Basic Information about How to Use SW-846
What is SW-846?
The Test Methods for Evaluating Solid Waste: Physical/Chemical Methods Compendium, also known as SW-846 or the Compendium, is EPA’s official collection of methods for use in complying with the Resource Conservation and Recovery Act (RCRA) regulations. SW-846 is organized into chapters providing guidance on how to use the methods and groups of methods, called “series”, which are organized by topic. The methods and chapters change over time as updates are published to keep up with evolving analytical and measurement needs.
In addition to the methods that are in the official SW-846 compendium, EPA has validated methods. These methods are tested and validated by laboratories and go through extensive review, but they have not been incorporated into SW-846 through the Federal Register process. EPA encourages using the validated methods, if possible, for the most current version of a method.
For more information on how to use the SW-846 Compendium and related documents, please view our collection of frequent questions.
Which Method Should I Use?
Chapter 2 of SW-846 provides general guidance on the important aspects of choosing an analytical method. This chapter also contains more detailed information on the appropriate methods for specific analytes.
Additionally, the interactive table below can be used to find methods by number, analyte, Chemical Abstracts Service (CAS) number, analytical technique, or matrix. Type your search terms into the search box or sort the categories by alphabet. The table includes a listing of all SW-846 Test Method documents along with details on each method a link to the method's PDF document.
Please note that validated methods are not included in this table.
Method # | Title | Type | Analyte | CAS # | Technique | Media/Matrix | Date |
---|---|---|---|---|---|---|---|
#0010 | Modified Method 5 Sampling Train | sampling | semivolatile principal organic hazardous compounds (POHCs) | NA | isokinetic sampling train | emissions | Sept. 1986 |
#0011 | Sampling for Selected Aldehyde and Ketone Emissions from Stationary Sources | sampling | formaldehyde, acetaldehyde,isophorone, propionaldehyde, other aldehydes and ketones | 50-00-0, 75-07-0, 98-86-2, 78-59-1, 123-38-6 | isokinetic extraction | emissions | Dec. 1996 |
#0020 | Source Assessment Sampling System (SASS) | sampling | particulate and semivolatile organic materials | NA | isokinetic sampling train | particulates, emissions | Sept. 1986 |
#0023A | Sampling Method for Polychlorinated Dibenzo-p-Dioxins and Polychlorinated Dibenzofuran Emissions from Stationary Sources | sampling | polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) | NA | isokinetic sampling train | emissions | Dec. 1996 |
#0030 | Volatile Organic Sampling Train | sampling | volatile principal organic hazardous constituents (POHCs) | NA | sampling train | emissions | Sept. 1986 |
#0031 | Sampling Method for Volatile Organic Compounds (SMVOC) | sampling | volatile organic compounds (VOCs) with a boiling point between -15°C and 121°C: acrylonitrile, benzene, bromodichloromethane, carbon disulfide, carbon tetrachloride, chlorodibromomethane, 1,1-dichloroethane, 1,2-dichlororethane, 1,1-dichloroethene, trans-1,2-dichloroethene, 1,2-dichloropropane, 1,3-dichloropropene, methylene chloride, tetrachloroethene, toluene, 1,1,1-trichloroethane, 1,1,2-trichloroethane, trichloroethene, trichlorofluoromethane | 107-13-1, 71-43-2, 75-27-4, 75-15-0, 56-23-5, 124-48-1, 67-66-3, 126-99-8, 74-95-3, 75-34-3, 107-06-2, 75-35-4, 156-60-5, 78-87-5, 542-75-6, 75-09-2, 127-18-4, 108-88-3, 71-55-6, 79-00-5, 79-01-6, 75-69-4 | sampling train | emissions | Dec. 1996 |
#0040 | Sampling of Principle Organic Hazardous Constituents from Combustion Sources Using Tedlar® Bags | sampling | volatile organic compounds (VOCs): 1,1,1-trichloroethane, trichloroethene, 1,1-dichloroethane, 1,1-dichloroethene, 2,2,4-trimethylpentane, allyl chloride, benzene, carbon tetrachloride, methyl chloride, n-hexane, methylene chloride, toluene, trichlorofluoromethane, vinyl bromide, vinyl chloride, methyl bromide, 1,3-butadiene, dichlorofluoromethane, 1,2-dichloro-1,1,2,2-tetrafluoroethane, 1,1,2-trichlorotrifluoroethane, chloroform, 1,2-dichloropropane, tetrachloroethene | 71-55-6, 79-01-6, 75-34-3, 75-35-4, 540-84-1, 107-05-1, 71-43-2, 56-23-5, 74-87-3, 110-54-3, 75-09-2, 108-88-3, 353-54-8, 593-60-2, 75-01-4, 74-83-9, 106-99-0, 75-71-8, 76-14-2, 76-13-1, 67-66-3, 78-87-5, 127-18-4 | time-integrated evacuated Tedlar® bags | emissions | Dec. 1996 |
#0050 | Isokinetic HCl/Cl2 Emission Sampling Train | sampling | hydrogen chloride (HCl), chlorine (Cl2) | 7647-01-0, 7782-50-5 | isokinetic sampling train | emissions | Dec. 1996 |
#0051 | Midget Impinger HCl/Cl2 Emission Sampling Train | sampling | hydrogen chloride (HCl), chlorine (Cl2) | 7647-01-0, 7782-50-5 | midget impinger sampling train | emissions | Dec. 1996 |
#0060 | Determination of Metals in Stack Emissions | sampling | metals: antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), lead (Pb), manganese (Mn), mercury (Hg), nickel (Ni), phosphorus (P), selenium (Se), silver (Ag), thallium (Tl), zinc (Zn) | 7440-36-0, 7440-38-2, 7440-39-3, 7440-41-7, 7440-43-9, 7440-47-3, 7440-48-4, 7440-50-8, 7439-92-1, 7439-96-5, 7439-97-6, 7440-02-0, 7803-51-2, 7782-49-2, 7440-22-4, 7440-28-0, 7440-66-6 | isokinetic chilled impinger sampling train | emissions | Dec. 1996 |
#0061 | Determination of Hexavalent Chromium Emissions from Stationary Sources | sampling | hexavalent chromium (Cr6+) | 18540-29-9 | Isokinetic sampling train | emissions | Dec. 1996 |
#0100 | Sampling for Formaldehyde and Other Carbonyl Compounds in Indoor Air | sampling | Carbonyl Compounds: acetaldehyde, acetone, acrolein, benzaldehyde, butyraldehyde, crotonaldehyde, 2,5-dimethylbenzaldehyde, formaldehyde, hexanal, isovaleraldehyde, propionaldehyde, m-tolualdehyde, o-tolualdehyde, p-tolualdehyde, valeraldehyde | 75-07-0, 67-64-1, 107-02-8, 100-52-7, 123-72-8, 123-73-9, 5779-94-2, 50-00-0, 66-25-1, 590-86-3, 123-38-6, 620-23-5, 529-20-4, 104-87-0, 110-62-3 | Derivatization with 2,4-dinitrophenylhydrazine (DNPH) | indoor air | Dec. 1996 |
25D | Determination of the Volatile Organic Concentration of Waste Samples | determinative | volatile organic compounds (VOCs) | NA | flame ionization detector (FID), electrolytic conductivity detector (ELCD) | air waste | Feb. 2007 |
25E | Determination of Vapor Phase Organic Concentration in Waste Samples | determinative | vapor phase organic compounds | NA | headspace analyzer, flame ionization detector (FID) | air waste | Feb. 2007 |
207/OTM 14 | Method for Measuring Isocyanates | determinative | isocyanates: 2,4-toluene diisocyanate (TDI), 1,6-hexamethylene diisocyanate (HDI), methylene diphenyl diisocyanate (MDI), methyl isocyanate (MI) | 584-84-9, 822-06-0, 101-68-8, 624-83-9 | isokinetic sampling train, high performance liquid chromatography (HPLC) | emissions | Feb. 2007 |
1010A | Test Methods for Flash Point by Pensky-Martens Closed-Cup Tester | characterization | flashpoint | NA | Pensky-Martens Closed-Cup Tester | petroleum products, biodiesel | Nov. 2004 |
1020B | Standard Test Methods for Flash Point by Setaflash (Small Scale) Closed-Cup Apparatus | characterization | flashpoint | NA | small scale closed-cup apparatus | paints, enamels, lacquers, varnishes, other products with a flash point between 0°C and 110°C | Nov. 2004 |
1030 | Ignitability of Solids | Characterization | ignitability | NA | combustion | pastes, granular materials, strips, powders | July 2014 |
1040 | Test Method for Oxidizing Solids | characterization | oxidizing hazard | NA | conical pile-type burning | solids, granular materials | Feb. 2007 |
1050 | Test Methods to Determine Substances Likely to Spontaneously Combust | characterization | spontaneous combustion | NA | pryophoric classification tests | liquid waste, solid waste | Feb. 2007 |
1110A | Corrosivity Toward Steel | characterization | corrosivity | NA | steel exposure | aqueous waste, non-aqueous liquid waste | Nov. 2004 |
1120 | Dermal Corrosion | characterization | corrosivity to skin | NA | in vitro test method | solids, liquids, and emulsions | Dec. 1996 |
1310B | Extraction Procedure (EP) Toxicity Test Method and Structural Integrity Test | characterization | extraction procedure toxicity, structural integrity | NA | extraction, structural integrity test | Liquids, solids, multiphase samples | Nov. 2004 |
1311 | Toxicity Characteristic Leaching Procedure (TCLP) | characterization | toxicity characteristic | NA | extraction | Liquids, solids, multiphase wastes | July 1992 |
1312 | Synthetic Precipitation Leaching Procedure (SPLP) | characterization | mobility of organic and inorganic compounds | NA | synthetic precipitation | liquids, soils, wastes | July 1992 |
1313 | Liquid-Solid Partitioning as a Function of Extract pH Using a Parallel Batch Extraction Procedure | characterization | leaching of inorganic compounds | NA | batch extraction | solid materials | July 2017 |
1314 | Liquid-Solid Partitioning as a Function of Liquid-Solid Ratio for Constituents in Solid Materials Using an Up-Flow Percolation Column Procedure | characterization | leaching of inorganic compounds | NA | up-flow percolation column | granular solid materials | July 2017 |
1315 | Mass Transfer Rates of Constituents in Monolithic or Compacted Granular Materials Using a Semi-Dynamic Tank Leaching Procedure | characterization | leaching of inorganic compounds | NA | tank leaching | monolithic and compacted granular solid materials | July 2017 |
1316 | Liquid-Solid Partitioning as a Function of Liquid-Solid Ratio Using a Parallel Batch Extraction Procedure | characterization | leaching of inorganic compounds | NA | batch extraction | solid materials | July 2017 |
1320 | Multiple Extraction Procedure | characterization | leaching of waste caused by acid rain | NA | multiple extractions | Liquids, solids, multiphase wastes | Sept. 1986 |
1330A | Extraction Procedure for Oily Wastes | characterization | mobile metals | NA | Soxhlet Extraction | oily wastes: API separator sludges, rag oils, slop oil emulsions, other oil wastes from petroleum refining | July 1992 |
