dd ddQPercent_RSD_ R%fC4 " C %%fdd ZR#90XX$#d79MethylChloride(_Chloromethane_) 0%A!< %f 0167.5 9%A*< U%A 956.4 Z%AK< U%A ^@123^@Z123 %Afm@< U ^@123 ^@%A fffff6@22.9fffff6@22.9 jAf[L< U fffff6@22.9 Z fffff6@%Af Jxj1,1_Dichloroethane_ 0AA!R Af 096.2 9AA*R UAA 912.6 [AALR UAA lW@93.7lW@[93.7 AAfnAR U lW@93.7 lW@AA 5@21.85@21.8 jAf[LR U 5@21.8 x J 5@AAf axj_Chlorobenzene_ 0AA!h Af 091.6 YAAJh UAA  *@13*@Y13.0 aAAfN?h U  *@13 *@AA anottested KAf<-h  " x a AAf axKVinylchloride 0AA!~ !Af 044.2 9AA*~ "UAA 924.2 ZAAK~ #UAA @[@109@[@Z109 AAfm@~ $U @[@109 @[@AA L9@25.3L9@25.3 jAf[L~ %U L9@25.3 x a L9@AAf Jxj_Vinylidene_ԀChloride(1,1-_Dichloroethene_) 0AA! &Af 096.8 9AA* 'UAA 917.2 [AAL (UAA 333333W@92.8333333W@[92.8 AAfnA )U 333333W@92.8 333333W@AA 8@24.18@24.1 jAf[L *U 8@24.1 x J 8@AAf axjChloroform 0AA! +Af 098.4 9AA* ,UAA 920.4 AAAf. -UAA Anottested KAf<- ." x a AAf JxKPropylene_Dichloride_(1,2-_Dichloropropane_) 0AA!^ 0Af 0149.4 9AA* 1UAA 914.0 AAAf. 2UAA Anottested KAf<- 3" x J AAf JxKMethylBromide(_Bromomethane_) 0AA!t4Af 045.7 9AA*t5UAA 946.7 ZAAKt6UAA e@168e@Z168 AAfm@t7U e@168 e@AA ?@31.6?@31.6 jAf[Lt8U ?@31.6 x J ?@AAf JxjEthylChloride(_Chloroethane_) 0AA!9Af 045.3 9AA*:UAA 930.0 AAAf.;UAA Anottested KAf<-<" x J AAf axKMethylenechloride 0AA!=Af 0120.7 9AA*>UAA 910.9 [AAL?UAA YW@93.4YW@[93.4 AAfnA@U YW@93.4 YW@AA 9@25.89@25.8 jAf[LAU 9@25.8 x a 9@AAf JxjMethylChloroform(1,1,1-_Trichloroethane_) 0AA!TCAf 087.1 9AA*DUAA 912.1 [AALEUAA 9W@92.99W@[92.9 AAfnAFU 9W@92.9 9W@AA fffff7@23.9fffff7@23.9 jAf[LGU fffff7@23.9 x J fffff7@AAf axjCarbontetrachloride 0AA!jHAf 089.3 9AA*jIUAA 912.5 ZAAKjJUAA @Y@101@Y@Z101 AAfm@jKU @Y@101 @Y@AA 5@21.65@21.6 jAf[LjLU 5@21.6 x a 5@AAf JxjEthylene_Dichloride_Ԁ(1,2-_Dichloroethane_) 0AA!MAf 083.2 9AA*NUAA 925.1 AAAf.OUAA Anottested KAf<-P" x J AAf axK_Trichloroethene_ 0AA!QAf 0148.7 9AA*RUAA 93.4 AAAf.SUAA Anottested KAf<-T" x a AAf axK_cis_Ԅ1,3_Dichloropropene_ SAADUAf ]@118.4]@S118.4 \AAMBVU ]@118.4 ]@AA \21.0 AAAf.WUAA Anottested KAf<-X" x a AAf axKtrans1,3_Dichloropropene_ 0AA!YAf 075.2 9AA*ZUAA 932.6 AAAf.[UAA Anottested KAf<-\" x a AAf axK1,1,2_Trichloroethane_ 0AA!(]Af 0117.3 9AA*(^UAA 920.5 [AAL(_UAA W@94.5W@[94.5 AAfnA(`U W@94.5 W@AA ffffff5@21.4ffffff5@21.4 jAf[L(aU ffffff5@21.4 x a ffffff5@AAf qxj_Tetrachloroethene_ 0AA!>bAf 061.8 9AA*>cUAA 98.0 AAAf.>dUAA Anottested KAf<->e" x q AAf ZKMethyliodide(_Iodomethane_) PAAA$ tfAf  @V@89@V@P89.0 YAAJ?$ tgU  @V@89 @V@AA Y11.9 AAAf.$ thUAA Anottested FAf7-$ ti" Z AAf xFAllylChloride(3-_Chloropropene_) 0AA!:!jAf 026.0 9AA*:!kUAA 921.1 [AAL:!lUAA T@82.0T@[82.0 AAfnA:!mU T@82.0 T@AA 9@25.69@25.6 eAfVG:!nU 9@25.6 x 9@AAf JxeEthylene_Dibromide_Ԁ(1,2-_Dibromoethane_) 0AA!P"oAf 0108.5 9AA*P"pUAA 923.2 AAAf.P"qUAA Anottested KAf<-P"r" x J AAf axKChloroprene 0AA!f#sAf 085.8 9AA*f#tUAA 915.3 AAAf.f#uUAA Anottested GAf8-f#v" x a AAf xGVinylBromide 0AA!|$wAf 038.0 9AA*|$xUAA 922.5 ZAAK|$yUAA \@112\@Z112 AAfm@|$zU \@112 \@AA ffffff:@26.4ffffff:@26.4 aAfRL|${U ffffff:@26.4 x0  ffffff:@AAf xaBenzene 4AA%%!|Af 4nottested \AAM"%!}"AA  X@98X@\98 AAfl?%!