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CFR Promulgated Test Methods (TM)

295 kb
CFR promulgated test methods have been published in the Federal Register as final rules. These are the official, legal Federal Register Versions.

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File Description

Posting Date

File Types

Chronology of Methods
10/2000 Federal Register Copy of the Amendments for Testing and Monitoring Provisions Exit EPA disclaimer http://www.access.gpo.gov/su_docs/fedreg/a001017c.html
Response to Comments on "Amendments for Testing and Monitoring Provisions" Published in the FR 8/27/97. 02/2001
Preamble to the Amendments for Testing and Monitoring Provisions. 4/2000
Method 1 - Traverse Points - Click here for Method FAQs and documents 9/2014
Method 1A - Small Ducts - Click here for Method FAQs and documents 8/2013
Method 2 - Velocity - S-type Pitot - Click here for Method FAQs and documents 9/2014
Method 2A - Volume Meters - Click here for Method FAQs and documents 9/2014
Methos 2B - Exhaust Volume Flow Rate - Click here for Method FAQs and documents 9/2014
Method 2C - Standard Pitot - Click here for Method FAQs and documents 12/2013
Method 2D - Rate Meters - Click here for Method FAQs and documents 9/2014
Method 2E - Landfill Gas Production Flow Rate - Click here for Method FAQs and documents 1/2014
Method 2F - Flow Rate Measurement with 3-D Probe - Click here for Method FAQs and documents 1/2014
Method 2G - Flow Rate Measurement with 2-D Probe - Click here for Method FAQs and documents 1/2014
Method 2H - Flow Rate Measurement with Velocity Decay Near Stack Walls - Click here for Method FAQs and documents 1/2014
Memo - New Test Procedures of Stack Gas Flow Rate in Place of Method 2 4/4/2000
Method 3 - Molecular Weight - Click here for Method FAQs and documents 9/2014
Method 3A - CO2, O2 - Instrumental - Click here for Method FAQs and documents 9/2014
Method 3B - CO2, O2 - Orsat - Click here for Method FAQs and documents 9/2014
Method 3C - CO2, CH4, N2, O2 - TCD - Click here for Method FAQs and documents 9/2014
Method 4 - Moisture Content - Click here for Method FAQs and documents 9/2014
Method 5 - Particulate Matter(PM) - Click here for Method FAQs and documents 9/2014
Method 5A - PM Asphalt Roofing - Click here for Method FAQs and documents 9/2014
Method 5B - PM Nonsulfuric Acid - Click here for Method FAQs and documents 9/2014
Method 5D - PM Baghouses (Particulate Matter) - Click here for Method FAQs and documents 9/2014
Method 5E - PM Fiberglass Plants (Particulate Matter) - Click here for Method FAQs and documents 9/2014
Method 5F - PM Fluid Catalytic Cracking Unit - Click here for Method FAQs and documents 9/2014
Method 5G - PM Wood Heaters from a Dilution Tunnel - Click here for Method FAQs and documents 9/2014
Method 5H - PM Wood Heaters from a Stack - Click here for Method FAQs and documents 9/2014
Method 5I - Determination of Low Level Particulate Matter Emissions - Click here for Method FAQs and documents 9/2014
Method 6 - Sulfur Dioxide (SO2) - Click here for Method FAQs and documents 9/2014
Method 6A - SO2, CO2 - Click here for Method FAQs and documents 9/2014
Method 6B - SO2, CO2 - Long Term Integrated - Click here for Method FAQs and documents 9/2014
Method 6C - SO2 - Instrumental - Click here for Method FAQs and documents 9/2014
Method 7 - Nitrogen Oxide (NOx) - Click here for Method FAQs and documents 9/2014
Method 7A - NOx - Ion Chromatographic Method - Click here for Method FAQs and documents 9/2014
Method 7B - NOx - Ultraviolet Spectrophotometry - Click here for Method FAQs and documents 9/2014
Method 7C - NOx - Colorimetric Method - Click here for Method FAQs and documents 9/2014
Method 7D - NOx - Ion Chromatographic - Click here for Method FAQs and documents 9/2014
Method 7E - NOx - Instrumental - Click here for Method FAQs and documents 9/2014
Method 8 - Sulfuric Acid Mist - Click here for Method FAQs and documents 9/2014
Method 9 - Visual Opacity - Click here for Method FAQs and documents 9/2014
Method 10 - Carbon Monoxide (NDIR) - Click here for Method FAQs and documents 9/2014
Method 10A - CO for Certifying CEMS - Click here for Method FAQs and documents 9/2014
Method 10B - CO from Stationary Sources - Click here for Method FAQs and documents 9/2014
Method 11 - H2S Content of Fuel - Click here for Method FAQs and documents 9/2014
Method 12 - Inorganic Lead - Click here for Method FAQs and documents 9/2014
Method 13A - Total Fluoride (SPADNS Zirconium Lake) - Click here for Method FAQs and documents 9/2014
Method 13B - Total Fluoride (Specific Ion Electrode) - Click here for Method FAQs and documents 9/2014