1340 | In Vitro Bioaccessibility Assay for Lead in Soil | characterization | lead (Pb) | 7439-92-1 | Extraction | soil | Feb. 2017 |
3005A | Acid Digestion of Waters for Total Recoverable or Dissolved Metals for Analysis by FLAA or ICP Spectroscopy | sample preparation | heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) | Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | acid digestion | surface water, ground water | July 1992 |
3010A | Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by FLAA or ICP Spectroscopy | sample preparation | heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) | Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | acid digestion | aqueous samples, extracts, wastes with suspended solids | July 1992 |
3015A | Microwave Assisted Acid Digestion of Aqueous Samples and Extracts | sample preparation | heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), boron (B), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), strontium (Sr), thallium (Tl), vanadium (V), zinc (Zn) | Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, B: 7440-42-8, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Hg: 7439-97-6, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Sr: 7440-24-6, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | Microwave Assisted Acid Digestion | aqueous samples, drinking water, extracts, wastes with suspended solids | Feb. 2007 |
3020A | Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by GFAA Spectroscopy | sample preparation | heavy metals: beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), lead (Pb), molybdenum (Mo), thallium (Tl), vanadium (V) | Be: 7440-41-7, Cd: 7440-43-9, Cr: 7440-47-3, Co: 7440-48-4, Pb: 7439-92-1, Mo: 7439-98-7, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | acid digestion | aqueous samples, extracts, wastes with suspended solids | July 1992 |
3031 | Acid Digestion of Oils for Metals Analysis by Atomic Absorption or ICP Spectrometry | sample preparation | heavy metals: antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), lead (Pb), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), strontium (Sr), thallium (Tl), vanadium (V), zinc (Zn) | Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Pb: 7439-92-1, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Sr: 7440-24-6, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | acid digestion | oils, oil sludges, tars, waxes, paints, paint sludges, other viscous petroleum products | Dec. 1996 |
3040A | Dissolution Procedure for Oils, Greases, or Waxes | sample preparation | heavy metals: antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), copper (Cu), iron (Fe), lead (Pb), manganese (Mn), nickel (Ni), vanadium (V) | Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Cr: 7440-47-3, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mn: 7439-96-5, Ni: 7440-02-0, V: 7440-62-2 | solvent dissolution | oils, greases, waxes | Dec. 1996 |
3050B | Acid Digestion of Sediments, Sludges, and Soils | sample preparation | heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) | Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | acid digestion | Sediments, Sludges, and Soils | Dec. 1996 |
3051A | Microwave Assisted Acid Digestion of Sediments, Sludges, Soils, and Oils | sample preparation | heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), boron (B), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe) | Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7,B: 7440-42-8, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6 | Microwave Assisted Acid Digestion | Sediments, Sludges, Soils, and Oils | Feb. 2007 |
3052 | Microwave Assisted Acid Digestion of Siliceous and Organically Based Matrices | sample preparation | heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) | Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | Microwave Assisted Acid Digestion | siliceous matrices, organic matrices, and other complex matrices | Dec. 1996 |
3060A | Alkaline Digestion for Hexavalent Chromium | sample preparation | Hexavalent Chromium | 18540-29-9 | Alkaline Digestion | solid waste, soils, sludges, sediment | Dec. 1996 |
3200 | Mercury Species Fractionation and Quantification by Microwave Assisted Extraction, Selective Solvent Extraction and/or Solid Phase Extraction | sample preparation | Mercury species: methylmercury chloride (CH3HgCl), ethylmercury chloride (CH3CH2HgCl), mercury(II) chloride (HgCl2), mercury hydroxide (Hg(OH)2), mercury nitrate (Hg(NO3)3), mercury sulfate (HgSO4), mercury oxide (HgO), Hg2+ complexes, elemental mercury (Hg0), mercury-metal almalgams (Hg0-M), mercury(I) chloride (Hg2Cl2), mercury sulfide (HgS), mercury selenide (HgSe) | CH3HgCl: 115-09-3, CH3CH2HgCl: 107-27-7, HgCl2: 7487-94-7, Hg(NO3)2: 10045-94-0, HgSO4, 13766-44-4, HgO: 21908-53-2, Hg0: 7439-97-6, Hg2Cl2: 10112-91-1, HgS: 1344-48-5, HgSe: 20601-83-6 | Microwave Assisted Extraction, Selective Solvent Extraction, Solid Phase Extraction | soils, sediments | July 2014 |
3500C | Organic Extraction and Sample Preparation | sample preparation guidance | semivolatile organics, nonvolatile organics | NA | Extraction | aqueous and solid samples | Feb. 2007 |
3510C | Separatory Funnel Liquid-Liquid Extraction | sample preparation | organic compounds | NA | Separatory Funnel Liquid-Liquid Extraction | aqueous samples | Dec. 1996 |
3511 | Organic Compounds in Water by Microextraction | sample preparation | Volatile Organic Compounds (VOCs) and Semivolatile Organic Compounds (SVOCs) | NA | Microextracion | water | July 2014 |
3520C | Continuous Liquid-Liquid Extraction | sample preparation | organic | NA | Continuous Liquid-Liquid Extraction | aqueous samples | Dec. 1996 |
3535A | Solid-Phase Extraction (SPE) | sample preparation | organic groups: Phthalate esters, Organochlorine pesticides, Polychlorinated biphenyls (PCBs), Organophosphorus pesticides, Nitroaromatics and nitramines, Explosives, TCLP leachates containing organochlorine pesticides, TCLP leachates containing semivolatiles, TCLP leachates containing phenoxyacid herbicides | NA | solid-phase extraction (SPE) | aqueous samples | Feb. 2007 |
3540C | Soxhlet Extraction | sample preparation | nonvolatile and semivolatile organic compounds | NA | Soxhlet extraction | soils, sludges, solid wastes | Dec. 1996 |
3541 | Automated Soxhlet Extraction | sample preparation | organic analytes | NA | Automated Soxhlet Extraction | soil, sediment, sludges, solid waste | Sept. 1994 |
3542 | Extraction of Semivolatile Analytes Collected Using Method 0010 (Modified Method 5 Sampling Train) | sample preparation | semivolatile organic compounds | NA | Separatory Funnel & Soxhlet Extraction | air sampling train | Dec. 1996 |
3545A | Pressurized Fluid Extraction (PFE) | sample preparation | water soluble organic compounds: semivolatiles, organophosphorus pesticides, organochlorine pesticides, chlorinated herbicides, polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofurans (PCDDs/PCDFs), and diesel range organics (DRO) | NA | pressurized fluid extraction (PFE) | soils, sediments, sludges, solid waste, | Feb. 2007 |
3546 | Microwave Extraction | sample preparation | water insoluble organic compounds: semivolatiles, organophosphorus pesticides, organochlorine pesticides, chlorinated herbicides, phenoxyacid herbicides, substituted phenols, polychlorinated biphenyls (PCBs), and polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofurans (PCDDs/PCDFs) | NA | Microwave Extraction/Soxhlet extraction | soils, clays, sediments, sludges, solid waste | Feb. 2007 |
3550C | Ultrasonic Extraction | sample preparation | nonvolatile and semivolatile organic compounds | NA | Ultrasonic Extraction | soils, sludges, wastes | Feb. 2007 |
3560 | Supercritical Fluid Extraction of Total Recoverable Petroleum Hydrocarbons | sample preparation | total recoverable petroleum hydrocarbons (TRPHs) | NA | supercritical fluid extraction (SFE) | soils, sediments, fly ash, solid-phase extraction media | Dec. 1996 |
3561 | Supercritical Fluid Extraction of Polynuclear Aromatic Hydrocarbons | sample preparation | polynuclear aromatic hydrocarbons (PAHs): acenaphthene, acenaphthylene, anthracene, benz(a)anthracene, benzo(b)fluoranthene, benzo(k)fluoranthene, benzo(g,h,i)perylene, benzo(a)pyrene, chrysene, dibenzo(a,h)anthracene, fluoranthene, fluorene, indeno(1,2,3-cd)pyrene, naphthalene, phenanthrene, pyrene | 83-32-9, 208-96-8, 120-12-7, 56-55-3, 205-99-2, 207-08-9, 191-24-2, 50-32-8, 218-01-9, 53-70-3, 206-44-0, 86-73-7, 193-39-5, 91-20-3, 85-01-8, 129-00-0 | supercritical fluid extraction (SFE) | soils, sediments, fly ash, solid-phase extraction media | Dec. 1996 |
3562 | Supercritical Fluid Extraction of Polychlorinated Biphenyls (PCBs) and Organochlorine Pesticides | sample preparation | polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs): 2,4,4'-Trichlorobiphenyl, 2,2',5,5'-Tetrachlorobiphenyl, 2,2',4,5,5'-Pentachlorobiphenyl , 2,3,3',4,4'-Pentachlorobiphenyl, 2,3',4,4',5-Pentachlorobiphenyl, 2,2',3,3',4,4'-Hexachlorobiphenyl, 2,2',3,4,4',5'-Hexachlorobiphenyl, 2,2',3,4',5',6-Hexachlorobiphenyl, 2,2',4,4',5,5'-Hexachlorobiphenyl, 2,3,3',4,4',5'-Hexachlorobiphenyl, 2,2',3,3',4,4',5-Heptachlorobiphenyl, 2,2',3,4,4',5,5'-Heptachlorobiphenyl, Aldrin, ?-Hexachlorocyclohexane (?-BHC), ?-Hexachlorocyclohexane (?-BHC), ?-Hexachlorocyclohexane (?-BHC, or Lindane), ?-Chlordane, 4,4'-DDD, 4,4'-DDE, 4,4'-DDT, Dieldrin, Endosulfan II, Endrin, Endrin aldehyde, Heptachlor, Heptachlor epoxide | 7012-37-5, 35693-99-3, 37680-73-2, 32598-14-4, 31508-00-6, 38380-07-3, 35065-28-2, 38380-04-0, 35065-27-1, 38380-08-4, 35065-30-6, 35065-29-3, 309-00-2, 319-85-7, 319-86-8, 58-89-9, 5103-71-9, 72-54-8, 72-55-9, 50-29-3, 60-57-1, 33213-65-9, 72-20-8, 7421-93-4, 76-44-8, 1024-57-3 | supercritical fluid extraction (SFE) | soils, sediments, fly ash, solid-phase extraction media | Feb. 2007 |
3572 | Extraction of Chemical Agents from Wipe Samples Using Microextraction | sample preparation | GB (o-Isopropyl methylphosphonofluoridate), VX (O-Ethyl S-2-diisopropylaminoethyl methyl phosphonothiolate), HD [Bis(2-chloroethyl)sulfide] | GB: 107-44-8, VX: 50782-69-9, HD: 505-60-2 | Microextracion | wipe samples | July 2014 |