~U  X@98 X@AA fffff8@24.9fffff8@24.9 \AfMG%!U fffff8@24.9 x0 fffff8@AAf x\1,3Butadiene 4AA%'X"Af 4nottested ^AAO"'X""AA 33333sJ@52.933333sJ@^52.9 AAfnA'X"U 33333sJ@52.9 33333sJ@AA 33333sL@56.933333sL@56.9 aAfRG'X"U 33333sL@56.9 x0 33333sL@AAf Lxa_Dichlorodifluoromethane_Ԁ(Freon12) 4AA%N(#Af 4nottested ^AAO"N(#"AA ̌I@51.1̌I@^51.1 AAfnAN(#U ̌I@51.1 ̌I@AA 33333sN@60.933333sN@60.9 aAfRLN(#U 33333sN@60.9 x0 L 33333sN@AAf xanHexane 4AA%)$Af 4nottested ^AAO")$"AA W@94.0W@^94.0 AAfnA)$U W@94.0 W@AA 4@20.54@20.5 \AfMG)$U 4@20.5 x0 4@AAf x\Toluene 4AA%*0&Af 4nottested ^AAO"*0&"AA ,U@84.7,U@^84.7 AAfnA*0&U ,U@84.7 ,U@AA =@29.8=@29.8 \AfMG*0&U =@29.8 x0 =@AAf x\2,2,4_Trimethylpentane_ 4AA%&,v'Af 4nottested ]AAN"&,v'"AA @Z@105@Z@]105 AAfm@&,v'U @Z@105 @Z@AA 6@22.86@22.8 ^AffMG&,v'U 6@22.8 x0 6@AAf x^_Trichlorofluoromethane_Ԁ(Freon11) 6AAf%l-(Aff 6nottested _AAfN"l-("AAf @^@121@^@_121 AAffm@l-(U @^@121 @^@AAf ffffff8@24.4ffffff8@24.4WMKl-(U ffffff8@24.4 x0  ffffff8@AAff W#97d+#^9a#9^]#ԄMeanofsixreplicatequadtrainruns,withdynamicspiking.Organicchemicalmanufacturingfacility.Fromreferences9,28&29. .(* bMeanofelevenreplicatequadtrainruns,withdynamicspiking.Coalfiredpowerplant.Fromreferences1&2.# 9$#  >0+ C XXX   Q   9Z Q SELECTEDAIR_TOXICS_ԀMETHODSREFERENCES  X #Q 9Z_#XX Q1.0  #X2HXXX^#XXXX2H_McGaughey_,_J.F._,_Bursey_,_J.T._,#X2HXXX_#XXXX2HԀMerrill,_R.G._#X2HXXX`#XXXX2H,FieldEvaluationofEPAMethod0040 N (_Volatiles_ԀUsingBags),EPA600/R98/030,PB98133085,U.S.#X2HXXXLa#XXXX2HEnvironmental @ ProtectionAgency,ResearchTrianglePark,NC,January1998.#X2HXXX*b#XXXX2H2(#(# 2.0  #X2HXXXb#XXXX2H_McGaughey_,_J.F._,_Bursey_,_J.T._,Merrill,R.,G.,_Fuerst_,_R.G._ԀandJackson,M.D.,    FieldEvaluationofEPAProposedMethod0040(SamplingandAnalysisofVolatileCompoundsUsing_Tedlar_ԀBags),Proceedingsofthe#X2HXXX:c#XXXX2HԀEPA/A&_WMA_ԀInternational    Symposium:MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,April1997#X2HXXXJe#XXXX2H,VIP74,Air&WasteManagementAssociation,Pittsburgh,PA,1997,  |  pp#X2HXXX>f#XXXX2HԀ#X2HXXXf#XXXX2H159165. n (#(# #X2HXXXg#XXXX2H3.#X2HXXXg#XXXX2H0  #X2HXXXg#XXXX2HJohnson,_L.D._,"#X2HXXXh#XXXX2HResearchandEvaluationofOrganicHazardousAirPollutantSource N  EmissionTestMethods,"#X2HXXXh#XXXX2HԀ#X2HXXX9i#XXXX2HJ.Air&WasteManage.Assoc.,46,pp.11351148, > December1996.#X2HXXX|i#XXXX2H0(#(# 4.0  #X2HXXXj#XXXX2H_Margeson_,#X2HXXXj#XXXX2HԀ#X2HXXXj#XXXX2H_J.H._#X2HXXX5k#XXXX2H,Knoll,_J.E._#X2HXXXk#XXXX2H,_Midgett_,_M.R._,#X2HXXX l#XXXX2HԀWagoner,_D.E._,#X2HXXXl#XXXX2HRice,#X2HXXXm#XXXX2HԀJ.,#X2HXXXUm#XXXX2HԀand_Homolya_, h _J.B._,#X2HXXXm#XXXX2H"AnEvaluationofTheSemi_VOST_ԀMethodforDeterminingEmissionsfrom X HazardousWasteIncinerators,"J.Air_Pollut_.ControlAssoc.,37:(9)1067(1987).#X2HXXXDn#XXXX2HH(#(# #X2HXXXuo#XXXX2H5.0  Jackson,M.D.,Knoll,_J.E._,_Midgett_,_M.R._,_Bursey_,_J.T._,_McAllister_ԀR.A.,Merrill, * _R.G_,"Evaluationof_VOST_Ԁand_SemiVOST_ԀMethodsfor_Halogenated_ԀCompoundsintheCleanAirActAmendmentsTitleIII,BenchandLaboratoryStudies,"Proceedings   oftheNationalA&_WMA_ԀMeeting,KansasCity,June1992,Air&WasteManagement  Association,Pittsburgh,PA,1992. (#(# 6.0  Jackson,M.D.,Knoll,_J.E._,_Midgett_,_M.R._,_Bursey_,_J.T._,_McGaughey_,_J.F._,Merrill, v _R.G._Ԁ"Evaluationof_VOST_ԀandSemi_VOST_ԀMethodsfor_Halogenated_ԀCompoundsintheCleanAirActAmendmentsTitleIII,ValidationStudyatFossilFuelPlant,"ProceedingsoftheNationalA&_WMA_ԀMeeting,Denver,CO,June1993,Air&Waste F ManagementAssociation,Pittsburgh,PA,1993. (#(# 7.0  _Bursey_,_J.T._,Merrill,_R.G._,_McAllister_,R.A.,_McGaughey_,_J.F._,Laboratory p" " Validationof_VOST_Ԁand_SemiVOST_Ԁfor_Halogenated_ԀHydrocarbonsfromtheCleanAirActAmendmentsList,Volumes1&2,EPA600/R93/123a,EPA600/R93/123b, R$!