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I. 1. A. a.(1)(a) i) a)S ($0 ($0 0 (($0 0 0  A_ekqwDocumentDocument StyleI.1.A.a.(1)(a)i)a)jo4Tech InitInitialize Technical StyleS #   1 .1 .1 .1 .1 .1 .1 .1 S  CuyTechnicalTechnical Document Style11.11.1.11.1.1.11.1.1.1.11.1.1.1.1.11.1.1.1.1.1.11.1.1.1.1.1.1.1x?t2PleadingHeader for numbered pleading paper %  &(   aXXX  XaXXa'XaXXXaXX?1('*dE*??1('*dE*?HH1HH2HH3HH4HH5HH6HH7HH8HH910111213141516171819202122232425262728  .+('2$ KT!   <6X9`("Courier NewTT'     0 .   .('2$ KT!   < 9(CourierBold dTable_A&0 d d d'dxd Level 1 Level 2 Level 3 Level 4 Level 5('2$ KT!   ($ (    ) 3452M << deUUXX$%XX$EAXX$<:XQXX%XXO2XXXX0XXC.XX5XX_ %XX COXX0XX[.XX264XXg%XXNW:2XXXXw(XX%XXgO:2XX[ XX 0XX .XX 5XX %XX! COXX )XX $'XXx$100 dfunc{%EA~=~{%Osub2`````0.5``%CO}over{0.264``%Nsub2````(%Osub2`````0.5``%CO)}``times``100} 4#   r^XpP hp x (#%'0*,.8135@8:<H?ACXr,XD XXX]]  Eq.3B1XX FoXX9 lX'3XXF20XX6.XX9XXRXX %XXOf2XXm}%XX}CO82 6func{F_o~=~}func{{20.9`````%Osub2}over{%COsub2}} 4#   r^XpP hp x (#%'0*,.8135@8:<H?ACXr,XD XXX _ Eq.3B2XX}%XX}CO|82XX}(XXD}adjXX})XX|}XXL}%XX}CO82XX\}XX,}%XX}CO func{%CO_2(adj)~=~%CO_2~+~%CO} 4#   r^XpP hp x (#%'0*,.8135@8:<H?ACXr,XD XXX]]  Eq.3B3XX}%XX}O82XXT}(XX}adjXX4})XX}XX}%XXL}O82XXl}XX<}0XX}.XX,}5XX}%XXt }CO func{%O_2(adj)~=~%O_2~~0.5~%CO} 4#   r^XpP hp x (#%'0*,.8135@8:<H?ACXr _  Eq.3B4 XX FoXX9 X'3XXF0XX.XX6209XXFGfdXX}F8c -func{Fsubo~=~{0.209``Fsubd}overFsubc} 4#   r^XpP hp x (#%'0*,.8135@8:<H?ACXr,XD XXX _ Eq.3B5Table_B CRight ParRight-Aligned Paragraph NumbersI.A.1.a.(1)(a)i)a)3|x<6X9`(CourierXx6X@`7X@<6X9`("Courier NewTTXx6X@7X@< 9(CourierBoldTXx `7X( T$  ((3$ KT!   Fj% T M'   RXtXXX<( 9Z &Courier Regular KT!   J  r^XpP hp x (#%'0*,.8135@8:<H?ACXrQ7tXXdd7   METHOD3BGASANALYSISFORTHEDETERMINATIONOF Z EMISSIONRATECORRECTIONFACTOROREXCESSAIR  >   * DXXXpP X* NOTE: Thismethoddoesnotincludeallofthe   specifications(e.g.,equipmentandsupplies)andprocedures  r (e.g.,sampling)essentialtoitsperformance.Some  6 materialisincorporatedbyreferencefromothermethodsinthispart.Therefore,toobtainreliableresults,personsusingthismethodshouldhaveathoroughknowledgeofatleastthefollowingadditionaltestmethods:Method1and3.1.0ScopeandApplication. (  1.1Analytes.*q./ ddd Xdd Xdd X(#(#q, dd ,dd , dd +  301" h 3Analyte 201!j01 2CASNo. 201!j01 2Sensitivity C9!j   01 @xCOxygen(O2)  z 7782447  z 2,000ppmv 6,z x @ @x6CarbonDioxide(CO2)  . 124389  . 2,000ppmv =1,. x @ Px=CarbonMonoxide(CO) 21!. 1 2630080 21!.!1 2N/A1'%." x P  1 1 1.2Applicability.ThismethodisapplicableforthedeterminationofO2,CO2,andCOconcentrationsinthe #& effluentfromfossilfuelcombustionprocessesforuseinexcessairoremissionratecorrectionfactorcalculations.WherecompoundsotherthanCO2,O2,CO,andnitrogen(N2)are N(!, presentinconcentrationssufficienttoaffecttheresults,thecalculationprocedurespresentedinthismethodmustbemodified,subjecttotheapprovaloftheAdministrator. -@'2 Q 1.3Othermethods,aswellasmodificationstotheproceduredescribedherein,arealsoapplicableforalloftheabovedeterminations.Examplesofspecificmethodsandmodificationsinclude:(1)amultipointsamplingmethodusinganOrsatanalyzertoanalyzeindividualgrabsamplesobtainedateachpoint,and(2)amethodusingCO2orO2and .  