3580A | Waste Dilution | sample preparation | organic compounds with concentration > 20,000 mg/kg | NA | solvent dilution | non-aqueous wastes | July 1992 |
3585 | Waste Dilution for Volatile Organics | sample preparation | volatile organic compounds (VOCs) with concentration > 1 mg/kg | NA | solvent dilution | non-aqueous wastes | Dec. 1996 |
3600C | Cleanup | sample cleanup guidance | NA | NA | cleanup | sample extracts | Dec. 1996 |
3610B | Alumina Cleanup | sample cleanup | phthalate esters, nitrosamines | NA | separation (alumina) | sample extracts | Dec. 1996 |
3611B | Alumina Column Cleanup and Separation of Petroleum Wastes | sample cleanup | organic analytes | NA | chromatographic separation (alumina) | sample extracts | Dec. 1996 |
3620C | Florisil Cleanup | sample cleanup | phthalate esters, nitrosamines, nitroaromatics, haloethers, aniline & derivatives, chlorinated hydrocarbons, organochlorine pesticides, organophosphates, organophosphorus pesticides, polychlorinated biphenyls (PCBs) | NA | separation (Florisil®) | sample extracts | July 2014 |
3630C | Silica Gel Cleanup | sample cleanup | polynuclear aromatic hydrocarbons (PAHs), derivatized phenolic compounds, organochlorine pesticides, polychlorinated biphenyls (PCBs) as Aroclors, pentafluorobenzyl bromide-derivatized phenols | NA | separation (silica gel) | sample extracts | Dec. 1996 |
3640A | Gel-Permeation Cleanup | sample cleanup | acenaphthene, acenaphthlylene, acetophenone, 2-acetylaminofluorene, aldrin, 4-aminobiphenyl, aniline, anthracene, benomyl, benzenethiol, benzidine, benz(a)anthracene, benzo(b)fluoranthene, benzo(a)pyrene, benzo(k)fluoranthene, benzoic acid, benzotrichloride, benzyl alcohol, benzyl chloride, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, 4-bromophenyl phenyl ether, butyl benzyl phthalate, 2-sec-butyl-4,6-dinitrophenol (Dinoseb), carbazole, carbendazim, alpha-chlordane, gamma-chlordane, 4-chloro-3-methylphenol, 4-chloroaniline, chlorobenzilate, bis(2-chloroethoxy)methane, bis(2-chloroethyl)ether, bis(2-chloroisopropyl)ether, 2-chloronaphthalene, 2-chlorophenol, 4-chlorophenol, 3-chlorophenol, 4-chlorophenyl phenyl ether, 3-chloropropionitrile, chrysene, 2-cresol, 3-cresol, 4-cresol, cyclophosphamide, DDD, DDE, DDT, di-n-butyl phthalate, diallate, dibenzo(a,e)pyrene, dibenzo(a,i)pyrene, dibenzo(a,j)acridine, dibenzo(a,h)anthracene, dibenzofuran, dibenzothiophene, 1,2-dibromo-3-chloropropane, 1,2-dibromoethane, trans-1,4-dichloro-2-butene, cis-1,4-dichloro-2-butene, 1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene, 3,3'-dichlorobenzidine, 2,6-dichlorophenol, 2,4-dichlorophenoxyacetic acid (2,4-D), 2,4-dichlorophenol, 2,4-dichlorotoluene, 1,3-dichloro-2-propanol, dieldrin, diethyl phthalate, dimethoate, dimethyl phthalate, p-dimethylaminoazobenzene, 7,12-dimethyl-benz(a)anthracene, 2,4-dimethylphenol, 3,3-dimethylbenzidine, 4,6-dinitrobenzene, 4,6-dinitro-o-cresol, 1,3-dinitrobenzene, 2,4-dinitrophenol, 2,4-dinitrotoluene, 2,6-dinitrotoluene, diphenylamine, diphenyl ether, 1,2-diphenylhydrazine, disulfoton, endosulfan sulfate, endosulfan I, endosulfan II, endrin, endrin aldehyde, endrin ketone, ethyl methane sulfonate, ethyl methacrylate, bis(2-ethylhexyl)phthalate, famphur, fluorene, fluoranthene, heptachlor, heptachlor epoxide, hexachlorobenzene, hexachlorobutadiene, hexachlorocyclopentadiene, hexachloroethane, hexachloropropene, indeno(1,2,3-cd)pyrene, isodrin, isophorone, cis-isosafrole, trans-isosafrole, kepone, malononitrile, merphos, methoxychlor, 3-methylcholanthrene, 2-methylnaphthalene, methyl parathion, 4,4'-methylene-bis(2-chloroaniline), naphthalene, 1,4-naphthoquinone, 2-naphthylamine, 1-naphthylamine, 5-nitro-o-toluidine, 2-nitroaniline, 3-nitroaniline, 4-nitroaniline, nitrobenzene, 2-nitrophenol, 4-nitrophenol, n-nitrosodi-n-butylamine, n-nitrosodiethanolamine, n-nitrosodiethylamine, n-nitrosodimethylamine, n-nitrosodiphenylamine, n-nitrosodi-n-propylamine, n-nitrosomethylethylamine, n-nitrosomorpholine, n-nitrosopiperidine, n-nitrosopyrolidine, di-n-octyl phthalate, parathion, pentachlorobenzene, pentachloroethane, pentachloronitrobenzene (PCNB), pentachlorophenol, phenacetin, phenanthrene, phenol, 1,2-phenylenediamine, phorate, 2-picoline, pronamide, pyrene, resorcinol, safrole, 1,2,4,5-tetrachlorobenzene, 2,3,5,6-tetrachloronitrobenzene, 2,3,5,6-tetrachlorophenol, 2,3,4,6-tetrachlorophenol, tetratheyl dithiopyrophosphate (Sulfotep), thiosemicarbazide, 2-toluidine, 4-toluidine, thiourea,1-(o-chlorophenyl), toluene-2,4-diamine, 1,2,3-trichlorobenzene, 1,2,4-trichlorobenzene, 2,4,6-trichlorophenol, 2,4,5-trichlorophenol, 2,4,5-trichlorophenoxyacetic acid (2,4,5-T), 2,4,5-trichlorophenoxypropionic acid (2,4,5-TP), warfarin | 83-32-9, 208-96-8, 98-86-2, 53-96-3, 309-00-2, 92-67-1, 62-53-3, 120-12-7, 17804-35-2, 108-98-5, 92-87-5, 56-55-3, 205-99-2, 50-32-8, 191-24-2, 207-08-9, 65-85-0, 98-07-7, 100-51-6, 100-44-7, 319-84-6, 319-85-7, 58-89-9, 319-86-8, 101-55-3, 85-68-7, 88-85-7, 86-74-8, 10605-21-7, 5103-71-9, 5566-34-7, 59-50-7, 106-47-8, 510-15-6, 111-91-1, 111-44-4, 108-60-1, 91-58-7, 95-57-8, 106-48-9, 108-43-0, 7005-72-3, 542-76-7, 218-01-9, 95-48-7, 108-39-4, 106-44-5, 50-18-0, 72-54-8, 72-55-9, 50-29-3, 84-74-2, 2303-16-4, 192-65-4, 189-55-9, 224-42-0, 53-70-3, 132-64-9, 132-65-0, 96-12-8, 106-93-4, 110-57-6, 1476-11-5, 95-50-1, 106-46-7, 541-73-1, 91-94-1, 87-65-0, 94-75-7, 120-83-2, 95-73-8, 96-23-1, 60-57-1, 84-66-2, 60-51-5, 131-11-3, 60-11-7, 57-97-6, 105-67-9, 119-93-7, 534-52-1, 99-65-0, 51-28-5, 121-14-2, 606-20-2, 122-39-4, 101-84-8, 122-66-7, 298-04-4, 1031-07-8, 959-98-8, 33213-65-9, 72-20-8, 7421-93-4, 53494-70-5, 62-50-0, 97-63-2, 117-81-7, 52-85-7, 86-73-7, 206-44-0, 76-44-8, 1024-57-3, 118-74-1, 87-68-3, 77-47-4, 67-72-1, 1888-71-7, 193-39-5, 465-73-6, 78-59-1, 17627-76-8, 4043-71-4, 143-50-0, 109-77-3, 150-50-5, 72-43-5, 56-49-5, 91-57-6, 298-00-0, 101-14-4, 91-20-3, 130-15-4, 91-59-8, 134-32-7, 99-55-8, 88-74-4, 99-09-2, 100-01-6, 98-95-3, 79-46-9, 100-02-7, 924-16-3, 1116-54-7, 55-18-5, 62-75-9, 86-30-6, 621-64-7, 10595-95-6, 59-89-2, 100-75-4, 930-55-2, 117-84-0, 56-38-2, 608-93-5, 76-01-7, 82-68-8, 87-86-5, 62-44-2, 85-01-8, 108-95-2, 95-54-5, 298-02-2, 109-06-8, 23950-58-5, 129-00-0, 108-46-3, 94-59-7, 95-94-3, 117-18-0, 935-95-5, 58-90-2, 3689-24-5, 79-19-6, 106-49-0, 95-53-4, 5344-82-1, 95-80-7, 87-61-6, 120-82-1, 88-06-2, 95-95-4, 93-76-5, 93-72-1, 81-81-2 | gel-permeation chromatography (GPC) | sample extracts | Sept. 1994 |
3650B | Acid-Base Partition Cleanup | sample cleanup | benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, chlordane, chlorinated dibenzodioxins, 2-chlorophenol, chrysene, creosote, cresols, dichlorobenzenes, dichlorophenoxyacetic acid, 2,4-dimethylphenol, dinitrobenzene, 4,6-dinitro-o-cresol, 2,4-dinitrotoluene, heptachlor, hexachlorobenzene, hexachlorobutadiene, hexachloroethane, hexachlorocyclopentadiene, naphthalene, nitrobenzene, 4-nitrophenol, pentachlorophenol, phenol, phorate, 2-picoline, pyridine, tetrachlorobenzenes, tetrachlorophenols, toxaphene, trichlorophenols, 2,4,5-TP (Silvex) | 56-55-3, 50-32-8, 205-99-2, 57-74-9, 95-57-8, 218-01-9, 8001-58-9, 94-75-7, 105-67-9, 25154-54-5, 534-52-1, 121-14-2, 76-44-8, 118-74-1, 87-68-3, 67-72-1, 77-47-4, 91-20-3, 98-95-3, 100-02-7, 87-86-5, 108-95-2, 298-02-2, 109-06-8, 110-86-1, 8001-35-2, 93-72-1, and others | liquid-liquid partitioning | petroleum waste, sample extracts | Dec. 1996 |
3660B | Sulfur Cleanup | sample cleanup | organochlorine pesticides, organophosphorus pesticides | NA | sulfur removal | sediments, marine algae, and industrial wastes containing sulfur | Dec. 1996 |
3665A | Sulfuric Acid/Permanganate Cleanup | sample cleanup | polychlorinated biphenyls (PCBs) | NA | separation (sulfuring acid) | sample extracts | Dec. 1996 |
3815 | Screening Solid Samples for Volatile Organics | screening | volatile organic compounds (VOCs) | NA | photoionization detection (PID) | soils, solids | Feb. 2007 |
3820 | Hexadecane Extraction and Screening of Purgeable Organics | screening | purgeable organics | NA | hexadecane extraction and gas chromatography/ flame-ionization detection (GC/FID) | not specified | Sept. 1986 |
4000 | Immunoassay | screening guidance | organic and inorganic analytes | NA | Immunoassay | environmental and waste matrices | Dec. 1996 |
4010A | Screening for Pentachlorophenol by Immunoassay | screening | pentachlorophenol (PCP) | 87-86-5 | Immunoassay | soils, sludges, aqueous media | Dec. 1996 |
4015 | Screening for 2,4-Dichlorophenoxyacetic Acid by Immunoassay | screening | 2,4-dichloropyhenoxyacetic acid (2,4-D) | 94-75-7 | Immunoassay | soils, aqueous matrices | Dec. 1996 |
4020 | Screening for Polychlorinated Biphenyls by Immunoassay | screening | polychlorinated biphenyls (PCBs) | NA | Immunoassay | soils, non-aqueous liquid waste | Dec. 1996 |
4025 | Screening for Polychlorinated Dibenzodioxins and Polychlorinated Dibenzofurans (PCDD/PCDFs) By Immunoassay | screening | Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) | NA | Immunoassay | soil | July 2014 |
4030 | Soil Screening for Petroleum Hydrocarbons by Immunoassay | screening | total petroleum hydrocarbons (TPH) | NA | Immunoassay | soils | Dec. 1996 |
4035 | Soil Screening for Polynuclear Aromatic Hydrocarbons by Immunoassay | screening | polynuclear aromatic hydrocarbons (PAHs) | NA | Immunoassay | soils | Dec. 1996 |
4040 | Soil Screening for Toxaphene by Immunoassay | screening | toxaphene | 8001-35-2 | Immunoassay | soils | Dec. 1996 |
4041 | Soil Screening for Chlordane by Immunoassay | screening | Chlordane | 57-74-9 | Immunoassay | soils | Dec. 1996 |
4042 | Soil Screening for DDT by Immunoassay | screening | 1,1,1-trichloro-2,2-bis(4-chlorophenyl)ethane (DDT) | 50-29-3 | Immunoassay | soils | Dec. 1996 |
4050 | TNT Explosives in Soil by Immunoassay | screening | trinitrotoluene (TNT) | 118-96-7 | Immunoassay | soils | Dec. 1996 |
4051 | Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) in Soil by Immunoassay | screening | hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) | 121-82-4 | Immunoassay | soils | Dec. 1996 |