Method 14 - Fluoride for Primary Aluminum Plants - Click here for Method FAQs and documents 9/2014
Method 14A - Total Fluoride Emissions from Selected Sources at Primary Aluminum Plants 9/2014
Method 15 - Hydrogen Sulfide, Carbonyl Sulfide, and Carbon Disulfide - Click here for Method FAQs and documents 9/2014
Method 15A - Total Reduced Sulfur (TRS Alt.) - Click here for Method FAQs and documents 9/2014
Method 16 - Sulfur (Semicontinuous Determination) - Click here for Method FAQs and documents 9/2014
Method 16A - Total Reduced Sulfur (Impinger) - Click here for Method FAQs and documents 9/2014
Method 16B - Total Reduced Sulfur (GC Analysis) - Click here for Method FAQs and documents 9/2014
Method 16C - Total Reduced Sulfur (Real Time Data) - Click here for Method FAQs and documents 9/2014
Method 17 - In-Stack Particulate (PM) - Click here for Method FAQs and documents 9/2014
Method 18 - VOC by GC - Click here for Method FAQs and documents 9/2014
Method 19 - SO2 Removal & PM, SO2, NOx Rates from Electric Utility Steam Generators - Click here for Method FAQs and documents 9/2014
Method 20 - NOx from Stationary Gas Turbines - Click here for Method FAQs and documents 9/2014
Method 21 - VOC Leaks - Click here for Method FAQs and documents 9/2014
Method 22 - Fugitive Opacity - Click here for Method FAQs and documents 9/2014
Method 23 - Dioxin and Furan (02/91 FR Copy) - Click here for Method FAQs and documents 9/2014
Method 24 - Surface Coatings - Click here for Method FAQs and documents 9/2014
Method 24A - Publication Rotogravure Inks and Related Publication Rotogravure Coatings - Click here for Method FAQs and documents 9/2014
Method 25 - Gaseous Nonmethane Organic Emissions - Click here for Method FAQs and documents 9/2014
Method 25A - Gaseous Organic Concentration (Flame Ionization) - Click here for Method FAQs and documents 9/2014
Method 25B - Gaseous Organic Concentration (Infrared Analyzer) - Click here for Method FAQs and documents 9/2014
Method 25C - NMOC in Landfill Gases - Click here for Method FAQs and documents 9/2014
Method 25D - VOC of Waste Samples - Click here for Method FAQs and documents 9/2014
Method 25E- Vapor Phase Organic Concentration in Waste Samples - Click here for Method FAQs and documents 9/2014
Method 26 - Hydrogen Chloride, Halides, Halogens - Click here for Method FAQs and documents 9/2014
Method 26A - Hydrogen Halide & Halogen-Isokinetic - Click here for Method FAQs and documents 9/2014
Method 27 - Vapor Tightness of Gasoline Tank-Pressure Vacuum - Click here for Method FAQs and documents 9/2014
Method 28 - Certification and Auditing - Wood Heaters - Click here for Method FAQs and documents 9/2014
Method 28A - Air to Fuel Ratio, Burn Rate - Wood-fired Appliances - Click here for Method FAQs and documents 9/2014
Method 29 - Metals Emissions from Stationary Sources - Click here for Method FAQs and documents 9/2014
Method 30A - Determination of Mercury from Coal-Fired Combustion Sources (Instrumental Analyzer Procedure) - Click here for Method FAQs and documents 9/2014
Method 30B - Determination of Mercury from Coal-Fired Combustion Sources Using Carbon Sorbent Traps - Click here for Method FAQs and documents 9/2014
Method 101 - Mercury from Chlor-Alkali Plants (Air) - Click here for Method FAQs and documents 9/2014
Method 101A - Mercury from Sewage Sludge Incinerators - Click here for Method FAQs and documents 9/2014
Method 102 - Mercury from Chlor-Alkali Plants (Hydrogen Streams) - Click here for Method FAQs and documents 9/2014
Method 103 - Beryllium Screening Method - Click here for Method FAQs and documents 9/2014
Method 104 - Beryllium Emissions Determination - Click here for Method FAQs and documents 9/2014
Method 105 -Mercury in Wastewater Treatment Plant Sewage Sludge - Click here for Method FAQs and documents 9/2014
Method 106 - Determination of Vinyl Chloride - Click here for Method FAQs and documents 9/2014
Method 107 - Vinyl Chloride content of Inprocess Wastewater Samples - Click here for Method FAQs and documents 9/2014
Method 107A - Vinyl Choride content of Solvents - Click here for Method FAQs and documents 9/2014
Method 108 - Particulate & Gaseous Arsenic emissions - Click here for Method FAQs and documents 9/2014
Method 108A - Determination of Arsenic Content in Ore Samples from Nonferrous Smelters - Click here for Method FAQs and documents 9/2014
Method 108B - Arsenic - Click here for Method FAQs and documents 9/2014
Method 108C - Arsenic - Click here for Method FAQs and documents 9/2014
Method 111 - Polonium-210 Emissions - Click here for Method FAQs and documents 9/2014
Method 114 - Radionuclide Emissions - Click here for Method FAQs and documents 5-23-97