$ PB93227163,PB93227171,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,July1993. (#(# 8.0  _McGaughey_,_J.F._,_Bursey_,_J.T._,Merrill,_R.G._,FieldTestofaGenericMethodfor (%( _Halogenated_ԀHydrocarbons,EPA600/R93/101,PB93212181AS,U.S. )&) EnvironmentalProtectionAgency,ResearchTrianglePark,NC,September1993. (#(# 9.0  _McGaughey_,_J.F._,_Bursey_,_J.T._,Merrill,_R.G._,Jackson,M.D.,"FieldTestofa +), GenericMethodforTheSamplingandAnalysisof_Halogenated_ԀHydrocarbonsListedinTitleIIIofTheCleanAirActAmendmentsof1990,"Proceedingsofthe13th -`+. AnnualInternationalIncinerationConference,Houston,TX,May1994,Universityof .R,/ California,Irvine,CA,1994./D-0(#(# Ї_10.0  Jackson,M.D.,_Bursey_,_J.T._,_McGaughey_,_J.F._,Merrill,_R.G._,"AnEvaluationofthe X _SemiVOST_ԀMethodfor_Halogenated_ԀCompoundsataChemicalManufacturingFacility,"ProceedingsoftheEPA/A&_WMA_ԀInternationalSymposiumonMeasurement 8 ofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,May1995,VIP50, * Air&WasteManagementAssociation,Pittsburgh,PA,1995,pp227232. (#(# #X2HXXXo#XXXX2H11.0  Jackson,M.D.,_Bursey_,_J.T._,_McGaughey_,_J.F._,Merrill,_R.G._,"Applicationof_VOST_  and_SemiVOST_Ԁto_Nonhalogenated_Ԁ_CAAA_ԀCompounds,"Proceedingsofthe  EPA/A&_WMA_ԀInternationalSymposiumonMeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,May1995,VIP50,Air&Waste  v  ManagementAssociation,Pittsburgh,PA,1995,pp233238. (#(# 12.0  Jackson,M.D.,Johnson,_L.D._,_McGaughey_,_J.F._,Wagoner,_D.E._,_Bursey_,_J.T._,  H  Merrill,_R.G._,"ImprovementsinPreparationofSamplesGeneratedbySW846Method0010,"ProceedingsoftheEPA/A&_WMA_ԀInternationalSymposiumon (  MeasurementofToxicandRelatedAirPollutants,Durham,NC,May1994,VIP39, r Air&WasteManagementAssociation,Pittsburgh,PA,1994,pp331338. (#(# #X2HXXX#XXXX2H13.0  Jackson,M.D.,_Bursey_,_J.T._,_McGaughey_,_J.F._ԀandMerrill,R.G.,"AnEvaluationof D the_SemiVOST_ԀMethodfornon_Halogenated_ԀCompoundsataAgriculturalChemicalManufacturingFacility",Proceedingsofthe#X2HXXXֆ#XXXX2HԀEPA/A&_WMA_ԀInternationalSymposium: $ MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,April1997#X2HXXXɈ#XXXX2H,VIP74,Air&WasteManagementAssociation,Pittsburgh,PA,1997,pp#X2HXXX#XXXX2HԀ134  141.#X2HXXXE#XXXX2H(#(# 14.0  _Bursey_,_J.T._,_McGaughey_,_J.F._ԀandMerrill,R.G.,FieldEvaluationatanAgricultural  ManufacturingFacilityof_VOST_Ԁand_SemiVOST_ԀMethodsforSelected_CAAA_ԀOrganicCompounds,EPA/600R97/037,PB97174585,U.S.EnvironmentalProtection b Agency,ResearchTrianglePark,NC,March1997. (#(# 15.0  Jackson,M.D.,_McGaughey_,_J.F._,Merrill,R.G.,and_Bursey_,_J.T._,"Method 4 EvaluationStudy:TheApplicationofSemi_VOST_Ԁtothe_Nonhalogenated_Ԁ_Semivolatile_OrganicCompoundsfromtheCleanAirActAmendments",Proceedingsofthe l   EPA/A&_WMA_ԀInternationalSymposium:MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,May1996,VIP64,Air&Waste N"" ManagementAssociation,Pittsburgh,PA,1996pp620625#X2HXXX#XXXX2H.@# #(#(# 16.0  _Bursey_,_J.T._,_McGaughey_,_J.F._ԀandMerrill,R.G.,FieldEvaluation(First)of_VOST_  %"% andSemi_VOST_ԀMethodsforSelected_CAAA_ԀOrganicCompoundsataCoalFiredPlant,EPA/600R97/076,PB97196117,U.S.EnvironmentalProtectionAgency, '$' ResearchTrianglePark,NC,February1997. (#(# #X2HXXXP#XXXX2H17.0  _Bursey_,_J.T._,_McGaughey_,_J.F._ԀandMerrill,R.G.,FieldTestofaGenericMethodfor )|'* _Halogenated_ԀHydrocarbons:_SemiVOST_ԀatanAgriculturalChemicalManufacturingFacility,EPA/600R97/033,PB97162499,U.S.EnvironmentalProtectionAgency, +^), ResearchTrianglePark,NC,February1997.#X2HXXX#XXXX2H,P*-(#(# 18.