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T h'   XԮXXX  T!   5  o[X` hp x (#%'0*,.8135@8:<H?AXoXԮXXXl7ԮXXdd7ћ  @ PERFORMANCESPECIFICATION7SPECIFICATIONS < @ANDTESTPROCEDURESFORHYDROGENSULFIDECONTINUOUSEMISSION@ "MONITORINGSYSTEMSINSTATIONARYSOURCES      1.0ScopeandApplication.  p Л ` 1.1Analytes.̛*wddd Xdd Xdd X(#(#w,| dT ,| dT +  )5  F  P()Analyte ,5 P 5  ,CASNo. @5/!P  d( P 5  P8@HydrogenSulfide 25! 5 277830647-+  d8 P  5 7М ` 1.2Applicability. ` 1.2.1Thisspecificationistobeusedforevaluatingtheacceptabilityofhydrogensulfide(H2S)continuous B emissionmonitoringsystems(CEMS)atthetimeoforsoonafterinstallationandwheneverspecifiedinanapplicablesubpartoftheregulations. ` 1.2.2ThisspecificationisnotdesignedtoevaluatetheinstalledCEMSperformanceoveranextendedperiodoftimenordoesitidentifyspecificcalibrationtechniquesandotherauxiliaryprocedurestoassessCEMSperformance.Thesourceowneroroperator,however,isresponsibletocalibrate,maintain,andoperatetheCEMS.ToevaluateCEMSperformance,theAdministratormayrequire,underSection114oftheAct,thesourceowneroroperatortoconductCEMSperformanceevaluationsatothertimesbesidestheinitialtest.SeeSection60.13(c). ,6&, l2.0Summary.󛀀 Z  ` Calibrationdrift(CD)andrelativeaccuracy(RA)testsareconductedtodeterminethattheCEMSconformstotheϜspecification.3.0Definitions. j   ` SameasSection3.0ofPS2.4.0Interferences.[Reserved]   5.0Safety.󀀜 P   ` Theproceduresrequiredunderthisperformancespecificationmayinvolvehazardousmaterials,operations,andequipment.ThisperformancespecificationmaynotϜaddressallofthesafetyproblemsassociatedwiththeseprocedures.Itistheresponsibilityoftheusertoestablishappropriatesafetyproblemsassociatedwiththeseprocedures.ItistheresponsibilityoftheusertoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicationregulatorylimitationspriortoϜperformingtheseprocedures.TheCEMSusersmanualandmaterialsrecommendedbythereferencemethodshouldbeconsultedforspecificprecautionstobetaken.6.0EquipmentandSupplies. )D#(  ` 6.1InstrumentZeroandSpan.ThisspecificationisthesameasSection6.1ofPS2. -&,  ` 6.2CalibrationDrift.TheCEMScalibrationmustnotdriftordeviatefromthereferencevalueofthecalibrationgasorreferencesourcebymorethan5percentoftheestablishedspanvaluefor6outof7testdays(e.g.,theestablishedspanvalueis300ppmforSubpartJfuelgascombustiondevices). ` 6.3RelativeAccuracy.TheRAoftheCEMSmustbenogreaterthan20percentwhentheaveragereferencemethod(RM)valueisusedtocalculateRAor10percentwhentheapplicableemissionstandardisusedtocalculateRA.7.0ReagentsandStandards.󀀜   ` SameasSection7.0ofPS2.8.0SampleCollection,Preservation,Storage,and 0 МTransport. B Л ` 8.1InstallationandMeasurementLocationϜSpecification.SameasSection8.1ofPS2. ` 8.2PretestPreparation.SameasSection8.2ofPS2. ` 8.3CalibrationDriftTestProcedure.SameasSection8.3ofPS2. ` 8.4RelativeAccuracyTestProcedure. ` 8.4.1SamplingStrategyforRMTests,Correlationof RMandCEMSData,andNumberofRMTests.Thesearethe V+$* sameasthatinPS2,Sections8.4.3,8.4.5,and8.4.4,respectively.  ` 8.4.2ReferenceMethods.Unlessotherwisespecifiedinanapplicablesubpartoftheregulation,Method11istheRMforthisPS. ` 8.5Reporting.SameasSection8.5ofPS2.9.0QualityControl.[Reserved]   10.0CalibrationandStandardizations.[Reserved] \  11.0AnalyticalProcedures. z   ` SampleCollectionandanalysisareconcurrentforthisPS(seeSection8.0).RefertotheRMforspecificanalyticalprocedures.12.0DataAnalysisandCalculations.󀀜 0  ` SameasSection12.0ofPS2.13.0MethodPerformance.[Reserved]  14.0PollutionPrevention.[Reserved]  | М15.0WasteManagement.[Reserved] "@  16.0References. ^$"  ` 1.U.S.EnvironmentalProtectionAgency.StandardsofPerformanceforNewStationarySources;AppendixB;PerformanceSpecifications2and3forSO2,NOx,CO2,andO2 )D#(  ContinuousEmissionMonitoringSystems;FinalRule.48CFR b+%* 23608.Washington,D.C.U.S.GovernmentPrintingOffice.May25,1983.  ` 2.U.S.GovernmentPrintingOffice.GaseousContinuousEmissionMonitoringSystemsPerformanceSpecificationGuidelinesforSO2,NOx,CO2,O2,andTRS. j  U.S.EnvironmentalProtectionAgency.Washington,D.C.EPA450/382026.October1982.26p. ` 3.Maines,G.D.,W.C.Kelly(ScottEnvironmentalTechnology,Inc.),andJ.B.Homolya.EvaluationofMonitorsforMeasuringH2SinRefineryGas.PreparedfortheU.S. > EnvironmentalProtectionAgency.ResearchTrianglePark,N.C.ContractNo.68022707.1978.60p. ` 4.Ferguson,B.B.,R.E.Lester(HarmonEngineeringandTesting),andW.J.Mitchell.FieldEvaluationofCarbonMonoxideandHydrogenSulfideContinuousEmissionMonitorsatanOilRefinery.PreparedfortheU.S.EnvironmentalProtectionAgency.ResearchTrianglePark,N.C.PublicationNo.EPA600/482054.August1982.100p.17.0Tables,Diagrams,Flowcharts,andValidationData.󀀜 "&$  ` SameasSection18.0ofPS2.