4425 | Screening Extracts of Environmental Samples for Planar Organic Compounds (PAHs, PCBs, PCDDs/PCDFs) by a Reporter Gene on a Human Cell Line | screening | polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs), coplanar polychlorinated biphenyl (PCB) congeners, high molecular weight polynuclear aromatic hydrocarbons (PAHs) | NA | reporter gene system (RGS) | soil, sediment, tissue, and water extracts | Feb. 2007 |
4430 | Screening for Polychlorinated Dibenzo-p-dioxins and Poly chlorinated Dibenzofurans (PCDD/PCDFs) in Soil and Sediments Using an Aryl Hydrocarbon Receptor-Based PCR Assay | screening | Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) | NA | Aryl Hydrocarbon Receptor-Based PCR Assay | soil and sediments | July 2014 |
4435 | Screening for Dioxin-like Chemical Activity in Soils and Sediments Using the CALUX® Bioassay and TEQ Determinations | screening | Dioxin-like Chemicals | NA | CALUX® Bioassay and Toxic Equivalent (TEQ) Determinations | soil and sediments | July 2014 |
4670 | Triazine Herbicides as Atrazine in Water by Quantitative Immunoassay | determinative | Atrazine | 1912-24-9 | Immunoassay | water | Feb. 2007 |
5000 | Sample Preparation for Volatile Organic Compounds | sample preparation guidance | volatile organic compounds (VOCs) | NA | NA | aqueous waste, soil, sediment, solid waste, organic solvents, air, oily waste | Dec. 1996 |
5021A | Volatile Organic Compounds in Various Sample Matrices Using Equilibrium Headspace Analysis | sample preparation | volatile organic compounds (VOCs): Benzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, Carbon tetrachloride, Chlorobenzene, Chloroethane, Chloroform, Chloromethane, Dibromochloromethane, 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, Ethylbenzene, Hexachlorobutadiene, Methylene chloride, Naphthalene, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, Vinyl chloride, o-Xylene, m-Xylene, p-Xylene, gasoline range organics, bromobenzene, n-butylbenzene, sec-butylbenzene, tert-butylbenzene, 2-chlorotoluene, 4-chlorotoluene, cis-1,2-dichloroethene, 1,3-dichloropropane, 2,2-dichloropropane, 1,1-dichloropropene, isopropylbenzene, 4-isoproyltoluene, n-propylbenzene, 1,2,3-trichlorobenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene | 71-43-2, 74-97-5,75-27-4, 75-25-2, 74-83-9, 56-23-5,108-90-7, 75-00-3, 67-66-3, 74-87-3, 124-48-1,96-12-8, 106-93-4, 74-95-3, 95-50-1, 541-73-1, 106-46-7, 75-71-8, 75-34-3, 107-06-2, 75-35-4, 156-60-5, 78-87-5, 100-41-4, 87-68-3, 75-09-2, 91-20-3, 100-42-5, 630-20-6, 79-34-5, 127-18-4, 108-88-3, 120-82-1, 71-55-6, 79-00-5, 79-01-6, 75-69-4, 96-18-4, 75-01-4, 95-47-6, 108-38-3, 106-42-3, 108-86-1, 104-51-8, 135-98-8, 98-06-6, 95-49-8, 106-43-4, 156-59-4, 142-28-9, 590-20-7, 563-58-6, 98-82-8, 99-87-6, 103-65-1, 87-61-6, 95-63-6, 108-67-8 | equilibrium headspace analysis | soils, sediments, solid waste, aqueous samples, water-miscible liquids | July 2014 |
5030B | Purge-and-Trap for Aqueous Samples | sample preparation | volatile organic compounds (VOCs) with boiling points < 200 C | NA | purge-and-trap | aqueous samples, water miscible liquid samples, soil and waste sample extracts | Dec. 1996 |
5031 | Volatile, Nonpurgeable, Water-Soluble Compounds by Azeotropic Distillation | sample preparation | nonpurgeable, water-soluble, and volatile organic compounds: Acetone, Acetonitrile, Acrylonitrile, Allyl alcohol, 1-Butanol, t-Butyl alcohol, Crotonaldehyde, 1,4-Dioxane, Ethanol, Ethyl Acetate, Ethylene oxide, Isobutyl alcohol, Methanol, Methyl ethyl ketone, Methyl isobutyl ketone, N-Nitroso-di-n-butylamine, Paraldehyde, 2-Pentanone, 2-Picoline, 1-Propanol, 2-Propanol, Propionitrile, Pyridine, o-Toluidine | 67-64-1, 75-05-8, 107-13-1, 107-18-6, 104-51-8, 75-65-0, 123-73-9, 123-91-1, 64-17-5, 141-78-6, 75-21-8, 78-83-1, 67-56-1, 78-93-3, 108-10-1, 924-16-3, 123-63-7, 107-87-9, 109-06-8, 71-23-8, 67-63-0, 107-12-0, 110-86-1, 95-53-4 | Azeotropic Distillation | aqueous samples, leachates from solid matrices | Dec. 1996 |
5032 | Volatile Organic Compounds by Vacuum Distillation | determinative | volatile organic compounds (VOCs): Acetone, Acrolein, Acrylonitrile, Benzene, Bromodichloromethane, Bromoform, Bromomethane, 2-Butanone, Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, 2-Chloroethyl vinyl ether, Chloroform, Chloromethane, Dibromomethane, 1,4-Dichloro-2-butene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, Ethanol, Ethylbenzene, Ethyl methacrylate, 2-Hexanone, Iodomethane, Methylene chloride, 4-Methyl-2-pentanone, Styrene, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, Vinyl acetate, Vinyl chloride, m-Xylene, p-Xylene, o-Xylene | 67-64-1, 107-02-8, 107-13-1, 71-43-2, 75-27-4, 75-25-2,74-83-9, 78-93-3, 75-15-0, 56-23-5, 108-90-7, 124-48-1,75-00-3, 110-75-8,67-66-3, 74-87-3, 74-95-3, 764-41-0, 75-71-8, 75-35-4, 107-06-2, 75-35-3, 156-60-5, 78-87-5, 10061-01-5, 10061-02-6, 64-17-5, 100-41-4, 97-63-2, 591-78-6, 74-88-4, 75-09-2, 108-10-1, 100-42-5, 79-34-5, 75-71-8, 75-35-4, 107-06-2, 75-35-3,156-60-5, 78-87-5, 10061-01-5, 10061-02-6,l 64-17-5, 100-41-4, 97-63-2, 591-78-6, 74-88-4, 75-09-2, 108-10-1, 100-42-5, 79-34-5 | Vacuum Distillation | liquids, solids, oily waste, animal tissues | Dec. 1996 |
5035 | Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples | sample preparation | volatile organic compounds (VOCs) | NA | purge-and-trap, extraction | soils, sediments, solid waste | Dec. 1996 |
5041A | Analysis for Desorption of Sorbent Cartridges from Volatile Organic Sampling Train (VOST) | determinative | non-polar organic compounds: Acetone, Acrylonitrile, Benzene, Bromodichloromethane, Bromoform, Bromomethane, Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, Chloroform, Chloromethane, Dibromomethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, Ethylbenzene, Iodomethane, Methylene chloride, Styrene, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, Vinyl chloride, Xylenes | 67-64-1, 107-13-1, 71-43-2, 75-27-4, 75-25-2, 74-83-9, 75-15-0, 56-23-5, 108-90-7, 124-48-1, 75-00-3, 67-66-3, 74-87-3, 74-95-3, 75-35-3, 107-06-2, 75-35-4, 156-60-5, 78-87-5, 10061-01-5, 10061-02-6, 100-41-4, 74-88-4, 75-09-2, 100-42-5, 79-34-5, 127-18-4, 108-88-3, 71-55-6, 79-00-5 | desorption | sorbent cartridges from stack gas effluents | Dec. 1996 |
5050 | Bomb Preparation Method for Solid Waste | sample preparation | chlorine (Cl2) | 7782-50-5 | bomb oxidation | solid waste, oily waste, fuels | Sept. 1994 |
6010D | Inductively Coupled Plasma-Optical Emissions Spectrometry | determinative | heavy metals: aluminum (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), boron (B) cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), lithium (Li), magnesium (Mg). magnese (Mn), mercury (Hg), molybdenum (Mo), nickel (Ni), phosphorous (P), potassium (K), selenium (Se), silica (SiO2), silver (Ag), sodium (Na), strotium (Sr), thallium (Tl), tin (Sn), titanium (Ti), vanadium (V), zinc (Zn) | Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Li: 7439-93-2, Mg: 7439-95-4, Mn: 7439-96-5, Hg: 7439-97-6, Mo: 7439-98-7, Ni: 7440-02-0, P: 7723-14-0, K: 7440-09-7, Se: 7782-49-2, SiO2: 7631-86-9, Ag: 7440-22-4, Na: 7440-23-5, Sr: 7440-24-6, Tl: 7440-28-0, Sn: 7440-31-5, Ti: 7440-32-6V: 7440-62-2, Zn: 7440-66-6 | Inductively Coupled Plasma-Atomic (or Optical) Emission Spectrometry (ICP-AES or ICP-OES) | groundwater, digested aqueous and solid matrices | July 2018 |
6020B | Inductively Coupled Plasma-Mass Spectrometry | determinative | heavy metals: aluminum (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), mercury (Hg), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) | Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1,Mg: 7439-95-4, Mn: 7439-96-5, Hg: 7439-97-6, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | Inductively coupled plasma-mass spectrometry (ICP-MS) | water samples, waste extracts, digests | July 2014 |
6200 | Field Portable X-Ray Fluorescence Spectrometry for the Determination of Elemental Concentrations in Soil and Sediment | Determinative | heavy metals: antimony (Sb), arsenic (As), barium (Ba), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), lead (Pb), mercury (Hg), nickel (Ni), selenium (Se), silver (Ag), thallium (Tl), tin (Sn), vanadium (V), zinc (Zn), iron (Fe), manganese (Mn), molybdenum (Mo), potassium (K), rubidium (Rb), strontium (Sr), thorium (Th), titanium (Ti), zirconium (Zr) | Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Pb: 7439-92-1, Hg: 7439-97-6, Ni: 7440-02-0, Se: 7782-49-2, Ag: 7440-22-4, Tl: 7440-28-0, Sn: 7440-31-5, V: 7440-62-2, Zn: 7440-66-6, 7439-89-6, 7439-96-5, 7439-93-7, 7440-09-7, 7440-17-7, 7440-24-6, 7440-29-1, 7440-32-6, 7440-67-7 | X-ray Fluorescence | soils, sediment | Feb. 2007 |
6500 | Dissolved Inorganic Anions in Aqueous Matrices by Capillary Ion Electrophoresis | Determinative | inorganic anions: bromide, chloride, fluoride, nitrate, nitrite, o-phosphate, sulfate | 24959-67-9, 16887-00-6, 16984-48-8, 14797-55-8, 14797-65-0, 14265-44-2, 14808-79-8 | Capillary Ion Electrophoresis | aqueous matrices: drinking water, wastewater, ground water) | Feb. 2007 |
6800 | Elemental and Molecular Speciated Isotope Dilution Mass Spectrometry | determinative | heavy metals: antimony (Sb), boron (B), barium (Ba), cadmium (Cd), calcium (Ca), chromium (Cr), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), mercury (Hg), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), strontium (Sr), thallium (Tl), vanadium (V), zinc (Zn) | Sb: 7440-36-0, B: 7440-42-8, Ba: 7440-39-3, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Hg: 7439-97-6, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Sr: 7440-24-6, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 | isotope dilution mass spectrometry (IDMS), molecular speciated isotope dilution mass spectrometry (SIDMS) | water samples, solid samples, extracts, digests, blood, foods | July 2014 |