stoichiometriccalculationstodetermineexcessair.Thesemethodsandmodificationsmaybeused,butaresubjecttotheapprovaloftheAdministrator. 1.4DataQualityObjectives.Adherencetotherequirementsofthismethodwillenhancethequalityofthedataobtainedfromairpollutantsamplingmethods.2.0SummaryofMethod. 0  2.1Agassampleisextractedfromastackbyoneofthefollowingmethods:(1)singlepoint,grabsampling;(2)singlepoint,integratedsampling;or(3)multipoint,integratedsampling.ThegassampleisanalyzedforpercentCO2,percentO2,and,ifnecessary,percentCOusingan ^$" Orsatcombustiongasanalyzer.3.0Definitions.[Reserved] '!& 4.0Interferences. )P#(  4.1Severalcompoundscaninterfere,tovaryingdegrees,withtheresultsofOrsatanalyses.Compoundsthat 2-&, interferewithCO2concentrationmeasurementincludeacid Z gases(e.g.,sulfurdioxide,hydrogenchloride);compounds  thatinterferewithO2concentrationmeasurementinclude   unsaturatedhydrocarbons(e.g.,acetone,acetylene),nitrous  L oxide,andammonia.AmmoniareactschemicallywiththeO2 j  absorbingsolution,andwhenpresentintheeffluentgasstreammustberemovedbeforeanalysis.5.0Safety. \   5.1Disclaimer.Thismethodmayinvolvehazardousmaterials,operations,andequipment.Thistestmethodmaynotaddressallofthesafetyproblemsassociatedwithitsuse.Itistheresponsibilityoftheuserofthistestmethodtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortoperformingthistestmethod. 5.2CorrosiveReagents.AtypicalOrsatanalyzerrequiresfourreagents:agasconfiningsolution,CO2 "4  absorbent,O2absorbent,andCOabsorbent.Thesereagents R$" maycontainpotassiumhydroxide,sodiumhydroxide,cuprouschloride,cuproussulfate,alkalinepyrogallicacid,and/orchromouschloride.Followmanufacturer'soperatinginstructionsandobserveallwarninglabelsforreagentuse.6.0EquipmentandSupplies. &-&,  NOTE: Asanalternativetothesamplingapparatusand Z systemsdescribedherein,othersamplingsystems(e.g., " liquiddisplacement)maybeused,providedsuchsystemsarecapableofobtainingarepresentativesampleandmaintainingaconstantsamplingrate,andare,otherwise,capableofyieldingacceptableresults.UseofsuchsystemsissubjecttotheapprovaloftheAdministrator. 6.1GrabSamplingandIntegratedSampling.SameasinSections6.1and6.2,respectivelyforMethod3. 6.2Analysis.AnOrsatanalyzeronly.ForlowCO2 B (lessthan4.0percent)orhighO2(greaterthan15.0  percent)concentrations,themeasuringburetteoftheOrsatmusthaveatleast0.1percentsubdivisions.ForOrsatmaintenanceandoperationprocedures,followtheinstructionsrecommendedbythemanufacturer,unlessotherwisespecifiedherein.7.0ReagentsandStandards. "D   7.1Reagents.SameasinMethod3,Section7.1. 