Method 115 - Radon-222 Emissions - Click here for Method FAQs and documents 4-1-96
Method 201 - PM10 - Click here for Method FAQs and documents 9/2014
Method 201A - PM10 and PM2.5 (In-stack, CRS) (Revised 12-1-2010) - Click here for Method FAQs and documents 9/2014
Method 202 - Condensable Particulate Matter (Revised 12-1-2010) - Click here for Method FAQs and documents 9/2014
Methods 203A - Opacity Determination for Time-Averaged Regulations Click here for Method FAQs and documents 8/2013
Methods 203B - Opacity Determination for Time-Exception Regulations Click here for Method FAQs and documents 8/2013
Methods 203C - Opacity Determination for Instantaneous Limitation Regulations Click here for Method FAQs and documents 8/2013
Method 204-204f Preamble. 4/2007
Method 204 - Permanent or Temporary Total Enclosure (TTE) for Determining Capture Efficiency - Click here for Method FAQs and documents 9/2014
Method 204A - VOCs in Liquid Input Stream - Click here for Method FAQs and documents 9/2014
Method 204B - VOCs in Captured Stream - Click here for Method FAQs and documents 9/2014
Method 204C - VOCs in Captured Stream (Dilution Technique) - Click here for Method FAQs and documents 9/2014
Method 204D - Fugitive VOCs from Temporary Total Enclosure - Click here for Method FAQs and documents 9/2014
Method 204E - Fugitive VOCs from Building Enclosure - Click here for Method FAQs and documents 9/2014
Method 204F - VOCs in Liquid Input Stream (Distillation) - Click here for Method FAQs and documents 9/2014
Method 205 - Gas Dilution Device Certification Procedure - Click here for Method FAQs and documents 9/2014
Method 207 - Presurvey for Corn Wet-Milling Facilities - Click here for Method FAQs and documents 3/8/12
Method 301 - Method Validation Protocol - Click here for Method FAQs and documents 9/2014
Method 303 - By-product Coke Oven Batteries - Click here for Method FAQs and documents 9/2014
Method 303A - Nonrecovery Coke Oven Batteries - Click here for Method FAQs and documents 9/2014
Method 304A - Biodegradation Rates-Vent Option - Click here for Method FAQs and documents 2/2000
Method 304B - Biodegradation Rates - Scrubber Option - Click here for Method FAQs and documents 2/2000
Method 305 - Potential VOC in Waste - Click here for Method FAQs and documents 2/2000
Method 306 - Chromium Emissions Electroplating/Anodizing - Click here for Method FAQs and documents 9/2014
Method 306A - Chromium Emissions Electroplating/Anodizing (Mason Jar Method) - Click here for Method FAQs and documents 9/2014
Method 306B - Surface Tension for Tanks Electroplating/Anodizing - Click here for Method FAQs and documents 2/2000
Method 307 - Emissions from Solvent Vapor Cleaners (Dec. 2, 1994) - Click here for Method FAQs and documents 9/25/96
Method 308 - Methanol Emissions (Appeared in Federal Register 11/14/97) - Click here for Method FAQs and documents 9/2014
Method 310A - Residual Hexane - Click here for Method FAQs and documents 3/14/97
Method 310B - Residual Solvent - Click here for Method FAQs and documents 3/14/97
Method 310C - Residual N-Hexane in EDPM Rubber - Click here for Method FAQs and documents 3/14/97
Method 311 - HAPS in Paints & Coatings - Click here for Method FAQs and documents 1/17/96
Method 312A - Styrene in SBR Latex (GC) - Click here for Method FAQs and documents 3/14/97
Method 312B - Styrene in SBR Latex by Capillary GC - Click here for Method FAQs and documents 3/14/97
Method 312C - Styrene in SBR Latex Produced by Emulsion Polymerization - Click here for Method FAQs and documents 3/14/97
Method 313A - Residual Hydrocarbon in Rubber Crumb - Click here for Method FAQs and documents 3/14/97
Method 313B - Residual HC in Rubber Crumb by Capillary GC - Click here for Method FAQs and documents 3/14/97
Method 315 - PM and MCEM from Aluminum Production Facilities - Click here for Method FAQs and documents 9/2014
Method 316 - Sample & Analysis for Formaldehyde emissions in the Mineral Wool & Wool Fiberglass Industries - Click here for Method FAQs and documents 9/2014
Method 318 - Extractive FTIR Method for Measurement of Emissions from the Mineral Wool and Wool Fiberglass Industries - Click here for Method FAQs and documents 5/24/99
Method 320 - Vapor Phase Organic & Inorganic Emissions by Extractive FTIR - Click here for Method FAQs and documents 5/19/99
Method 321 - Gaseous HCl Emissions at Portland Cement Kilns by FTIR - Click here for Method FAQs and documents 9/2014
Method 323 - Formaldehyde Measurement Using Derivitization - Click here for Method FAQs and documents 3/8/12

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