#X2HXXXT#XY,XXX2H0  #X2HX,XXY#XXXX2H_McGaughey_,_J.F._,#X2HXXX#XXXX2HFoster,S.C.,Merrill,_R.G._,LaboratoryDevelopmentandField .0,/ EvaluationofAGenericMethodforSamplingandAnalysisof_Isocyanates_,EPA z/"-0 600/R95/144,PB95273801,U.S.EnvironmentalProtection_Agency,Research_TrianglePark,NC,August1995. (#(# 19.0  Jackson,M.D.;Johnson,_L.D._;_McGaughey_,_J.F._;Wagoner,_D.E._;_Bursey_,_J.T._; ( Merrill,_R.G._,"ImprovementsinPreparationofSamplesGeneratedbySW846Method0010,"ProceedingsoftheEPA/A&_WMA_ԀInternationalSymposiumon  MeasurementofToxicandRelatedAirPollutants,Durham,NC,May1994,VIP39,  Air&WasteManagementAssociation,Pittsburgh,PA,1994,pp331338.#X2HXXX#XXXX2H#ǯ XX_#XX ǯ(#(# 20.0  #X2HXXX8#XXXX2H#ǯ XXz#XX ǯJohnson,_L.D._,_Fuerst_,_R.G._,Foster,_A.L._Ԁand_Bursey_,_J.T._,#X2HXXX## XX2H-#ǯ   XX ǯ"ReplacementofCharcoal  t  SorbentInTheSamplingofVolatile_Organics_ԀfromStationarySources,"Intern.J.  d  Environ.Anal.Chem.,Vol62,pp.231244,(1996).#X2HXXX#XXXX2H#ǯ XX#XX ǯ V (#(# 21.0  Eaton,W.C.;Jaffe,_L.B._;_Rickman_,E.E.;_Jayanty_,_R.K.M._,FieldTestsofChloroform 8  Collection/AnalysisMethods,EPA600/R94/082,PB94176948,U.S.Environmental *  ProtectionAgency,ResearchTrianglePark,NC,July1994. (#(# 22.0  Eaton,W.C.;Jaffe,_L.B._;_Rickman_,E.E.;_Jayanty_,_R.K.M._;Wilshire,_F.W._;Knoll, T _J.E._,"ValidationofaTestMethodforCollectionandAnalysisofChloroformEmissionsfromStationarySources,"J.Air&WasteManage.Assoc.,46,pp6671, 4 1996. (#(# #X2HXXX؞#XXXX2H#ǯ XX#XX ǯ23.0  _Steger_,_J.L._,Knoll,_J.E._,"DynamicSpikingStudiesUsingthe_DNPH_ԀSampling  Train,#X2HXXX5#XXXX2H"#X2HXXX#XY,XXX2HԀ#X2HX,XXY#XXXX2HpresentedatEPA/A&_WMA_ԀInternationalSymposium:MeasurementofToxic  andRelatedAirPollutants,ResearchTrianglePark,NC,May1996.#X2HXXX4#XXXX2H(#(# 24.0  _Steger_,_J.L._,#X2HXXX0#XXXX2H_Bursey_,_J.T._#X2HXXX#XXXX2H,and_Epperson_,D.,_Acetonitrile_ԀFieldTest,#X2HXXX}#XXXX2HԀEPA600/R  97/140,PB98133143,U.S.#X2HXXX1#XXXX2HEnvironmentalProtectionAgency,ResearchTriangle  Park,NC,#X2HXXX#XXXX2HԀOctober1997.p(#(# #X2HXXX?#XXXX2H25.0  #X2HXXX#XXXX2H_R.G._Ԁ_Fuerst_,_T.J._ԀLogan,_M.R._Ԁ_Midgett_ԀandJ._Prohaska_,"ValidationStudiesofthe @"  P ProtocolfortheVolatileOrganicSamplingTrain,"J.Air_Pollut_.ControlAssoc., @V!  @ 37:(4)388(1987). (#(# 26.#X2HXXX#XXXX2H0  Johnson,_L.D._,_Fuerst_,_R.G._,#X2HXXX:#XXXX2HԀ_Steger_,_J.L._,and_Bursey_,_J.T._,#X2HXXX#XXXX2HԀ"Evaluationofa j!! SamplingMethodfor_Acetonitrile_ԀEmissionsfromStationarySources,"#X2HXXX#XXXX2HԀProceedingsof Z" " the#X2HXXX#XXXX2HԀEPA/A&_WMA_ԀInternationalSymposium:MeasurementofToxicandRelatedAir L# # Pollutants,ResearchTrianglePark,NC,April1997#X2HXXX#XXXX2H,VIP74,Air&Waste <$!$ ManagementAssociation,Pittsburgh,PA,1997,pp#X2HXXX#XXXX2HԀ149158#X2HXXX#XXXX2H.#X2HXXX#XXXX2H.%"%(#(# 27.#X2HXXX;#XXXX2H0  _McGaughey_,_J.F._,_Bursey_,_J.T._,Merrill,_R.G._,Jackson,M.D.,Johnson,_L.D._, '$' _Fuerst_,_R.G._,"ComparisonofaModified_VOST_ԀSamplingMethodwithSW846Method0030ataChemicalManufacturingFacility,"Proceedingsofthe13thAnnual (&) InternationalIncinerationConference,Houston,TX,May1994,Universityof )'* California,Irvine,CA,1994. (#(# 28.0  Jackson,M.D.,Johnson,_L.D._,_Fuerst_,_R.G._,_McGaughey_,_J.F._,_Bursey_,_J.T._, ,Z*- Merrill,_R.G._,"FieldEvaluationofaModified_VOST_ԀSamplingMethod,"Proceedings -J+. oftheEPA/A&_WMA_ԀInternationalSymposiumonMeasurementofToxicandRelatedAirPollutants,Durham,NC,May1994,VIP39,Air&WasteManagement /,-0 Association,Pittsburgh,PA,1994,pp354360. (#(# 29.0  _McGaughey_,_J.F._,_Bursey_,_J.T._,Merrill,_R.G._,FieldTestofaGenericMethodfor 8 _Halogenated_ԀHydrocarbons:A_VOST_ԀTestataChemicalManufacturingFacilityUsingaModified_VOST_ԀSamplingMethod,EPA600/R94/130,PB95142055,U.S.  