7000B | Flame Atomic Absorption Spectrophotometry | Determinative | heavy metals: aluminum (Al), antimony (Sb), Barium (Ba), beryllium (Be) cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), lithium (Li), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), nickel (Ni), osmium (Os), potassium (K), silver (Ag), sodium (Na), strontium (Sr), thallium (Tl), tin (Sn), vanadium (V), zinc (Zn) | Al: 7429-90-5, Sb: 7440-36-0, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Li: 7439-93-2, Mg: 7439-95-4, Mn: 7439-96-5, Hg: 7439-97-6, Mo: 7439-98-7, Ni: 7440-02-0, Os: 7440-04-2, K: 7440-09-7, Ag: 7440-22-4, Na: 7440-23-5, Sr: 7440-24-6, Tl: 7440-28-0, Sn: 7440-31-5, V: 7440-62-2, Zn: 7440-66-6 | flame atomic absorption spectrophotometry (FLAA or FAAS) | groundwater, aqueous samples, extracts, industrial waste, soils, sludges, sediments | Feb. 2007 |
7010 | Graphite Furnace Atomic Absorption Spectrophotometry | Determinative | heavy metals: , antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), manganese (Mn), molybdenum (Mo), nickel (Ni), selenium (Se), silver (Ag), thallium (Tl), vanadium (V), zinc (Zn) | Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, Se: 7782-49-2, Ag: 7440-22-4, Tl: 7440-28-0, Sn: 7440-31-5, V: 7440-62-2, Zn: 7440-66-6 | graphite furnace atomic absorption spectrophotometry (GFAA or GFAAS) | ground water, domestic wastes, industrial wastes, extracts, soils, sludges, sediments | Feb. 2007 |
7061A | Arsenic (Atomic Absorption, Gaseous Hydride) | Determinative | arsenic (As) | 7440-38-2 | Atomic Absorption Spectrophotometry (AAS) | wastes, mobility procedure extracts, soils, ground water | July 1992 |
7062 | Antimony and Arsenic (Atomic Absorption, Borohydride Reduction) | Determinative | arsenic (As), antimony (Sb) | 7440-38-2, 7440-36-0 | Atomic Absorption Spectrophotometry (AAS) | wastes, mobility procedure extracts, soils, ground water | Sept. 1994 |
7063 | Arsenic in Aqueous Samples and Extracts by Anodic Stripping Voltammetry (ASV) | Determinative | arsenic (As) | 7440-38-2 | anodic stripping voltammetry (ASV) | drinking water, natural surface water, seawater, domestic/industrial wastewater, soil extracts | Dec. 1996 |
7195 | Chromium, Hexavalent (Coprecipitation) | Determinative | Hexavalent Chromium (Cr(VI)) | 18540-29-9 | Coprecipitation and atomic absorption spectroscopy (AAS) | Extraction Procedure (EP) toxicity characteristic extracts, ground water | Sept. 1986 |
7196A | Chromium, Hexavalent (Chelation/Extraction) | Determinative | Hexavalent Chromium (Cr(VI)) | 18540-29-9 | colorimetry | Extraction Procedure (EP) toxicity characteristic extracts, ground water | July 1992 |
7197 | Chromium, Hexavalent (Chelation/Extraction) | Determinative | Hexavalent Chromium (Cr(VI)) | 18540-29-9 | Chelation/Extraction and atomic absorption spectroscopy (AAS) | Extraction Procedure (EP) toxicity characteristic extracts, ground water | Sept. 1986 |
7198 | Chromium, Hexavalent (Differential Pulse Polarography) | Determinative | Hexavalent Chromium (Cr(VI)) | 18540-29-9 | Differential Pulse Polarography | natural waters, waste waters, extraction procedure (EP) extracts | Sept. 1986 |
7199 | Determination of Hexavalent Chromium in Drinking Water, Groundwater and Industrial Wastewater Effluents by Ion Chromatography | Determinative | Hexavalent Chromium (Cr(VI)) | 18540-29-9 | ion chromotography | ground water, drinking water, industrial wastewater effluents | Dec. 1996 |
7470A | Mercury in Liquid Waste (Manual Cold-Vapor Technique) | Determinative | Mercury (Hg) | 7439-97-6 | Cold- vapor Atomic Absorption | mobility-procedure extracts, aqueous wastes, ground water | Sept. 1994 |
7471B | Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique) | Determinative | Mercury (Hg) | 7439-97-6 | Cold- vapor Atomic Absorption | soils, sediments, bottom deposits, sludge materials | Feb. 2007 |
7472 | Mercury in Aqueous Samples and Extracts by Anodic Stripping Voltammetry (ASV) | Determinative | Mercury (Hg) | 7439-97-6 | Anodic Stripping Voltammetry (ASV) | drinking water, natural surface water, seawater, domestic/industrial wastewater, soil extracts | Dec. 1996 |
7473 | Mercury in Solids and Solutions by Thermal Decomposition, Amalgamation, and Atomic Absorption Spectrophotometry | Determinative | Mercury (Hg) | 7439-97-6 | Thermal Decomposition and Atomic Absorption Spectrophotometry (AAS) | solids, aqueous samples, digested solutions | Feb. 2007 |
7474 | Mercury in Sediment and Tissue Samples by Atomic Fluorescence Spectrometry | Determinative | Mercury (Hg) | 7439-97-6 | atomic fluorescence spectrometry (AFS) | sediment, tissue | Feb. 2007 |
7580 | White Phosphorus (P4) by Solvent Extraction and Gas Chromatography | Determinative | White Phosphorus (P4) | 7723-14-0 | Solvent Extraction, Gas Chromatography (GC) | soil, sediment, water | Dec. 1996 |
7741A | Selenium (Atomic Absorption, Gaseous Hydride) | Determinative | Selenium (Se) | 7782-49-2 | atomic absorption spectroscopy (AAS), gaseous hydride | wastes, mobility procedure extracts, soils, ground water | Sept. 1994 |
7742 | Selenium (Atomic Absorption, Borohydride Reduction) | Determinative | Selenium (Se) | 7782-49-2 | atomic absorption spectroscopy (AAS), borohydride reduction | wastes, mobility procedure extracts, soils, ground water | Sept. 1994 |
8000D | Determinative Chromatographic Separations | determinative guidance | Perchlorate, white phosphorus (P4), ethylene dibromide (EDB), dibromochloropropane (DBCP), nonhalogenated volatiles, volatiles, acrylonitrile, acrylamide, acetonitrile, phenols, phthalates, nitrosamines, organochlorine pesticides, polychlorinated biphenyls (PCBs), nitroaromatics, cyclic ketones, polynuclear aromatic hydrocarbons (PAHs), haloethers, chlorinated hydrocarbons, aniline & derivatives, organophosphorus pesticides, acid herbicides, semivolatiles, toxaphene and congeners, dioxins, dibenzofurans, carbonyl compounds, acrolein, n-methyl carbamates, nonvolatiles, nitramines, tetrazene, nitroglycerine, bis(2-chloroethyl)ether hydrolysis products | NA | chromatography | NA | July 2014 |
8011 | 1,2-Dibromoethane and 1,2-Dibromo-3-chloropropane by Microextraction and Gas Chromatography | Determinative | 1,2-dibromethane, 1,2-dibromo-3-chloropropane | 106-93-4, 96-12-8 | microextraction, Gas chromatography (GC) | ground water, drinking water | July 1992 |
8015C | Nonhalogenated Organics by Gas Chromatography | Determinative | nonhalogenated volatiles and semi volatile organic compounds: Acetone, Acetonitrile, Acrolein, Acrylonitrile, Allyl alcohol, t-Amyl alcohol (TAA), t-Amyl ethyl ether (TAEE), t-Amyl methyl ether (TAME), Benzene, t-Butyl alcohol (TBA), Crotonaldehyde, Diethyl ether, Diisopropyl ether (DIPE), Ethanol, Ethyl acetate, Ethyl benzene, Ethylene oxide, Ethyl tert-butyl ether (ETBE), Isopropyl alcohol (2-Propanol), Methanol, Methyl ethyl ketone (MEK, 2-Butanone), Methyl tert-butyl ether (MTBE), N-Nitroso-di-n-butylamine, Paraldehyde, 2-Pentanone, 2-Picoline, 1-Propanol (n-Propyl alcohol), Propionitrile (Ethyl cyanide), Pyridine, Toluene, o-Toluidine, o-Xylene, m-Xylene, p-Xylene, triethylamine, gasoline range organics (GRO), diesel range organics (DRO) | 67-64-1, 75-05-8, 107-02-8, 107-13-1, 107-18-6, 75-85-4, 919-94-8, 994-05-8, 71-43-2, 75-65-0, 123-73-9, 60-29-7, 108-20-3, 64-17-5, 141-78-6, 100-41-4, 75-21-8, 637-92-3, 67-63-0, 67-56-1, 78-93-3, 1634-04-4, 924-16-3, 123-63-7, 107-87-9, 109-06-8, 71-23-8, 107-12-0, 110-86-1, 108-88-3, 95-53-4, 95-47-6, 108-38-3, 106-42-3, 121-44-8 | Gas chromatography (GC) | water, aqueous wastes, extracts | Feb. 2007 |
8021B | Aromatic and Halogenated Volatiles by Gas Chromatography Using Photoionization and/or Electrolytic Conductivity Detectors | Determinative | aromatic and halogenated volatiles: Allyl chloride, Benzene, Benzyl chloride, Bis(2-chloro-1-methylethyl)ether, Bromoacetone, Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, 2-Chloroethanol, 2-Chloroethyl vinyl ether, Chloroform, Chloromethyl methyl ether, Chloroprene, Chloromethane, 4-Chlorotoluene, 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, cis-1,2-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, 1,3-Dichloro-2-propanol, cis-1,3-dichloropropene, trans-1,3-dichloropropene, Epichlorhydrin, Ethylbenzene, Hexachlorobutadiene, Methylene chloride, Naphthalene, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, Vinyl chloride, o-Xylene, m-Xylene, p-Xylene | 107-05-1, 71-43-2, 100-44-7, 108-60-1, 598-31-2, 108-86-1, 74-97-5, 75-27-4, 75-25-2, 74-83-9, 56-23-5, 108-90-7, 124-48-1, 75-00-3, 107-07-03, 110-75-8, 67-66-3, 107-30-2, 126-99-8, 74-87-3, 106-43-4, 96-12-8, 106-93-4, 74-95-3, 95-50-1, 541-73-1, 106-46-7, 75-71-8, 75-34-3, 107-06-2, 75-35-4, 156-59-2, 156-60-5, 78-87-5, 96-23-1, 96-23-1, 10061-02-6, 106-89-8, 100-41-4, 87-68-3, 75-09-2, 91-20-3, 100-42-5, 630-20-6, 79-34-5, 127-18-4, 108-88-3, 120-82-1, 71-55-6, 79-00-5, 79-01-6, 75-69-4, 96-18-4, 75-01-4, 95-47-6, 108-38-3, 106-42-3 | Gas chromatography (GC) with photoionization, electrolytic conductivity detection | ground water, aqueous sludges, caustic liquors, acid liquors, waste solvents, oily wastes, mousses, tars, fibrous wastes, polymeric emulsions, filter cakes, spent carbons, spent catalysts, soils, sediments | July 2014 |
8031 | Acrylonitrile by Gas Chromatography | Determinative | acrylonitrile | 107-13-1 | Gas chromatography (GC) with nitrogen–phosphorus detection | water | Sept. 1994 |
8032A | Acrylamide by Gas Chromatography | Determinative | acrylamide | 79-06-1 | Gas chromatography (GC) with electron capture detection | aqueous matrices | Dec. 1996 |
8033 | Acetonitrile by Gas Chromatography with Nitrogen-Phosphorus Detection | Determinative | acetonitrile | 75-05-8 | Gas chromatography (GC) with nitrogen–phosphorus detection | aqueous matrices | Dec. 1996 |