7.2Standards.SameasinMethod3,Section7.2.8.0SampleCollection,Preservation,Storage,and '!& Transport. )H#(  NOTE: Eachofthethreeproceduresbelowshallbe f+ %* usedonlywhenspecifiedinanapplicablesubpartofthe .-&, standards.TheuseoftheseproceduresforotherpurposesmusthavespecificpriorapprovaloftheAdministrator.AFyritetypecombustiongasanalyzerisnotacceptableforexcessairoremissionratecorrectionfactordeterminations,unlessapprovedbytheAdministrator.IfbothpercentCO2andpercentO2aremeasured,theanalytical .  resultsofanyofthethreeproceduresgivenbelowmayalsobeusedforcalculatingthedrymolecularweight(seeMethod3). 8.1SinglePoint,GrabSamplingandAnalyticalProcedure. 8.1.1Thesamplingpointintheductshalleitherbeatthecentroidofthecrosssectionoratapointnoclosertothewallsthan1.0m(3.3ft),unlessotherwisespecifiedbytheAdministrator. 8.1.2SetuptheequipmentasshowninFigure31ofMethod3,makingsureallconnectionsaheadoftheanalyzeraretight.LeakchecktheOrsatanalyzeraccordingtotheproceduredescribedinSection11.5ofMethod3.Thisleakcheckismandatory. 8.1.3Placetheprobeinthestack,withthetipoftheprobepositionedatthesamplingpoint;purgethesamplinglinelongenoughtoallowatleastfiveexchanges. 2-&, Drawasampleintotheanalyzer.Foremissionratecorrectionfactordeterminations,immediatelyanalyzethesampleforpercentCO2orpercentO2,asoutlinedinSection   11.2.Forexcessairdetermination,immediatelyanalyzethesampleforpercentCO2,O2,andCO,asoutlinedinSection j  11.2,andcalculateexcessairasoutlinedinSection12.2. 8.1.4Aftertheanalysisiscompleted,leakcheck(mandatory)theOrsatanalyzeronceagain,asdescribedinSection11.5ofMethod3.Fortheresultsoftheanalysistobevalid,theOrsatanalyzermustpassthisleaktestbeforeandaftertheanalysis. 8.2SinglePoint,IntegratedSamplingandAnalyticalProcedure. 8.2.1ThesamplingpointintheductshallbelocatedasspecifiedinSection8.1.1. 8.2.2Leakcheck(mandatory)theflexiblebagasinSection6.2.6ofMethod3.SetuptheequipmentasshowninFigure32ofMethod3.Justbeforesampling,leakcheck(mandatory)thetrainbyplacingavacuumgaugeatthecondenserinlet,pullingavacuumofatleast250mmHg(10in.Hg),pluggingtheoutletatthequickdisconnect,andthenturningoffthepump.Thevacuumshouldremainstableforatleast0.5minute.Evacuatetheflexiblebag. 2-&, Connecttheprobe,andplaceitinthestack,withthetipoftheprobepositionedatthesamplingpoint;purgethesamplingline.Next,connectthebag,andmakesurethatallconnectionsaretight. 8.2.3Sampleataconstantrate,orasspecifiedbytheAdministrator.Thesamplingrunmustbesimultaneouswith,andforthesametotallengthoftimeas,thepollutantemissionratedetermination.Collectatleast28liters(1.0ft3)ofsamplegas.Smallervolumesmaybe z  collected,subjecttoapprovaloftheAdministrator. 8.2.4Obtainoneintegratedfluegassampleduringeachpollutantemissionratedetermination.Foremissionratecorrectionfactordetermination,analyzethesamplewithin4hoursafteritistakenforpercentCO2orpercent N O2(asoutlinedinSection11.2).   