EnvironmentalProtectionAgency,ResearchTrianglePark,NC,July1994. (#(# #X2HXXX#XXXX2H30.0  #X2HXXXA#XXXX2H_McGaughey_,_J.F._,_Bursey_,_J.T._,Merrill,_R.G._,FieldTestofaGenericMethodfor  _Halogenated_ԀHydrocarbons:_SemiVOST_ԀTestataChemicalManufacturingFacility,   EPA600/R96/133,PB97115349,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,November1996.#X2HXXX#XXXX2H h (#(# 31.#X2HXXX#XXXX2H0  _McGaughey_,_J.F._,_Bursey_,_J.T._,Merrill,_R.G._,FieldTestofaGenericMethodfor  H  _Halogenated_ԀHydrocarbons:A_VOST_ԀTestataChemicalManufacturingFacility,EPA :  600/R94/113,PB95129144,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,June1994.#X2HXXXU#XXXX2Ht(#(# 32.#X2HXXX#XXXX2H0  Rice,J.,_McGaughey_,_J.F._,_Bursey_,_J.T._,Merrill,_R.G._,_Harvan_,D.,Handbookof T GC/MSDataandInformationforSelectedCleanAirActAmendmentsCompounds, F EPA600/R94/021,PB94155884,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,January1994. (#(# 33.0  Wagoner,_D.E._,Merrill,_R.G._,_McGaughey_,_J.F._,_Bursey_,_J.T._,Evaluationof_CAAA_  Compounds:ApproachesforStationarySourceMethodDevelopment,EPA600/R  96/091,PB96193206,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,1996.#X2HXXX#XXXX2H(#(# 34.#X2HXXX#XXXX2H0  Jackson,M.D.,_McGaughey_,_J.F._,Merrill,R.G.,and_Bursey_,_J.T._,"Method d EvaluationStudy:TheApplicationof_VOST_Ԁtothe_Nonhalogenated_ԀVolatileOrganicCompoundsfromtheCleanAirActAmendments",ProceedingsoftheEPA/A&_WMA_ D InternationalSymposium:MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,May1996,VIP64,Air&WasteManagementAssociation, ~& Pittsburgh,PA,1996pp613619#X2HXXX#XXXX2H.#X2HXXX#XXXX2Hp  (#(# 35.#X2HXXXI#XXXX2H0  Jackson,M.D.,_Bursey_,_J.T._,_McGaughey_,_J.F._ԀandMerrill,R.G.,"AnEvaluationof P"" the_VOST_ԀMethodfornon_Halogenated_ԀCompoundsataAgriculturalChemicalManufacturingFacility",Proceedingsofthe#X2HXXX#XXXX2HԀEPA/A&_WMA_ԀInternationalSymposium: 0$!$ MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,April1997#X2HXXX#XXXX2H,VIP74,Air&WasteManagementAssociation,Pittsburgh,PA,1997,pp#X2HXXX#XXXX2HԀ129 &#& 133.#X2HXXX#XXXX2H'$'(#(# 36.0  _Prohaska_,J.,#X2HXXXu#XXXX2HԀ_T.J._ԀLogan,#X2HXXX#XXXX2HԀ#X2HXXX#XXXX2H_R.G._Ԁ_Fuerst_,_M.R._Ԁ_Midgett_#X2HXXX#XXXX2H,ValidationoftheVolatile (&) OrganicSamplingTrain(_VOST_)Protocol,Volume1,LaboratoryValidationPhase, )~'* PB86145547,#X2HXXX#XXXX2HԀU.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC, *p(+ January1986. (#(# 37.0  #X2HXXX#XXXX2H_Prohaska_,J.,#X2HXXXt#XXXX2HԀ_T.J._ԀLogan,#X2HXXX#XXXX2HԀ#X2HXXXQ#XXXX2H_R.G._Ԁ_Fuerst_,_M.R._Ԁ_Midgett_#X2HXXX#XXXX2H,ValidationoftheVolatile -@+. OrganicSamplingTrain(_VOST_)Protocol,Volume2,FieldValidationPhase,PB86 .2,/ 145554,#X2HXXXo#XXXX2HԀU.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,January |/$-0 1986. (#(# 38.0  Wilshire,_F.W._,Knoll,_J.E._,Foster,S.C.and_McGaughey_,_J.F._,"Developmentand 8 ValidationofaSourceTestMethodfor2,4Toluene_Diisocyanate_,"inProceedingsof ( the1993EPA/A&_WMA_ԀInternationalSymposiumonMeasurementofToxicandRelatedAirPollutants,VIP34,Air&WasteManagementAssociation,Pittsburgh,PA,1993,   pp399407. (#(# 39.0  Wilshire,_F.W._,Knoll,_J.E._,Foster,S.C.and_McGaughey_,_J.F._,"FieldTestand   ValidationofaSourceTestMethodforMethylene_Diphenyl_Ԁ_Diisocyanate_,"Proceedingsofthe87thAnnualNationalA&_WMA_ԀMeeting,Cincinnati,OH,June  d  1994,Air&WasteManagementAssociation,Pittsburgh,PA,1994. T (#(# #X2HXXXs#XXXX2H40.0  _Steger_,_J.L._ԀandWorkman,_G.S._,FieldValidationofthe_DNPH_ԀMethodforAldehydes 6  and_Ketones_,EPA/600/R96/050,PB96168398,U.S.EnvironmentalProtection (  Agency,ResearchTrianglePark,NC,April1996.#X2HXXX #XXXX2Hr(#(# 41.0  Jackson,M.D.,Johnson,_L.D._,"SamplingandAnalysisInformationAidsfor R StationarySourcePersonnel,"ProceedingsoftheEPA/A&_WMA_ԀInternational B SymposiumonMeasurementofToxicandRelatedAirPollutants,Durham,NC,May1994,VIP39,Air&WasteManagementAssociation,Pittsburgh,PA,1994,pp315 $ 318. (#(# 42.0  Jackson,M.D.,Johnson,_L.D._,StationarySourceSamplingandAnalysisDirectory,  Version2.1,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,  1995,EPA/600/R97/028,PB98120033(Report/Manual)andPB500598(Databaseonfloppydisk)February1997. (#(# #X2HXXX#XXXX2H43.0  _Steger_,_J.L._,Merrill,_R.G._,_Parrish_,C.R.,and#X2HXXX#XXXX2HԀJohnson,_L.D._,#X2HXXX#XXXX2HԀDevelopmentand R EvaluationofaSourceSamplingandAnalysisMethodforHydrogenCyanide,#X2HXXX##XXXX2H D EPA/600/R98/xxx,PB98_xxxxxx_,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,#X2HXXX#XXXX2HԀFebruary1998.|$(#(# 44.0  #X2HXXX#XXXX2H_Steger_,_J.L._,Merrill,_R.G._,#X2HXXX0#XXXX2HԀ_Fuerst_,_R.G._#X2HXXX#XXXX2H,Johnson,_L.D._,Jackson,M.D.#X2HXXX}#XXXX2HԀand_Parrish_, \!! C.R., DevelopmentandEvaluationofaSourceSamplingandAnalysisMethodforHydrogenCyanide,#X2HXXX#XXXX2HԀProceedingsofthe#X2HXXX#XXXX2HG %  G EPA/A&_WMA_ԀInternationalSymposium: <# # MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,April .$!$ 1997#X2HXXX@#XXXX2H,VIP74,Air&WasteManagementAssociation,Pittsburgh,PA,1997,pp#X2HXXX_#XXXX2H114  %"% 122.#X2HXXX#XXXX2H&#&(#(# #X2HXXXG#XXXX2H#X2HXXX#XXXX2H45.0  Fan,Z.,Peterson,_M.R._,_Jayanty_,_R.K.M._, DevelopmentofaTestMethodfor '%( CarbonylCompoundsfromStationarySourceEmissions,#X2HXXX#XXXX2HԀProceedingsofthe#X2HXXX7#XXXX2H (&) EPA/A&_WMA_ԀInternationalSymposium:MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,April1997#X2HXXX#XXXX2H,VIP74,Air&Waste *j(+ ManagementAssociation,Pittsburgh,PA,1997,pp#X2HXXX#XXXX2HԀ#X2HXXX#XXXX2H9297.#X2HXXXb#XXXX2H+\),(#(# 46.#X2HXXX#XXXX2H0  _Bursey_,_J.T._,_McGaughey_,_J.F._,Merrill,R.G.,Knoll,_J.E._,Ward,_T.E._,andJackson, -<+. M.D.,#X2HXXX#XXXX2HԀ FieldTestingtoCompleteValidationofaManualMethodforHighLevelsof .,,/ PhenolicCompounds,#X2HXXX#XXXX2HProceedingsofthe#X2HXXXL#XXXX2HԀEPA/A&_WMA_ԀInternationalSymposium: t/-0 MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark,NC,April1997#X2HXXX#XXXX2H,VIP74,Air&WasteManagementAssociation,Pittsburgh,PA,1997,pp#X2HXXX#XXXX2HԀ#X2HXXX#XXXX2H142 H 149.#X2HXXX_#XXXX2H:(#(# 47.0  Pau,_J.C._,_Romeu_,A.A.,_Whitacre_,M.,andCoates,_J.T._,ValidationofEmission  SamplingandAnalysisTestMethodfor_PCDDs_Ԁand_PCDFs_ԀII,#X2HXXX# XXXX2HԀEPA600/R390/047,   PB90235847/AS,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,August1990.#X2HXX X#XXXX2H(#(# 48.0  #X2HXXXY#XXXX2HCooke,M.,_DeRoos_,F.,Rising,B.,Jackson,M.D.,Johnson,_L.D._,andMerrill,  v  _R.G._,"DioxinCollectionfromHotStackGasUsingSourceAssessmentSamplingSystemandModifiedMethod5TrainsAnEvaluation,"presentedatNinthAnnualResearchSymposiumonLandDisposal,Incineration,andTreatmentofHazardousWaste,Ft.Mitchell,KY,May1983.#X2HXXX#XXXX2H6 (#(# 49.0  Fan,Z.,Peterson,_M.R._,_Jayanty_,_R.K.M._,Wilshire,_F.W._, Measurementof n CarbonylCompoundsfromStationarySourceEmissionsbya_PFBHA_Ԅ_ECD_ԀMethod,presentedat#X2HXXX#XXXX2Hthe91stAnnualNationalMeetingoftheAir&WasteManagement N Association,SanDiego,CA,June1998.#X2HXXX#XXXX2H>(#(# 50.0  Peterson,_M.R._,Fan,Z.,Jaffe,_L.B._,_Albritton_,_J.R._,_Grohse_,P.M.,_Jayanty_,  _R.K.M._,Research,Development,andEvaluationofStationarySourceEmissionTest  MethodsforAir_Toxics,Letter_ԀReport#X2HXXX#XXXX2H,ResearchTriangleInstituteto#X2HXXX#XXXX2HԀU.S.  EnvironmentalProtectionAgency,ResearchTrianglePark,NC,#X2HXXXI#XXXX2HԀMarch1998.(#(# 51.0  Peterson,_M.R._,Pate,B.A.,Wright,R.S.,_Jayanty_,_R.K.M._,Wilshire,_F.W._, ATest z MethodfortheMeasurementof_Arylamines_ԀinStationarySourceEmissions,#X2HXXX#XXXX2HԀ j ProceedingsoftheEPA/A&_WMA_ԀInternationalSymposium:MeasurementofToxicand Z RelatedAirPollutants,ResearchTrianglePark,NC,May1996,VIP64,Air&Waste J ManagementAssociation,Pittsburgh,PA,1996pp577582#X2HXXX#XXXX2H.<(#(# 52.0  #X2HXXX1#XXXX2H_Steger_,_J.L._,_Coppedge_,_E.A._ԀandJohnson,_L.D._,"ResearchandDevelopmentofA t SourceMethodforPhosgene,"#X2HXXX#XXXX2HProceedingsoftheEPA/A&_WMA_ԀInternational d   Symposium:MeasurementofToxicandRelatedAirPollutants,ResearchTrianglePark, V!! NC,May1996,VIP64,Air&WasteManagementAssociation,Pittsburgh,PA,1996,pp#X2HXXX#XXXX2H285289.#X2HXXXg#XXXX2H8# #(#(# 53.0  #X2HXXX#XXXX2H_Steger_,_J.L._,#X2HXXX"#XXXX2H_Bursey_,_J.T._#X2HXXX#XXXX2H,Merrill,_R.G._,#X2HXXX@#XXXX2HԀand_Epperson_,D.#X2HXXX#XXXX2H,Researchand %"% DevelopmentofaFieldReadyProtocolforSamplingofPhosgenefromStationarySourceEmissions:_Diethylamine_ԀReagentStudies,#X2HXXX%#XXXX2HEPA/600/R98/xxx,PB98_xxxxxx_,#X2HXXX/#XXXX2H &$' U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,#X2HXXX#XXXX2HԀMay1998.'%((#(# 54.0  Peterson,_M.R._,Jaffe,_L.B._,_Jayanty_,_R.K.M._,Wilshire,_F.W._, ATestMethodfor )t'* theMeasurementofAcrylicsinStationarySourceEmissions,presentedat#X2HXXXG#XXXX2Hthe90th *d(+ AnnualNationalMeetingoftheAir&WasteManagementAssociation,Toronto,Ontario,Canada,June1997.#X2HXXX #XXXX2H,D*-(#(# 55.0  _Giglio_,_J.J._,_ORourke_,_J.J._,_Grohse_,P.M.,Wilshire,_F.W._,Ryan,J.,_Linak_,W.,The |.$,/ DevelopmentofaMethodforthe_Speciation_ԀofSourceMercuryEmissions,Presented l/-0 attheInternationalConferenceonIncinerationandThermalTreatmentTechnologies,SaltLakeCity,UT,May,1998. (#(# #X2HXXX #XXXX2H56.0  James,R.H.,Adams,R.E.,_Finkel_,_J.M._,Miller,H.C.,andJohnson,_L.D._, ( "EvaluationofAnalyticalMethodsfortheDeterminationof_POHC_ԀinCombustionProducts,"J.AirPollutionControlAssociation,35,959(1985).#X2HXXX #XXXX2H(#(# 57.0  #X2HXXXp#XXXX2HJames,R.H.,Adams,R.E.,_Finkel_,_J.M._,Miller,H.C.,_POHC_ԀAnalysisMethodsfor  HazardousWasteIncineration,Vol.1,Parts1&2,Vol.2,#X2HXXX#XXXX2HEPA/600/887037a,b&   c,PB87227286/AS,PB87227294/AS,PB87227302/AS#X2HXXX'#XXXX2H,U.S.Environmental  v  ProtectionAgency,ResearchTrianglePark,NC,December1987.#X2HXXX#XXXX2H f (#(# 58.0  #X2HXXXn#XXXX2HJames,R.H.,Adams,R.E.,Farr,_L.B._,Miller,H.C.#X2HXXX#XXXX2H,_PIC_ԀAnalysisMethods,EPA  F  600/987011,PB87208955/AS,#X2HXXXs#XXXX2HԀU.S.EnvironmentalProtectionAgency,Research 8  TrianglePark,NC,June1987.#X2HXXX)## XX2Hw#ǯ   XX ǯ( (#(# 59.0  Pate,B.A.,Peterson,_M.R._,_Rickman_,E.E.,_Jayanty_,_R.K.M._,TestMethodforthe ` MeasurementofMethanolEmissionsfromStationarySources,EPA600/R94/080, R PB94170297,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC,July1994. (#(# 60.0  Pate,B.A.,Peterson,_M.R._,_Jayanty_,_R.K.M._,Wilshire,_F.W._,Knoll,_J.E._,  "DevelopmentofaTestMethodfortheMeasurementofGaseousMethanolEmissionsfromStationarySources,"inProceedingsofthe1993EPA/A&_WMA_ԀInternational  SymposiumonMeasurementofToxicandRelatedAirPollutants,VIP34,Air&Waste  ManagementAssociation,Pittsburgh,PA,1993,pp393398. (#(# 61.0  Peterson,_M.R._,Pate,B.A.,_Rickman_,E.E.,_Jayanty_,_R.K.M._,Wilshire,_F.W._, ` "ValidationofaTestMethodfortheMeasurementofMethanolEmissionsfromStationarySources,"J.Air&WasteManage.Assoc.,45,pp.311,1995.@(#(# 62.0  Eaton,W.C.,Jaffe,_L.B._,_Rickman_,E.E.,_Jayanty_,_R.K.M._,FieldTestsofChloroform z" Collection/AnalysisMethods,EPA600/R94/082,PB94176948,U.S.Environmental l   ProtectionAgency,ResearchTrianglePark,NC,July1994. (#(# 63.0  Eaton,W.C.,Jaffe,_L.B._,_Rickman_,E.E.,_Jayanty_,_R.K.M._,Wilshire,_F.W._,Knoll, ># # _J.E._,"ValidationofaTestMethodforCollectionandAnalysisofChloroformEmissionsfromStationarySources,"J.Air&WasteManage.Assoc.,46,pp6671, %"% 1996. (#(# 64.0  _Bursey_,_J.T._,_McGaughey_,_J.F._,_Steger_,_J.L._,Merrill,R.G.,XXXXFieldTestingto '%( CompleteValidationofaManualMethodforHighLevelsofPhenolicCompounds,#XXXX?# (&) DraftFinalReport,U.S.EnvironmentalProtectionAgency,ResearchTrianglePark,NC. (#(# 65.0  U.S.EPATentativeMethod317,Phenol,ManualMethod,U.S.Environmental ,L*- ProtectionAgency,ResearchTrianglePark,NC. (#(#   ..,/ !XXXX XXX!X9ZXXSOURCESOFMETHODSANDINFORMATION  X #XX9Z!#  Forthepersontryingtoobtaincurrentinformationortoenterintothefieldofsourcemeasurements,thereareseveralparticularlyhelpfulinformationsourcesavailable.TheU.S.EPAmethodsareintwogroups,thoseusedbyEPA'sOfficeofAirQualityPlanningandStandards(_OAQPS_),andthoseusedbyEPA'sOfficeofSolidWaste(_OSW_).#!XXXXj!# . XXX!X  TheEmissionMeasurementTechnicalInformationCenter(_EMTIC_)atResearch  TrianglePark,NCissupportedbyEPA'sOfficeofAirQualityPlanningandStandards.Perhapsthemostefficientofseveralavailableformsofassistanceisthe_EMTIC_ԀBulletinBoardSystem(BBS).Testmethodsareincluded,alongwithannouncements,utilityprograms,miscellaneousdocuments,andotherinformation.The_EMTIC_/BBSmaybereachedthrough_TTN_Ԁ2000ontheInternetathttp://www.epa.gov/ttn.An_EMTIC_Ԁrepresentativecanbereachedbytelephoneat9195410200._EMTIC_ԀsponsorsworkshopsandtrainingcoursesjointlywithEPA'sAirPollutionTrainingInstitute.Trainingvideotapes,anewsletter,andothermailingsarealsoavailablefrom_EMTIC_.  Anexcellentsourceforinformationconcerning_OSW_sSW846MethodsistheMethodsInformationCommunicationExchange(MICE).MICEcanbereachedontheInternetatmice@lan828.ehsg.saic.com.AtelephonecalltotheMICEline,at7038214690,willputtheinformationseekerintouchwithanautomatedinformationserviceorwithaliverepresentative.AlthoughthefunctionofMICEistoprovideinformation,theywillusuallysendcopiesofuptothreemethods.TheywillnotprovidecopiesoftheentireSW846MethodsManual.TheSW846MethodsManual,maybeobtainedonCDROMorhardcopyfromNationalTechnicalInformationService(_NTIS_).The_NTIS_ԀordernumberfortheCDROMwhichincludesthethirdeditionandupdates13isPB97501928INQ._NTIS_Ԁhasawebsiteathttp://www.ntis.gov.andmayalsobereachedbytelephoneat7034874650.SW846mayalsobeobtainedfromtheGovernmentPrintingOffice(GPO).OrderinginformationforGPOis0  TestMethodsforEvaluatingSolidWaste,Physical/ChemicalMethods,SW846 v Manual,3rded.DocumentNo.955001000001.AvailablefromSuperintendentof f Documents,U.S.GovernmentPrintingOffice,Washington,DC,November1986. (#(# ThefulldocumentisavailablefromU.S.GovernmentPrintingOffice,telephone2027833238.GPOalsohasa_website_Ԁathttp://www.access.gpo.gov.#!XXXX## 8   FormoreinformationorcopiesoftheCaliforniaEnvironmentalProtectionAgency,AirResourcesBoardMethods(a.k.a._CARB_ԀMethods),contacthttp://www.arb.ca.gov/testmeth/testmeth.htmortelephoneEngineeringandLaboratoryBranchat9162631630.H   EPAreportsmaybeoH I H btainedH I J rderedJ H fromNTISattheH K websiteortelephonenumbergivenabove.K L % $ L