8041A | Phenols by Gas Chromatography | Determinative | phenols: 4-Chloro-3-methylphenol, 2-Chlorophenol, 2,4-Dichlorophenol, 2,6-Dichlorophenol, 2,4-Dimethylphenol, 2,4-Dinitrophenol, Dinoseb (2-sec-Butyl-4,6-dinitro phenol), 2-Methyl-4,6-dinitrophenol, 2-Methylphenol (o-Cresol), 3-Methylphenol (m-Cresol), 4-Methylphenol (p-Cresol), 4-Nitrophenol, Pentachlorophenol, Phenol, 2,3,4,6-Tetrachlorophenol, 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol, 2-Chloro-5-methylphenol, 4-Chloro-2-methylphenol, 3-Chlorophenol, 4-Chlorophenol, 2-Cyclohexyl-4,6-dinitrophenol, 2,3-Dichlorophenol, 2,5-Dichlorophenol, 3,4-Dichlorophenol, 3,5-Dichlorophenol, 2,3-Dimethylphenol, 2,5-Dimethylphenol, 2,6-Dimethylphenol, 3,4-Dimethylphenol, 2,5-Dinitrophenol, 2-Nitrophenol, 3-Nitrophenol, 2,3,4,5-Tetrachlorophenol, 2,3,5,6-Tetrachlorophenol, 2,3,4-Trichlorophenol, 2,3,5-Trichlorophenol, 2,3,6-Trichlorophenol | 59-50-7, 95-57-, 120-83-2, 87-65-0, 105-67-9 , 51-28-5, 88-85-7, 534-52-1 , 95-48-7, 108-39-4, 106-44-5, 100-02-7, 87-86-5, 108-95-2, 58-90-2, 95-95-4, 88-06-2, 615-74-7, 1570-64-5, 108-43-0, 106-48-9, 131-89-5, 576-24-9, 583-78-8, 95-77-2, 591-35-5, 526-75-0, 95-87-4, 576-26-1, 95-65-8, 329-71-5, 88-75-5, 554-84-7, 4901-51-3, 935-95-5, 15950-66-0, 933-78-8, 933-75-5 | Gas chromatography (GC) | sample extracts | Feb. 2007 |
8061A | Phthalate Esters by Gas Chromatography with Electron Capture Detection (GC/ECD) | Determinative | phthalate esters: Benzyl benzoate (Int. Std.), Bis(2-ethylhexyl) phthalate, Butyl benzyl phthalate, Di-n-butyl phthalate, Diethyl phthalate, Dimethyl phthalate, Di-n-octyl phthalate, Bis(2-n-butoxyethyl) phthalate, Bis(2-ethoxyethyl) phthalate, Bis(2-methoxyethyl) phthalate, Bis(4-methyl-2-pentyl) phthalate, Diamyl phthalate, Dicyclohexyl phthalate, Dihexyl phthalate, Diisobutyl phthalate, Dinonyl phthalate, Hexyl 2-ethylhexyl phthalate | 120-51-4, 117-81-7, 85-68-7, 84-74-2, 84-66-2, 131-11-3, 117-84-0, 117-83-9, 605-54-9, 117-82-8, 146-50-9, 131-18-0, 84-61-7, 84-75-3, 84-69-5, 84-76-4, 75673-16-4 | Gas chromatography (GC) with electron capture detection (ECD) | groundwater, leachate, soil, sludge, sediment | Dec. 1996 |
8070A | Nitrosamines by Gas Chromatography | Determinative | nitrosamines: N-Nitrosodimethylamine, N-Nitrosodiphenylamine, N-Nitrosodi-n-propylamine, | 62-75-9, 86-30-6, 621-64-7 | Gas chromatography (GC) | groundwater, municipal discharge, industrial discharge, soils, sediments, sludges | Dec. 1996 |
8081B | Organochlorine Pesticides by Gas Chromatography | Determinative | organochlorine pesticides: Aldrin, ?-BHC, ?-BHC, ?-BHC (Lindane), ?-BHC, cis-Chlordane, trans-Chlordane, Chlordane -- not otherwise specified (n.o.s.), Chlorobenzilate, 1,2-Dibromo-3-chloropropane (DBCP), 4,4'-DDD, 4,4'-DDE, 4,4'-DDT, Diallate, Dieldrin, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin aldehyde, Endrin ketone, Heptachlor, Heptachlor epoxide, Hexachlorobenzene, Hexachlorocyclopentadiene, Isodrin, Methoxychlor, Toxaphene | 309-00-2, 319-84-6, 319-85-7, 58-89-9, 319-86-8, 5103-71-9, 5103-74-2, 57-74-9, 510-15-6, 96-12-8, 72-54-8, 72-55-9, 50-29-3, 2303-16-4, 60-57-1, 959-98-8, 33213-65-9, 1031-07-8, 72-20-8, 7421-93-4, 53494-70-5, 76-44-8, 1024-57-3, 118-74-1, 77-47-4, 465-73-6, 72-43-5, 8001-35-2 | Gas chromatography (GC) with electron capture detection (ECD) or electrolytic conductivity detection (ELCD) | solid matrices, liquid matrices | Feb. 2007 |
8082A | Polychlorinated Biphenyls (PCBs) by Gas Chromatography | Determinative | Polychlorinated Biphenyl (PCB) Aroclors and congeners: Aroclor 1016, aroclor 1221, aroclor 1232, aroclor 1242, aroclor 1248, aroclor 1252, aroclor 1260, 2-Chlorobiphenyl, 2,3-Dichlorobiphenyl, 2,2',5-Trichlorobiphenyl, 2,4',5-Trichlorobiphenyl, 2,2',3,5'-Tetrachlorobiphenyl, 2,2',5,5'-Tetrachlorobiphenyl, 2,3',4,4'-Tetrachlorobiphenyl, 2,2',3,4,5'-Pentachlorobiphenyl, 2,2',4,5,5'-Pentachlorobiphenyl, 2,3,3',4',6-Pentachlorobiphenyl, 2,2',3,4,4',5'-Hexachlorobiphenyl, 2,2',3,4,5,5'-Hexachlorobiphenyl, 2,2',3,5,5',6-Hexachlorobiphenyl, 2,2',4,4',5,5'-Hexachlorobiphenyl, 2,2',3,3',4,4',5-Heptachlorobiphenyl, 2,2',3,4,4',5,5'-Heptachlorobiphenyl, 2,2',3,4,4',5',6-Heptachlorobiphenyl, 2,2',3,4',5,5',6-Heptachlorobiphenyl, 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl | 12674-11-2, 11104-28-2, 11141-16-5, 53469-21-9, 12672-29-6, 11097-69-1, 11096-82-5, 2051-60-7, 16605-91-7, 37680-65-2, 16606-02-3, 41464-39-5, 35693-99-3, 32598-10-0, 38380-02-8, 37680-73-2, 38380-03-9, 35065-28-2, 52712-04-6, 52663-63-5, 35065-27-1, 35065-30-6, 35065-29-3, 52663-69-1, 52663-68-0, 40186-72-9 | Gas chromatography (GC) | solid matrices, aqueous matrices, tissue, oils, wipe samples | Feb. 2007 |
8085 | Compound-independent Elemental Quantitation of Pesticides by Gas Chromatography with Atomic Emission Detection (GC/AED) | Determinative | pesticides: Abate (Temephos), Acifluorfen, Alachlor, Aldrin, Ametryn, Atraton, Atrazine, Azinphos ethyl (Ethyl guthion), Azinphos methyl (Guthion), Benfluralin, alpha-BHC, beta-BHC, delta-BHC, gamma-BHC (Lindane), Bromacil, Bromoxynil (Brominal), Butachlor, Butylate, Captafol, Captan, Carbophenothion, Carboxin, trans-Chlordane, Chlorpropham, Chlorpyrifos, Chlorthalonil (Daconil), Coumaphos, Cyanazine, Cycloate, 2,4-D acid, 2,4-DB acid, DCPA (Dacthal), 2,4'-DDD, 4,4'-DDD, 2,4'-DDE, 4,4'-DDE, 2,4'-DDT, 4,4'-DDT, DEF (Butifos), Demeton-O, Demeton-S, Diallate, Diazinon, Dicamba, Dichlobenil (Casoron), 3,5-Dichlorobenzoic acid, Dichlorprop, Dichlorvos (DDVP), Diclofol (Kelthane), Diclofop-methyl, Dieldrin, Dimethoate, Dinoseb, Dioxathion, Diphenamid, Disulfoton (Disyston), Diuron, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin aldehyde, Endrin ketone, EPN, Eptam (EPTC), Ethalfluralin (Sonalan), Ethion, Ethoprop, Fenamiphos, Fenarimol, Fenitrothion, Fensulfothion, Fenthion, Fluridone, Fonofos, Gardona (Tetrachlovinphos), Heptachlor, Heptachlor epoxide, Hexachlorobenzene, Hexachlorocyclopentadiene, Hexazinone, Imidan (Phosmet), Ioxynil, Malathion, MCPA acid, MCPP acid, Merphos, Metalaxyl, Methoxychlor, Methyl chlorpyrifos, Methyl paraoxon, Methyl parathion, Metolachlor, Metribuzin, Mevinphos, MGK-264, Mirex, Molinate, Napropamide, Norflurazon, 4-Nitrophenol, Oxyfluorfen, Parathion, Pebulate, Pendimethalin, Pentachlorophenol (PCP), Phorate, Phosphamidon, Picloram, Profluralin, Prometon (Pramitol 5p), Prometryn, Pronamide (Kerb), Propachlor (Ramrod), Propargite (S-181), Propazine, Propetamidophos, Ronnel, Silvex (2,4,5-TP), Simazine, Sulfotepp, Sulprofos (Bolstar), 2,4,5-T acid, 2,4,5-TB, Tebuthiuron, Terbacil, Terbutryn (Igran), 2,3,4,5-Tetrachlorophenol, 2,3,4,6-Tetrachlorophenol, Triademefon, Triallate, Triclopyr (Garlon), 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol, Trifluralin (Treflan), Vernolate | 3383-96-13, 62476-59-9, 15972-60-8, 309-00-2, 834-12-8, 1610-17-9, 1912-24-9, 642-71-9, 86-50-0, 1861-40-1, 319-84-6, 319-85-7, 319-86-8, 58-89-9, 314-40-9, 1689-84-5, 23184-66-9, 2008-41-5, 2425-06-1, 133-06-2, 786-19-6, 5234-68-5, 5103-74-2, 101-21-3, 5598-13-0, 1897-45-6, 56-72-4, 21725-46-2, 1134-23-2, 94-75-7, 94-82-6, 2136-79-0, 53-19-0, 72-54-8, 3424-82-6, 72-55-9, 789-02-6, 50-29-3, 78-48-8, 298-02-3, 126-75-0, 2303-16-4, 333-41-5, 1918-00-9, 1194-65-6, 51-36-5, 120-36-5, 62-73-7, 115-32-2, 51338-27-3, 60-57-1, 60-51-5, 88-85-7, 78-34-2, 957-51-7, 298-04-4, 330-54-1, 959-98-8, 33213-65-9, 1031-07-8, 72-20-8, 7421-93-4, 53494-70-5, 2104-64-5, 759-94-4, 55283-68-6, 563-12-2, 13194-48-4, 22224-92-6, 60168-88-9, 122-14-5, 115-90-2, 55-38-9, 59756-60-4, 944-22-9, 961-11-5, 76-44-8, 1024-57-3, 118-74-1, 77-47-4, 51235-04-2, 732-11-6, 1689-83-4, 121-75-5, 94-74-6, 7085-19-0, 150-50-5, 57837-19-1, 72-43-5, 5598-13-0, 311-45-5, 298-00-0, 51218-45-2, 21087-64-9, 7786-34-7, 113-48-4, 2385-85-5, 2212-67-1, 15299-99-7, 27314-13-2, 100-02-7, 42874-03-3, 56-38-2, 1114-71-2, 40487-42-1, 87-86-5, 298-02-2, 297-99-4, 1918-02-1, 26399-36-0, 1610-18-0, 7287-19-6, 23950-58-5, 1918-16-7, 2312-35-8, 139-40-2, 31218-83-4, 299-84-3, 93-76-5, 122-34-9, 3689-24-5, 35400-43-2, 94-82-6, 93-80-1, 34014-18-1, 5902-51-2, 886-50-0, 4901-51-3, 58-90-2, 43121-43-3, 2303-17-5, 55335-06-3, 95-95-4, 88-06-2, 1582-09-8, 1929-77-7 | Gas Chromatography with Atomic Emission Detection (GC/AED) | liquid matrices, solid matrices | Feb. 2007 |
8091 | Nitroaromatics and Cyclic Ketones by Gas Chromatography | Determinative | 1,4-Dinitrobenzene, 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, 1,4-Naphthoquinone, Nitrobenzene, Pentachloronitrobenzene, Benefin, Butralin, 1-Chloro-2,4-dinitrobenzene, 1-Chloro-3,4-dinitrobenzene, 1-Chloro-2-nitrobenzene, 1-Chloro-4-nitrobenzene, 2-Chloro-6-nitrotoluene, 4-Chloro-2-nitrotoluene, 4-Chloro-3-nitrotoluene, 2,3-Dichloronitrobenzene, 2,4-Dichloronitrobenzene, 3,5-Dichloronitrobenzene, 3,4-Dichloronitrobenzene, 2,5-Dichloronitrobenzene, Dinitramine, 1,2-Dinitrobenzene, 1,3-Dinitrobenzene, Isopropalin, 1,2-Naphthoquinone, 2-Nitrotoluene, 3-Nitrotoluene, 4-Nitrotoluene, Penoxalin (Pendimethalin), Profluralin, 2,3,4,5-Tetrachloronitrobenzene, 2,3,5,6-Tetrachloronitrobenzene, 1,2,3-Trichloro-4-nitrobenzene, 1,2,4-Trichloro-5-nitrobenzene, 2,4,6-Trichloronitrobenzene, Trifluralin | 100-25-4, 121-14-2, 606-20-2, 130-15-4, 98-95-3, 82-68-8, 1861-40-1, 33629-47-9, 97-00-7, 610-40-2, 88-73-3, 100-00-5, 83-42-1, 89-59-8, 89-60-1, 3209-22-1, 611-06-3, 618-62-2, 99-54-7, 89-61-2, 29091-05-2, 528-29-0, 99-65-0, 33820-53-0, 524-42-5, 88-72-2, 99-08-1, 99-99-0, 40487-42-1, 26399-36-0, 879-39-0, 117-18-0, 17700-09-3, 89-69-0, 18708-70-8, 1582-09-8 | Gas chromatography (GC) with electron capture detection (ECD) or nitrogen-phosphorus detection (NPD) | water, soil, waste | Dec. 1996 |
8095 | Explosives by Gas Chromatography | Determinative | explosives: 2-Amino-4,6-dinitrotoluene, 4-Amino-2,6-dinitrotoluene, 3,5-Dinitroaniline, 1,3-Dinitrobenzene, 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, Hexahydro-1,3,5-trinitro-1,3,5-triazine, Nitrobenzene, Nitroglycerine, 2-Nitrotoluene, 3-Nitrotoluene, 4-Nitrotoluene, Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine, Pentaerythritoltetranitrate, 1,3,5-Trinitrobenzene, 2,4,6-Trinitrophenylmethylnitramine, 2,4,6-Trinitrotoluene | 35572-78-2, 1946-51-0, 618-87-1, 99-65-0, 121-14-2, 606-20-2, 121-82-4, 98-95-3, 55-63-0, 88-72-2, 99-08-1, 99-99-0, 2691-41-0, 78-11-5, 99-35-4, 479-45-8, 118-96-7 | Gas chromatography (GC) with electron capture detection (ECD) | water, soil | Feb. 2007 |
