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J  EMISSION MEASUREMENT TECHNICAL INFORMATION CENTER ; TEST METHOD ; R& 8BibliogrphyBibliography0....fp2Doc InitInitialize Document StyleS "    I. 1. A. a.(1)(a) i) a)S !($0 ($0 0 (($0 0 0   A_ekqwDocumentDocument StyleI.1.A.a.(1)(a)i)a)jo4Tech InitInitialize Technical StyleS $  1 .1 .1 .1 .1 .1 .1 .1 S CuyTechnicalTechnical Document Style11.11.1.11.1.1.11.1.1.1.11.1.1.1.1.11.1.1.1.1.1.11.1.1.1.1.1.1.1x?t2PleadingHeader for numbered pleading paper &  'HR(   .XXXXX?1('*dE*??1('*dE*?HH1HH2HH3HH4HH5HH6HH7HH8HH910111213141516171819202122232425262728  .+('2HR$ 0U!   <6X9`(Courier('2HR$ 0U!     CRight ParRight-Aligned Paragraph NumbersI.A.1.a.(1)(a)i)a)3|d2 Ha`$"Letter GothicX&d H@7X@<6X9`(CouriericXx6X@`7X@< 9(CourierBoldXx `7X( U$   dj% <( 9Z &Courier Regular((3>$ 0U!    r E>'   6XDXXX DXX 0U!   ݛ)XDXXX3 pP hx(#X3  H76D6XXdd7  METHOD5BDETERMINATIONOFNONSULFURICACIDPARTICULATE Z MATTEREMISSIONSFROMSTATIONARYSOURCES  >    p NOTE: Thismethoddoesnotincludeallofthe   specifications(e.g.,equipmentandsupplies)andprocedures  r (e.g.,samplingandanalytical)essentialtoits  6 performance.Somematerialisincorporatedbyreferencefromothermethodsinthispart.Therefore,toobtainreliableresults,personsusingthismethodshouldhaveathoroughknowledgeofatleastthefollowingadditionaltestmethods:Method1,Method2,Method3,Method5.1.0ScopeandApplication. (  p 1.1Analyte.Nonsulfuricacidparticulatematter.NoCASnumberassigned. p 1.2Applicability.Thismethodisdeterminingapplicableforthedeterminationofnonsulfuricacidparticulatematterfromstationarysources,onlywherespecifiedbyanapplicablesubpartoftheregulationsorwhereapprovedbytheAdministratorforaparticularapplication. p 1.3DataQualityObjectives.Adherencetotherequirementsofthismethodwillenhancethequalityofthedataobtainedfromairpollutantsamplingmethods.H2.0SummaryofMethod. X,%+  p Particulatematteriswithdrawnisokineticallyfromthesourceandcollectedonaglassfiberfiltermaintainedatatemperatureof16014$C(32025$F).Thecollected   sampleisthenheatedinanovenat160$C(320$F)for6  L hourstovolatilizeanycondensedsulfuricacidthatmayhavebeencollected,andthenonsulfuricacidparticulatemassisdeterminedgravimetrically.3.0Definitions.[Reserved] \  4.0Interferences.[Reserved] z  5.0Safety. >  p 5.1Disclaimer.Thismethodmayinvolvehazardousmaterials,operations,andequipment.Thistestmethodmaynotaddressallofthesafetyproblemsassociatedwithitsuse.Itistheresponsibilityoftheuserofthistestmethodtoestablishappropriatesafetyandhealthpracticesandtodeterminetheapplicabilityofregulatorylimitationspriortoperformingthistestmethod. "4  6.0EquipmentandSupplies. R$"  p SameasMethod5,Section6.0,withthefollowingadditionandexceptions: p 6.1SampleCollection.Theprobelinerheatingsystemandfilterheatingsystemmustbecapableofmaintainingasamplegastemperatureof16014$C(32025$F). &-&,  p 6.2SamplePreparation.Anovenisrequiredfordryingthesample.7.0ReagentsandStandards.    p SameasMethod5,Section7.0.8.0SampleCollection,Preservation,Storage,and j  Transport. "   p SameasMethod5,withtheexceptionofthefollowing: p 8.1InitialFilterTare.Ovendrythefilterat1605$C(32010$F)for2to3hours,coolina n desiccatorfor2hours,andweigh.Desiccatetoconstantweighttoobtaintheinitialtareweight.UsetheapplicablespecificationsandtechniquesofSection8.1.3ofMethod5forthisdetermination. p 8.2ProbeandFilterTemperatures.Maintaintheprobeoutletandfiltertemperaturesat16014$C(32025$F).  9.0QualityControl.  p  p SameasMethod5,Section9.0.10.0CalibrationandStandardization. R$"  p SameasMethod5,Section10.0.11.0AnalyticalProcedure. '!&  p SameasMethod5,Section11.0,exceptreplaceSection 11.2.2withthefollowing: b+%*  p 11.1ContainerNo.2.Notethelevelofliquidinthe container,andconfirmontheanalysissheetwhetherleakageoccurredduringtransport.Ifanoticeableamountofleakagehasoccurred,eithervoidthesampleorusemethods,subjecttotheapprovaloftheAdministrator,tocorrectthefinalresults.Measuretheliquidinthiscontainereithervolumetricallyto1mlorgravimetricallyto0.5g.Transferthecontentstoatared250mlbeaker,andevaporatetodrynessatambienttemperatureandpressure.Thenovendrytheprobeandfiltersamplesatatemperatureof1605$C(32010$F)for6hours.Coolina  desiccatorfor2hours,andweightoconstantweight.Reporttheresultstothenearest0.1mg.12.0DataAnalysisandCalculations. N  p SameasinMethod5,Section12.0.13.0MethodPerformance.[Reserved]  | 14.0PollutionPrevention.[Reserved] "@  15.0WasteManagement.[Reserved] ^$" 16.0References. "&$  p SameasMethod5,Section17.0.17.0Tables,Diagrams,Flowcharts,andValidationData. )P#( [Reserved]