8.3MultiPoint,IntegratedSamplingandAnalyticalProcedure. 8.3.1Unlessotherwisespecifiedinanapplicableregulation,orbytheAdministrator,aminimumofeighttraversepointsshallbeusedforcircularstackshavingdiameterslessthan0.61m(24in.),aminimumofnineshallbeusedforrectangularstackshavingequivalentdiameterslessthan0.61m(24in.),andaminimumof12traverse 2-&, pointsshallbeusedforallothercases.ThetraversepointsshallbelocatedaccordingtoMethod1. 8.3.2FollowtheproceduresoutlinedinSections8.2.2through8.2.4,exceptforthefollowing:Traverseallsamplingpoints,andsampleateachpointforanequallengthoftime.RecordsamplingdataasshowninFigure33ofMethod3.9.0QualityControl. \   9.1DataValidationUsingFuelFactor.Althoughinmostinstances,onlyCO2orO2measurementisrequired,it > isrecommendedthatbothCO2andO2bemeasuredtoprovidea  checkonthequalityofthedata.ThedatavalidationprocedureofSection12.3issuggested. NOTE :SincethismethodforvalidatingtheCO2andO2 N analysesisbasedoncombustionoforganicandfossilfuelsanddilutionofthegasstreamwithair,thismethoddoesnotapplytosourcesthat(1)removeCO2orO2through "D  processesotherthancombustion,(2)addO2(e.g.,oxygen b$" enrichment)andN2inproportionsdifferentfromthatof &&$ air,(3)addCO2(e.g.,cementorlimekilns),or(4)have '!& nofuelfactor,Fo,valuesobtainable(e.g.,extremely )T#( variablewastemixtures).ThismethodvalidatesthemeasuredproportionsofCO2andO2forfueltype,butthe 6-&, methoddoesnotdetectsampledilutionresultingfromleaksduringoraftersamplecollection.ThemethodisapplicableforsamplescollecteddownstreamofmostlimeorlimestonefluegasdesulfurizationunitsastheCO2addedorremoved  L fromthegasstreamisnotsignificantinrelationtothetotalCO2concentration.TheCO2concentrationsfromother .  typesofscrubbersusingonlywaterorbasicslurrycanbesignificantlyaffectedandwouldrenderthefuelfactorcheckminimallyuseful.10.0CalibrationandStandardization. >  10.1Analyzer.Theanalyzerandanalyzeroperatortechniqueshouldbeauditedperiodicallyasfollows:takeasamplefromamanifoldcontainingaknownmixtureofCO2and ~$ O2,andanalyzeaccordingtotheprocedureinSection11.3. B Repeatthisprocedureuntilthemeasuredconcentrationofthreeconsecutivesamplesagreeswiththestatedvalue0.5percent.Ifnecessary,takecorrectiveaction,asspecifiedintheanalyzerusersmanual. 10.2Rotameter.Therotameterneednotbecalibrated,butshouldbecleanedandmaintainedaccordingtothemanufacturer'sinstruction. 11.0AnalyticalProcedure. b+%*  11.1Maintenance.TheOrsatanalyzershouldbe maintainedaccordingtothemanufacturersspecifications. 11.2GrabSampleAnalysis.ToensurecompleteabsorptionoftheCO2,O2,orifapplicable,CO,make  L repeatedpassesthrougheachabsorbingsolutionuntiltwoconsecutivereadingsarethesame.Severalpasses(threeorfour)shouldbemadebetweenreadings.(Ifconstantreadingscannotbeobtainedafterthreeconsecutivereadings,replacetheabsorbingsolution.)Althoughinmostcases,onlyCO2orO2concentrationisrequired,itis > recommendedthatbothCO2andO2bemeasured,andthatthe  procedureinSection12.3beusedtovalidatetheanalyticaldata. NOTE :Sincethissinglepoint,grabsamplingand N analyticalprocedureisnormallyconductedinconjunctionwithasinglepoint,grabsamplingandanalyticalprocedureforapollutant,onlyoneanalysisisordinarilyconducted.Therefore,greatcaremustbetakentoobtainavalidsampleandanalysis. 11.3IntegratedSampleAnalysis.TheOrsatanalyzermustbeleakchecked(seeSection11.5ofMethod3)beforetheanalysis.Ifexcessairisdesired,proceedasfollows:(1)within4hoursafterthesampleistaken,analyzeit(as 6-&, inSections11.3.1through11.3.3)forpercentCO2,O2,and Z CO;(2)determinethepercentageofthegasthatisN2by  subtractingthesumofthepercentCO2,percentO2,and   percentCOfrom100percent;and(3)calculatepercentexcessair,asoutlinedinSection12.2. 11.3.1ToensurecompleteabsorptionoftheCO2,O2, .  orifapplicable,CO,followtheproceduredescribedinSection11.2. NOTE :AlthoughinmostinstancesonlyCO2orO2is z  required,itisrecommendedthatbothCO2andO2be B measured,andthattheproceduresinSection12.3beusedtovalidatetheanalyticaldata. 11.3.2Repeattheanalysisuntilthefollowingcriteriaaremet: 11.3.2.1ForpercentCO2,repeattheanalytical  procedureuntiltheresultsofanythreeanalysesdifferbynomorethan(a)0.3percentbyvolumewhenCO2isgreater "D  than4.0percentor(b)0.2percentbyvolumewhenCO2is b$" lessthanorequalto4.0percent.AveragethreeacceptablevaluesofpercentCO2,andreporttheresultstothenearest '!& 0.2percent. 11.3.2.2ForpercentO2,repeattheanalytical r+%* procedureuntiltheresultsofanythreeanalysesdifferby 6-&, nomorethan(a)0.3percentbyvolumewhenO2islessthan Z 15.0percentor(b)0.2percentbyvolumewhenO2isgreater  thanorequalto15.0percent.AveragethethreeacceptablevaluesofpercentO2,andreporttheresultstothenearest  L 0.1percent. 11.3.2.3ForpercentCO,repeattheanalyticalprocedureuntiltheresultsofanythreeanalysesdifferbynomorethan0.3percent.AveragethethreeacceptablevaluesofpercentCO,andreporttheresultstothenearest0.1percent. 11.3.3Aftertheanalysisiscompleted,leakcheck(mandatory)theOrsatanalyzeronceagain,asdescribedinSection11.5ofMethod3.Fortheresultsoftheanalysistobevalid,theOrsatanalyzermustpassthisleaktestbeforeandaftertheanalysis. 11.4Standardization.AperiodiccheckofthereagentsandofoperatortechniqueshouldbeconductedatleastonceeverythreeseriesoftestrunsasindicatedinSection10.1.12.0CalculationsandDataAnalysis. '!&  12.1Nomenclature.SameasSection12.1ofMethod3withtheadditionofthefollowing:  &-&,  %EA  L =Percentexcessair. Z  0.2640 L =RatioofO2toN2inair,v/v.L(#L(#  12.2PercentExcessAir.DeterminethepercentageofthegasthatisN2bysubtractingthesumofthepercent  L CO2,percentCO,andpercentO2from100percent.Calculate j  thepercentexcessair(ifapplicable)bysubstitutingtheappropriatevaluesofpercentO2,CO,andN2into   Equation3B1.6879P@<x ( X 0 @XddddddddE z Nwd6 z   (#(#           (#(#   NOTE :Theequationaboveassumesthatambientairis l usedasthesourceofO2andthatthefueldoesnotcontain 4 appreciableamountsofN2(asdocokeovenorblastfurnace R gases).ForthosecaseswhenappreciableamountsofN2are  present(coal,oil,andnaturalgasdonotcontainappreciableamountsofN2)orwhenoxygenenrichmentis "D  used,alternativemethods,subjecttoapprovaloftheAdministrator,arerequired. 12.3DataValidationWhenBothCO2andO2Are '!& Measured. L  )T#(  12.3.1FuelFactor,Fo.Calculatethefuelfactor r+%* (ifapplicable)usingEquation3B2: 6-&, 6;:<QA=z  0 @Xdddddddd@EZ dM@_ Zy   (#(#      (#(#  where: %O2  L =PercentO2byvolume,drybasis.  L  %CO2  L =PercentCO2byvolume,drybasis. j   20.9  L =PercentO2byvolumeinambientair. .   IfCOispresentinquantitiesmeasurablebythismethod,adjusttheO2andCO2valuesusingEquations3B3 \  and3B4beforeperformingthecalculationforFo: z  6>=?P@<x ( X 0 @XddddddddE > d  >K   (#(#           (#(#  6A@BQA=z  0X @Xdddddddd@E dx @_ K߰where: %CO=PercentCObyvolume,drybasis. 12.3.2ComparethecalculatedFofactorwiththe  | expectedFovalues.Table3B1inSection17.0maybeused "@  inestablishingacceptablerangesfortheexpectedFoifthe ^$" fuelbeingburnedisknown.Whenfuelsareburnedincombinations,calculatethecombinedfuelFdandFcfactors '!& (asdefinedinMethod19,Section12.2)accordingtotheprocedureinMethod19,Sections12.2and12.3.ThencalculatetheFofactoraccordingtoEquation3B5. 2-&, 6DCEVFBz X  0 @Xdddddddd@EZ mdM@_  Z  12.3.3CalculatedFovalues,beyondtheacceptable  * rangesshowninthistable,shouldbeinvestigatedbeforeacceptingthetestresults.Forexample,thestrengthofthesolutionsinthegasanalyzerandtheanalyzingtechniqueshouldbecheckedbysamplingandanalyzingaknownconcentration,suchasair;thefuelfactorshouldbereviewedandverified.Anacceptabilityrangeof12percentisappropriatefortheFofactorofmixedfuelswith  variablefuelratios.Theleveloftheemissionraterelativetothecompliancelevelshouldbeconsideredindeterminingifaretestisappropriate;i.e.,ifthe , measuredemissionsaremuchlowerormuchgreaterthanthecompliancelimit,repetitionofthetestwouldnotsignificantlychangethecompliancestatusofthesourceandwouldbeunnecessarilytimeconsumingandcostly.13.0MethodPerformance.[Reserved] '  14.0PollutionPrevention.[Reserved] (j"" 15.0WasteManagement.[Reserved] *.$$ 16.0References. L,%&  SameasMethod3,Section16.0.17.0Tables,Diagrams,Flowcharts,andValidationData.   @X X TABLE3B1.FoFACTORSFORSELECTEDFUELS Z *qFG dd dd dd dd ./(#(#q,<dd ,\ dd +  301"  3@ FuelType 201!l01 2C<#FoRange1'%l   01 1 Coal: L Anthraciteandlignite>(#.41.0161.130  @    L Bituminous>(#.(1.0831.230 | "  Oil: Distillate>(#.#1.2601.413 ^     L Residual>(#.  &1.2101.370 @   Gas: Natural>(#.<< 1.6001.836 "     L Propane>(#.%1.4341.586      L Butane>(#.$1.4051.553    Wood>(#.| | 1.0001.120 n   Woodbark>(#. 1.0031.130 P  A1() xdFE A 2