8100 | Polynuclear Aromatic Hydrocarbons | Determinative | Polynuclear Aromatic Hydrocarbons (PAHs): Acenaphthene, acenaphthylene, anthracene, benz(a)anthracene, Benzo(a)pyrene, benzo(b)fluoranthene, benzo(j)fluoranthene, benzo(k)fluoranthene, benzo(g,h,i)perylene, chrysene, dibenzo(a,h)acridine, Dibenz(a,j)acridine, Dibenzo(a,h)anthracene, 7H-Dibenzo(c,g)carbazole, Dibenzo(a,e)pyrene, ibenzo(a,h)pyrene, Dibenzo(a,i)pyrene, Fluoranthene, Fluorene, Indeno(1,2,3-cd)pyrene, 3-Methylcholanthrene, Naphthalene, Phenanthrene, Pyrene | 83-32-9, 208-96-8, 120-12-7, 56-55-3, 50-32-8, 205-99-2, 205-82-3, 207-08-9, 191-24-2, 218-01-9, 226-36-8, 224-42-0, 53-70-3, 194-59-2, 192-65-4, 189-64-0, 189-55-9, 206-44-0, 86-73-7, 193-39-5, 56-49-5, 91-20-3, 85-01-8, 129-00-0 | Gas chromatography (GC) | waste | Sept. 1986 |
8111 | Haloethers by Gas Chromatography | Determinative | haloethers: Bis(2-chloroethoxy)methane, Bis(2-chloroethyl) ether, Bis(2-chloro-1-methylethyl)ether, 4-Chlorophenyl phenyl ether, 4-Bromophenyl phenyl ether, 2-Chlorophenyl 4-nitrophenyl ether, 3-Chlorophenyl 4-nitrophenyl ether, 4-Chlorophenyl 4-nitrophenyl ether, 2,4-Dibromophenyl 4-nitrophenyl ether, 2,4-Dichlorophenyl 3-methyl-4-nitrophenyl ether, 2,6-Dichlorophenyl 4-nitrophenyl ether, 3,5-Dichlorophenyl 4-nitrophenyl ether, 2,5-Dichlorophenyl 4-nitrophenyl ether, 2,4-Dichlorophenyl 4-nitrophenyl ether, 2,3-Dichlorophenyl 4-nitrophenyl ether, 3,4-Dichlorophenyl 4-nitrophenyl ether, 4-Nitrophenyl phenyl ether, 2,4,6-Trichlorophenyl 4-nitrophenyl ether, 2,3,6-Trichlorophenyl 4-nitrophenyl ether, 2,3,5-Trichlorophenyl 4-nitrophenyl ether, 2,4,5-Trichlorophenyl 4-nitrophenyl ether, 3,4,5-Trichlorophenyl 4-nitrophenyl ether, 2,3,4-Trichlorophenyl 4-nitrophenyl ether | 111-91-1, 111-44-4, 108-60-1, 7005-72-3, 101-55-3, 209-61-4, 2303-23-3, 1836-74-4, 2671-93-4, 42488-57-3, 2093-28-9, 391-48-7, 1836-75-5, 82239-20-1, 22532-80-5, 620-88-2, 1836-77-7, 22532-68-9 | Gas chromatography (GC) | water, soil, waste | July 2014 |
8121 | Chlorinated Hydrocarbons by Gas Chromatography: Capillary Column Technique | Determinative | chlorinated hydrocarbons: Benzal chloride, Benzotrichloride, Benzyl chloride, 2-Chloronaphthalene, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, Hexachlorobenzene, Hexachlorobutadiene, ?-Hexachlorocyclohexane ( ?-BHC), ?-Hexachlorocyclohexane ( ? -BHC), ?-Hexachlorocyclohexane ( ?-BHC), ? -Hexachlorocyclohexane ( ?-BHC), Hexachlorocyclopentadiene, Hexachloroethane, Pentachlorobenzene, 1,2,3,4-Tetrachlorobenzene, 1,2,4,5-Tetrachlorobenzene, 1,2,3,5-Tetrachlorobenzene, 1,2,4-Trichlorobenzene, 1,2,3-Trichlorobenzene, 1,3,5-Trichlorobenzene | 98-87-3, 98-07-7, 100-44-7, 91-58-7, 95-50-1, 541-73-1, 106-46-1, 118-74-1, 87-68-3, 319-84-6, 319-85-7, 58-89-9, 319-86-8, 77-47-4, 67-72-1, 608-93-5, 634-66-2, 95-94-2, 634-90-2, 120-82-1, 108-70-3 | Gas chromatography (GC) : capillary column | water, soil, waste | Sept. 1986 |
8131 | Aniline and Selected Derivatives by Gas Chromatography | Determinative | Aniline, 4-Bromoaniline, 2-Bromo-6-chloro-4-nitroaniline, 2-Bromo-4,6-dinitroaniline, 2-Chloroaniline, 3-Chloroaniline, 4-Chloroaniline , 2-Chloro-4,6-dinitroaniline, 2-Chloro-4-nitroaniline, 4-Chloro-2-nitroaniline, 2,6-Dibromo-4-nitroaniline, 3,4-Dichloroaniline, 2,6-Dichloro-4-nitroaniline, 2,4-Dinitroaniline, 2-Nitroaniline, 3-Nitroaniline, 4-Nitroaniline, 2,4,6-Trichloroaniline, 2,4,5-Trichloroaniline | 62-53-3, 106-40-1, 99-29-6, 1817-73-8, 95-51-2, 108-42-9, 106-47-8, 3531-19-9, 121-87-9, 89-63-4, 827-94-1, 95-76-1, 99-30-9, 97-02-9, 88-74-4, 99-09-2, 100-01-6, 634-93-5, 636-30-6 | Gas chromatography (GC) | aqueous matrices, sample and waste extracts | Dec. 1996 |
8141B | Organophosphorus Compounds by Gas Chromatography | Determinative | Organophosphorus compounds: Asponb, Azinphos-ethyla, Azinphos-methyl, Bolstar (Sulprofos), Carbophenothiona, Chlorfenvinphosa, Chlorpyrifos, Chlorpyrifos methyl, Coumaphos, Crotoxyphosa, Demeton-Oc, Demeton-Sc, Diazinon, Dichlorofenthion, Dichlorvos (DDVP), Dicrotophosa, Dimethoate, Dioxathion, Disulfoton, EPN, Ethion, Ethoprop, Famphur, Fenitrothion, Fensulfothion, Fenthion, Fonophos, Leptophos, Malathion, Merphos, Mevinphos, Monocrotophos, Naled, Parathion, ethyl, Parathion, methyl, Phorate, Phosmet, Phosphamidon, Ronnel, Stirophos (Tetrachlorvinphos, Gardona), Sulfotepp, Tetraethyl pyrophosphate (TEPP), Terbufos, Thionazin (Zinophos), Tokuthion (Prothiofos), Trichlorfon, Trichloronate, Hexamethyl phosphoramide (HMPA), Tri-o-cresyl phosphate (TOCP), Atrazinea, Simazinea, Bendiocarb, Butylate, EPTC, Methiocarb, Molinate, Pebulate, o-Phenylenediamine, Propham, Prosulfocarb, Triallate | 3244-90-4, 2642-71-9, 86-50-0, 35400-43-2, 786-19-6, 470-90-6, 2921-88-2, 5598-13-0, 56-72-4, 7700-17-6, 8065-48-3, 8065-48-3, 333-41-5, 97-17-6, 62-73-7, 141-66-2, 60-51-5, 78-34-2, 298-04-4, 2104-64-5, 563-12-2, 13194-48-4, 52-85-7, 122-14-5, 115-90-2, 55-38-9, 944-22-9, 21609-90-5, 121-75-5, 150-50-5, 7786-34-7, 6923-22-4, 300-76-5, 56-38-2, 298-00-0, 298-02-2, 732-11-6, 13171-21-6, 299-84-3, 22248-79-9, 3689-24-5, 107-49-3, 13071-79-9, 297-97-2, 34643-46-4, 52-68-6, 327-98-0, 680-31-9, 78-30-8, 1912-24-9, 122-34-9, 22781-23-3, 2008-41-5, 759-94-4, 2032-65-7, 2212-67-1, 1114-71-2, 95-54-5, 122-42-9, 52888-80-9, 2303-17-5 | Gas chromatography (GC) with flame photometric detection (FPD) or nitrogen-phosphorus detection (NPD) | liquids, solids | Feb. 2007 |
8151A | Chlorinated Herbicides by GC Using Methylation or Pentafluorobenzylation Derivatization | Determinative | chlorinated acid herbicides: 2,4-D, 2,4-DB, 2,4,5-TP (Silvex), 2,4,5-T, Dalapon, Dicamba, Dichloroprop, Dinoseb, MCPA, MCPP, 4-Nitrophenol, Pentachlorophenol, Acifluorfen, Bentazon, Chloramben, DCPA diacid, 3,5-Dichlorobenzoic acid, 5-Hydroxydicamba, Picloram | 94-75-7, 94-82-6, 93-72-1, 93-76-5, 75-99-0, 1918-00-9, 120-36-5, 88-85-7, 94-74-6, 93-65-2, 100-02-1, 87-86-5, 50594-66-6, 25057-89-0, 133-90-4, 2136-79-0, 51-36-5, 7600-50-2, 1918-02-1 | Gas chromatography (GC) with electron capture detection (ECD) | water, soils, wastes | Dec. 1996 |
8260D | Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) | Determinative | Volatile Organic Compounds (VOCs): Acetone, Acetonitrile, Acrolein (Propenal), Acrylonitrile, Allyl alcohol, Allyl chloride, t-Amyl ethyl ether (TAEE, 4,4-Dimethyl-3-oxahexane), t-Amul methyl ether (TAME), Benzene, Benzyl chloride, Bromoacetone, Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, n-Butanol, 2-Butanone (MEK), t-Butyl alcohol, n-Butylbenzene, sec-Butylbenzene, tert-Butylbenzene, Carbon disulfide, Carbon tetrachloride, Chloral hydrate, Chlorobenzene, 1-Chlorobutane, Chlorodibromomethane, Chloroethane, 2-Chloroethanol, 2-Chloroethyl vinyl ether, Chloroform, 1-Chlorohexane, Chloromethane, Chloroprene, 2-Chlorotoluene, 4-Chlorotoluene, Crotonaldehyde, Cyclohexane, 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, cis-1,4-Dichloro-2-butene, trans-1,4-Dichloro-2-butene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene (Vinylidene chloride), cis-1,2-Dichloroethene, trans-1,2-Dichloroethene, 1,3-Dichloropropane, 1,2-Dichloropropane, 2,2-Dichloropropane, 1,3-Dichloro-2-propanol, 1,1-Dichloropropene, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, 1,2,3,4-Diepoxybutane, Diethyl ether, Diisopropyl ether (DIPE), 1,4-Dioxane, Epichlorohydrin, Ethanol, Ethyl acetate, Ethylbenzene, Ethylene oxide, Ethyl methacrylate, Ethyl-t-butyl-ether (ETBE), Hexachlorobutadiene, Hexachloroethane, 2-Hexanone, Iodomethane (Methyl iodide), Isobutyl alcohol, Isopropylbenzene, p-Isopropyltoluene, Malononitrile, Methacrylonitrile, Methanol, Methyl acetate, Methyl acrylate, Methyl methacrylate, Methyl-tert-butyl ether (MTBE), Methylcyclohexane, Methylene chloride (DCM), 4-Methyl-2-pentanone (MIBK), Naphthalene, Nitrobenzene (NB), 2-Nitropropane, N-Nitroso-di-n-butylamine (N-Nitrosodibutylamine), Paraldehyde, Pentachloroethane, Pentafluorobenzene, 2-Pentanone, 2-Picoline, 1-Propanol, 2-Propanol, Propargyl alcohol, $-Propiolactone, Propionitrile (ethyl cyanide), n-Propylamine, n-Propylbenzene, Pyridine, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, o-Toluidine, 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene (Trichloroethylene), Trichlorofluoromethane, 1,1,2-Trichlorotrifluoroethane, 1,1,1-Trichlorotrifluoroethane, 1,2,3-Trichloropropane, 1,2,3-Trimethylbenzene, 1,2,4-Trimethylbenzene, 1,3,4-Trimethylbenzene, Vinyl acetate, Vinyl chloride, o-Xylene, m-Xylene, p-Xylene | 67-64-1, 75-05-8, 107-02-8, 107-13-1, 107-18-6, 107-05-1, 919-94-8, 994-05-8, 71-43-2, 100-44-7, 598-31-2, 108-86-1, 74-97-5, 75-27-4, 75-25-2, 74-83-9, 71-36-3, 78-93-3, 75-65-0, 104-51-8, 135-98-8, 98-06-6, 75-15-0, 56-23-5, 302-17-0, 108-90-7, 109-69-3, 124-48-1, 75-00-3, 107-07-3, 110-75-8, 67-66-3, 544-10-5, 74-87-3, 126-99-8, 95-49-8, 106-43-4, 4170-30-3, 110-82-7, 96-12-8, 106-93-4, 74-95-3, 95-50-1, 541-73-1, 106-46-7, 1476-11-5, 110-57-6, 75-71-8, 75-34-3, 107-06-2, 75-35-4, 156-59-2, 156-60-5, 142-28-9, 78-87-5, 594-20-7, 96-23-1, 563-58-6, 10061-01-5, 10061-02-6, 1464-53-5, 60-29-7, 108-20-3, 123-91-1, 106-89-8, 64-17-5, 141-78-6, 100-41-4, 75-21-8, 97-63-2, 637-92-3, 87-68-3, 67-72-1, 591-78-6, 74-88-4, 78-83-1, 98-82-8, 99-87-6, 109-77-3, 126-98-7, 67-56-1, 79-20-9, 96-33-3, 80-62-6, 1634-04-4, 108-87-2, 75-09-2, 108-10-1, 91-20-3, 98-95-3, 79-46-9, 924-16-3, 123-63-7, 76-01-7, 363-72-4, 107-87-9, 109-06-8, 71-23-8, 67-63-0, 107-19-7, 57-57-8, 107-12-0, 107-10-8, 103-65-1, 110-86-1, 100-42-5, 630-20-6, 79-34-5, 127-18-4, 108-88-3, 2037-26-5, 95-53-4, 87-61-6, 120-82-1, 71-55-6, 79-00-5, 79-01-6, 76-13-1, 354-58-5, 75-69-4, 96-18-4, 526-73-8, 95-63-6, 108-67-8, 108-05-4, 75-01-4, 95-47-6, 108-38-3, 106-42-3 | Gas Chromatography/ Mass Spectrometry (GC/MS) | air sampling trapping, ground water, surface water, aqueous sludges, caustic liquors, acid liquors, waste solvents, oily wastes, mousses, tars, fibrous wastes, polymeric emulsions, filter cakes, spent carbons, spent catalysts, soils, sediments | July 2018 |
8261 | Volatile Organic Compounds by Vacuum Distillation in Combination with Gas Chromatography/Mass Spectrometry (VD/GC/MS) | Determinative | volatile organic compounds (VOCs): Acetone, Acetonitrile, Acetophenone, Acrolein, Acrylonitrile, Allyl chloride, t-Amyl ethyl ether (TAEE, 4,4-Dimethyl-3-oxahexane), t-Amyl methyl ether (TAME), Aniline, Benzene, Bromochloromethane, Bromodichloromethane, Bromomethane, 2-Butanone, t-Butyl alcohol (TBA), n-Butylbenzene, sec-Butylbenzene, tert-Butylbenzene, Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, Chloroform, Chloromethane, 2-Chlorotoluene, 4-Chlorotoluene, 1,2-Dibromo-3-chloropropane, Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, cis-1,4-Dichloro-2-butene, trans-1,4-Dichloro-2-butene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, trans-1,2-Dichloroethene, cis-1,2-Dichloroethene, 1,2-Dichloropropane, 1,3-Dichloropropane, 2,2-Dichloropropane, 1,1-Dichloropropene, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, Diethyl ether, Diisopropyl ether (DIPE), 1,4-Dioxane, Ethanol, Ethyl acetate, Ethylbenzene, Ethyl t-butyl ether (ETBE), Ethyl methacrylate, Hexachlorobutadiene, 2-Hexanone, Iodomethane, Isobutyl alcohol, Isopropylbenzene, p-Isopropyltoluene, Methacrylonitrile, Methyl t-butyl ether (MTBE), Methylene chloride, Methyl methacrylate, 1-Methylnaphthalene, 2-Methylnaphthalene, 4-Methyl-2-pentanone (MIBK), Naphthalene, N-Nitrosodibutylamine, N-Nitrosodiethylamine, N-Nitrosodimethylamine, N-Nitrosodi-n-propylamine, N-Nitrosomethylethylamine, Pentachloroethane, 2-Picoline, Propionitrile, n-Propylbenzene, Pyridine, Styrene, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Tetrahydrofuran, Toluene, o-Toluidine, 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, 1,2,4-Trimethylbenzene, 1,3,5-Trimethylbenzene, Vinyl chloride, o-Xylene, m-Xylene, p-Xylene | 67-64-1, 75-05-8, 98-86-2, 107-02-8, 107-13-1, 107-05-1, 919-94-8, 994-05-8, 62-53-3, 71-43-2, 74-97-5, 75-27-4, 75-25-2, 74-83-9, 78-93-3, 75-65-0, 104-51-8, 135-98-8, 98-06-6, 75-15-0, 56-23-5, 108-90-7, 124-48-1, 75-00-3, 67-66-3, 74-87-3, 95-49-8, 106-43-4, 96-12-8, 74-95-3, 95-50-1, 541-73-1, 106-46-7,764-41-0, 110-57-6,75-71-8, 75-34-3, 107-06-2, 75-35-4, 156-60-5, 156-59-2, 78-87-5, 142-28-9, 594-20-7, 563-58-6, 10061-01-5, 10061-02-6, 60-29-7, 108-20-3, 123-91-1, 64-17-5, 141-78-6, 100-41-4, 637-92-3, 97-63-2, 87-68-3, 591-78-6, 74-88-4, 78-83-1, 98-82-8, 99-87-6, 126-98-7, 1634-04-4, 75-09-2, 80-62-6, 90-12-0, 91-57-6, 108-10-1, 91-20-3, 924-16-3, 55-18-5, 62-75-9, 621-64-7, 10595-95-6, 76-01-7, 109-06-8, 107-12-0, 103-65-1, 110-86-1, 100-42-5, 79-34-5, 127-18-4, 109-99-9, 108-88-3, 95-53-4, 87-61-6, 120-82-1, 71-55-6, 79-00-5, 79-01-6, 75-69-4, 96-18-4, 95-63-6, 108-67-8, 75-01-4, 95-47-6, 108-38-3, 106-42-3 | Vacuum Distillation, Gas Chromatography/ Mass Spectrometry (VD/GC/MS) | liquid waste, solid waste, oily waste, tissue | Feb. 2007 |
8270E | Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) | Determinative | semivolatile organics: Acenaphthene, Acenaphthylene, Acetophenone, 2-Acetylaminofluorene, 1-Acetyl-2-thiourea, Aldrin, 2-Aminoanthraquinone, Aminoazobenzene, 4-Aminobiphenyl, 3-Amino-9-ethylcarbazole, Anilazine, Aniline, o-Anisidine, Anthracene, Aramite, Aroclor 1016, Aroclor 1221, Aroclor 1232, Aroclor 1242, Aroclor 1248, Aroclor 1254, Aroclor 1260, Atrazine, Azinphos-methyl (Guthion), Azonbenzene, Barban, Benzaldehyde, Benzidine, Benzoic acid, Benz(a)anthracene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Benzo(g,h,i)perylene, Benzo(a)pyrene, Benzo(e)pyrene, p-Benzoquinone, Benzyl alcohol, alpha-BHC, beta-BHC, delta-BHC, gamma-BHC (Lindane), 1,1'-Biphenyl, Bis(2-chloroethoxy)methane, Bis(2-chloroethyl) ether, Bis(2-chloro-1-methylethyl)ether, Bis(2-ethylhexyl) phthalate, 4-Bromophenyl phenyl ether, Bromoxynil, Butyl benzyl phthalate, Caprolactam, Captafol, Captan, Carbaryl (Sevin), Carbazole, Carbofuran (Furaden), Carbophenothion, Chlordane (NOS), Chlorfenvinphos, 4-Chloroaniline, Chlorobenzilate, 5-Chloro-2-methylaniline, 4-Chloro-3-methylphenol, 3-(Chloromethyl)pyridine hydrochloride, 1-Chloronaphthalene, 2-Chloronaphthalene, 2-Chlorophenol, 4-Chloro-1,2-phenylenediamine, 4-Chloro-1,3-phenylenediamine, 4-Chlorophenyl phenyl ether, Chrysene, Coumaphos, p-Cresidine, Crotoxyphos, 2-Cyclohexyl-4,6-dinitro-phenol, 4,4'-DDD, 4,4'-DDE, 4,4'-DDT, Demeton-O, Demeton-S, Diallate (cis or trans), 2,4-Diaminotoluene, Dibenz(a,j)acridine, Dibenz(a,h)anthracene, Dibenzofuran, Dibenzo(a,e)pyrene, 1,2-Dibromo-3-chloropropane, Di-n-butyl phthalate, Dichlone, 1,2-Dichlorobenzene. 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 3,3'-Dichlorobenzidine, 2,4-Dichlorophenol, 2,6-Dichlorophenol, Dichlorovos, Dicrotophos, Dieldrin, Diethyl phthalate, Diethylstilbestrol, Diethyl sulfate, Dimethoate, 3,3'-Dimethoxybenzidine, Dimethylaminoazobenzene, 7,12-Dimethylbenz(a)-anthracene, 3,3'-Dimethylbenzidine, alpha,alpha-Dimethylphenethylamine, 2,4-Dimethylphenol, Dimethyl phthalate, 1,2-Dinitrobenzene, 1,3-Dinitrobenzene (1,3-DNB), 1,4-Dinitrobenzene, 4,6-Dinitro-2-methylphenol, 2,4-Dinitrophenol, 2,4-Dinitrotoluene (2,4-DNT), 2,6-Dinitrotoluene (2,6-DNT), Dinocap, Dinoseb (DNBP), 1,4-Dioxane, Diphenylamine, 5,5-Diphenylhydantoin, 1,2-Diphenylhydrazine, Di-n-octyl phthalate, Disulfoton, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin aldehyde, Endrin ketone, EPN, Ethion, Ethyl carbamate, Ethyl methanesulfonate, Famphur, Fensulfothion, Fenthion, Fluchloralin, Fluoranthene, Fluorene, 2-Fluorobiphenyl (surr), 2-Fluorophenol (surr), Heptachlor, Heptachlor epoxide, Hexachlorobenzene, Hexachlorobutadiene, Hexachlorocyclopentadiene, Hexachloroethane, Hexachlorophene, Hexachloropropene, Hexamethylphosphoramide, Hydroquinone, Indeno(1,2,3-cd)pyrene, Isodrin, Isophorone, Isosafrole, Kepone, Leptophos, Malathion , Maleic anhydride, Mestranol, Methapyrilene, Methoxychlor, 3-Methylcholanthrene, 4,4'-Methylenebis (2-chloroaniline), 4,4'-Methylenebis(N,N-dimethylaniline), 1-Methylnaphthalene, 2-Methylnaphthalene, Methyl parathion, 2-Methylphenol, 3-Methylphenol, 4-Methylphenol, Mevinphos, Mexacarbate, Mirex, Monocrotophos, Naled, Naphthalene, 1,4-Naphthoquinone, 1-Naphthylamine, 2-Naphthylamine, Nicotine, 5-Nitroacenaphthene, 2-Nitroaniline, 3-Nitroaniline, 4-Nitroaniline, 5-Nitro-o-anisidine, Nitrobenzene, 4-Nitrobiphenyl, Nitrofen, 2-Nitrophenol, 4-Nitrophenol, 4-Nitroquinoline-1-oxide, N-Nitrosodi-n-butylamine, N-Nitrosodiethylamine, N-Nitrosodimethylamine, N-Nitrosodiphenylamine, N-Nitrosodi-n-propylamine, N-Nitrosomethylethylamine, N-Nitrosomorpholine, N-Nitrosopiperidine, N-Nitrosopyrrolidine, 5-Nitro-o-toluidine, Octamethyl pyrophosphoramide, 4,4'-Oxydianiline, Parathion, Pentachlorobenzene, Pentachloronitrobenzene, Pentachlorophenol, Perylene, Phenacetin, Phenanthrene, Phenobarbital, Phenol, 1,4-Phenylenediamine, Phorate, Phosalone, Phosmet, Phosphamidon, Phthalic anhydride, 2-Picoline (2-Methylpyridine), Piperonyl sulfoxide, Pronamide, Propylthiouracil, Pyrene, Pyridine, Resorcinol, Safrole, Strychnine, Sulfallate, Terbufos, 1,2,4,5-Tetrachlorobenzene, 2,3,4,6-Tetrachlorophenol, Tetrachlorvinphos, Tetraethyl dithiopyrophosphate, Tetraethyl pyrophosphate, Thionazine, Thiophenol (Benzenethiol), 2,4-Toluene diisocyanate, o-Toluidine, Toxaphene, 1,2,4-Trichlorobenzene, 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol, Trifluralin, 2,4,5-Trimethylaniline, Trimethyl phosphate, 1,3,5-Trinitrobenzene, Tris(2,3-dibromopropyl) phosphate, Tri-p-tolyl phosphate, O,O,O-Triethyl phosphorothioate | 83-32-9, 208-96-8, 98-86-2, 53-96-3, 591-08-2, 309-00-2, 117-79-3, 60-09-3, 92-67-1, 132-32-1, 101-05-3, 62-53-3, 90-04-0, 120-12-7, 140-57-8, 12674-11-2,11104-28-2, 11141-16-5, 53469-21-9, 12672-29-6, 11097-69-1, 11096-82-5, 1912-24-9, 86-50-0, 103-33-3, 101-27-9, 100-52-7, 92-87-5, 65-85-0, 56-55-3, 205-99-2, 207-08-9, 191-24-2, 50-32-8, 192-97-2, 106-51-4,100-51-6, 319-84-6,319-85-7, 319-86-8, 58-89-9, 92-52-4, 111-91-1, 111-44-4,39638-32-9, 117-81-7, 101-55-3, 1689-84-5, 85-68-7, 105-60-2, 2425-06-1, 133-06-2, 63-25-2, 86-74-8, 1563-66-2, 786-19-6, 57-74-9, 470-90-6, 106-47-8, 510-15-6, 95-79-4, 59-50-7, 6959-48-4, 90-13-1, 91-58-7, 95-57-8, 95-83-0, 5131-60-2,7005-72-3, 218-01-9, 56-72-4, 120-71-8, 7700-17-6, 131-89-5, 72-54-8, 72-55-9, 50-29-3, 298-03-3, 126-75-0, 2303-16-4, 95-80-7, 224-42-0, 53-70-3, 132-64-9, 192-65-4, 96-12-8, 84-74-2, 117-80-6, 95-50-1, 541-73-1, 106-46-7, 91-94-1, 120-83-2 , 87-65-0, 62-73-7, 141-66-2, 60-57-1 , 84-66-2, 56-53-1, 64-67-5, 60-51-5, 119-90-4, 60-11-7, 57-97-6, 119-93-7, 122-09-8, 105-67-9, 131-11-3, 528-29-0, 99-65-0, 100-25-4, 534-52-1, 51-28-5, 121-14-2, 606-20-2, 39300-45-3, 88-85-7, 123-91-1, 122-39-4,57-41-0, 122-66-7, 117-84-0, 298-04-4, 959-98-8, 33213-65-9, 1031-07-8, 72-20-8, 7421-93-4, 53494-70-5, 2104-64-5, 563-12-2, 51-79-6, 62-50-0, 52-85-7, 115-90-2, 55-38-9, 33245-39-5, 206-44-0, 86-73-7, 321-60-8, 367-12-4, 76-44-8, 1024-57-3 , 118-74-1, 87-68-3, 77-47-4, 67-72-1, 70-30-4, 1888-71-7, 680-31-9, 123-31-9, 193-39-5, 465-73-6, 78-59-1, 120-58-1, 143-50-0, 55-38-9, 33245-39-5, 206-44-0, 86-73-7, 321-60-8, 367-12-4, 76-44-8, 1024-57-3, 118-74-1, 87-68-3, 77-47-4, 67-72-1,70-30-4, 1888-71-7, 680-31-9, 123-31-9, 193-39-5, 465-73-6, 78-59-1, 120-58-1, 143-50-0, 21609-90-5, 121-75-5, 108-31-6, 72-43-5, 66-27-3, 298-00-0, 56-49-5, 101-14-4, 101-61-1, 90-12-0, 91-57-6, 95-48-7, 108-39-4, 106-44-5, 7786-34-7, 315-18-4, 2385-85-5, 6923-22-4, 300-76-5, 91-20-3, 130-15-4, 134-32-7, 91-59-8, 54-11-5, 602-87-9, 88-74-4, 99-09-2, 100-01-6, 99-59-2, 98-95-3, 92-93-3, 1836-75-5, 88-75-5, 100-02-7, 99-55-8, 56-57-5, 924-16-3, 55-18-5, 62-75-9, 86-30-6, 621-64-7, 10595-95-6, 59-89-2, 100-75-4, 930-55-2, 152-16-9, 101-80-4, 56-38-2, 608-93-5, 82-68-8, 87-86-5, 198-55-0, 62-44-2, 85-01-8, 50-06-6, 108-95-2, 106-50-3, 298-02-2, 2310-17-0, 732-11-6, 13171-21-6, 85-44-9, 109-06-8, 120-62-7, 23950-58-5, 51-52-5, 129-00-0, 110-86-1, 108-46-3, 94-59-7, 57-24-9, 95-06-7, 13071-79-9, 95-94-3, 58-90-2, 961-11-5, 3689-24-5, 107-49-3, 297-97-2, 108-98-5, 584-84-9, 95-53-4, 8001-35-2, 120-82-1, 95-95-4, 88-06-2, 126-68-1, 1582-09-8, 512-56-1, 137-17-7, 99-35-4, 126-72-7, 78-32-0 | Gas Chromatography/ Mass Spectrometry (GC/MS) | solid waste matrices, soils, air sampling media, water samples | July 2018 |
8275A | Semivolatile Organic Compounds (PAHs and PCBs) in Soils/Sludges and Solid Wastes Using Thermal Extraction/Gas Chromatography/Mass Spectrometry (TE/GC/MS) | Determinative | Polynuclear Aromatic Hydrocarbons (PAHs) and Polychlorinated Biphenyls (PCBs): Acenaphthene, Acenaphthylene, Anthracene, Benz[a]anthracene, Benzo[a]pyrene, Benzo[b]fluoranthene, