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Procedures for Detection and Quantitation

 

Federal Advisory Committee on Detection and Quantitation Approaches and Uses in Clean Water Act (CWA) Programs

Summary of Technical Work Group Conference Call #1
June 24, 2005
1:00 – 2:00 p.m. EDT

Action Items

Richard Reding of US EPA will

  • send a roster of all 21 committee members and the 13 Technical Work Group members to Technical Work Group members via email.
  • update the four Technical Work Group members unable to attend the teleconference regarding assignments, composition, ground rules and teleconference protocols.
  • circulate via email a summary of concerns heard during the public comment period on the Revised Assessment Document regarding the current procedures.
  • obtain the current quantitation procedure for the Drinking Water Minimum Reporting Level from Steve Wendelken, US EPA.
  • obtain from US EPA's Office of Resource Conservation and Reclamation its quantitation limit procedure and will post all of the existing procedures on the Engineering and Analysis Division web site for review by all Technical Work Group members and other interested parties.
  • coordinate up to 25 teleconference lines and provide access information for the two calls.

David Rocke, John Phillips and Tim Fitzpatrick will draft definitions and a glossary for review by the Technical Work Group.

John Phillips will

  • email a starter list of definitions for the terms identified by the committee to the group.
  • circulate a schematic that shows where these terms fall on a continuum from zero to “quantification.”
  • send to US EPA the current detection limit procedure that he has worked on with NCASI (Larry LaFleur), ACIL (Richard Burrows) and others.

The facilitators, Triangle Associates, will send the final ground rules, the draft matrix of existing procedures, desirable characteristics, and the draft summary of the first teleconference to Technical Work Group members by email.


Welcome and Introductions

Bob Wheeler, facilitator, welcomed participants to the call at 1:00 p.m. (EDT) and conducted a roll call of Technical Work Group members. He briefly reviewed protocols for the teleconference and explained that ground rules for the Technical Work Group would be sent to all participants early next week.

Protocols for Technical Work Group teleconference meetings

  • Participants on the phone include Technical Work Group members, facilitators, and other interested parties.
  • Participants should keep their phones on mute until they are called upon or wish to speak.
  • Participants who are not members of the Technical Work Group may not speak until the designated public comment period at the end of the teleconference or unless called upon by a Technical Work Group member.
  • Participants should keep comments brief to allow time for others to comment.
  • Participants need to listen to others.
  • When speaking, participants must first identify themselves before commenting.
  • The facilitators are taking notes of the meeting, tracking the overall discussion and decisions made. The facilitators may interrupt to ask for clarification.
  • The facilitator will announce each agenda item, briefly identify the topic and then call for comments by interest group. Each member of the interest group may speak on the topic. The facilitator may also allow for discussion among interest groups on the topic.
  • All participants agree to abide by the Technical Work Group ground rules.

Richard Reding of US EPA and the Designated Federal Officer of the Federal Advisory Committee on Detection and Quantitation Approaches and Uses in Clean Water Act (CWA) Programs (committee) briefly summarized progress made at the first federal advisory committee meeting held in Washington, D.C. June 21-22, 2005. All but one of the 21 committee members attended this meeting, and most members provided individual statements of interest, which will be posted on the EPA website. The committee was given a short history of detection and quantitation procedures, and a list of several current procedures. The committee drafted some characteristics of desirable procedures, recommended a slate of members to serve on a technical workgroup, and charged this workgroup with several tasks which are described under Task Assignments.

To keep the group at a manageable size, the Technical Work Group is comprised of two members from each of the five stakeholder groups represented on the committee, two members from US EPA, and one other member from the federal family (DOD). Although Bill Foreman of the US Geological Survey and one of the developers of the long-term MDL was unable to participate due to workload, he agreed to provide a copy of his procedure for the group to consider.

Task Assignments

Mr. Wheeler described the four assignments from the committee to the Technical Work Group. The Technical Work Group was asked to:

  • Draft definitions of terms and a glossary;
  • Draft a matrix of existing detection and quantitation procedures to be evaluated;
  • Develop characteristics for existing detection and quantitation procedures; and
  • Draft a narrative description of concerns with the existing detection (MDL) and quantitation (ML) procedures.

He explained that the general timeline for completion of any draft products would be at least two weeks before the next committee meeting. The next committee meeting, he said, is to be held on September 29-30, 2005.

  • Definition of terms and glossary

Mr. Wheeler said that the committee had identified the following terms for the Technical Work Group to define:

    • Detection
    • Quantitation
    • False positive
    • False negative
    • Uncertainty
    • L c, L d and L q

He added that it was important to cite sources and the history of the definitions in developing the draft for review.

  • Matrix of existing detection and quantitation procedures

Mr. Wheeler explained that Triangle Associates and US EPA were working together to draft a matrix of procedures and desirable characteristics for these procedures based on input from committee members at the first meeting. He said the draft matrix would be circulated to Technical Work Group members along with the draft summary of the first Technical Work Group meeting before the next teleconference call on July 13, 2005. (See schedule below.) He asked Technical Work Group members to focus on filling in the matrix in preparation for the July 25, 2005 teleconference meeting.

  • Characteristics for existing detection and quantitation procedures

Mr. Wheeler identified the characteristics of a desirable procedure identified by the committee at its first meeting. He explained that the characteristics would be used as criteria to evaluate the procedures and that they would be included in the draft matrix distributed to Technical Work Group members.

Mr. Wheeler asked for additions or clarifications to the characteristics identified by the federal advisory committee. Mr. Reding clarified that Technical Work Group members could add characteristics but could not remove any that the committee had identified.

  • Narrative description of concerns about the existing MDL and ML procedures

Mr. Wheeler suggested that this task would likely be completed once the Technical Work Group had the chance to review, refine and fill in the draft matrix. Mr. Reding briefly described the existing procedures that were evaluated in the Revised Assessment Document (EPA).

Schedule

Mr. Wheeler mentioned the possibility of having assistance from a technical consultant and/or calling on “experts” in the field as the need arose and suggested that Technical Work Group members consider the need for this assistance at future meetings.

Mr. Wheeler proposed and Technical Work Group members agreed to the following schedule:

  • Wednesday, July 13, 2005 from 1:00 p.m. – 2:30 p.m. (EDT)
  • Monday, July 25, 2005 from 5:15 p.m. – 6:45 p.m. (EDT)

Public Comment

Bob Wyeth, ELAB Advisory Committee Chair, expressed his appreciation for the additional phone lines. He asked if there would be a way for other interested people to know when the teleconference meetings would take place. Mr. Reding said that US EPA anticipated having up to 25 lines for each teleconference meeting: 15 would be reserved for Technical Work Group members and the facilitators; the remainder would be for other interested parties. Mr. Reding also added that the next committee meetings were scheduled for September 29-30 (Washington, DC) and December 8-9 (TBD).

Mr. Wheeler thanked everyone and reminded participants that the next Technical Work Group meeting was scheduled for Wednesday, July 13, 2005 from 1:00 p.m. – 2:30 p.m. (EDT).

 

Attendance

 

Technical Work Group Members

  • States: Timothy Fitzpatrick
  • Environmental Laboratories: Steve Bonde and Richard Burrows
  • Environmental Community: Richard Rediske and Dave Rocke
  • POTWs:
  • Industry: Larry LaFleur and John Phillips
  • US EPA: Richard Reding (Office of Water) and Brad Venner (Office of Enforcement and Compliance Assurance)
  • Other Federal:

Triangle Associates - Derek Van Marter and Bob Wheeler

Guests: Steve Wendelken ( US EPA) and Bob Wyeth (ELAB Chair)


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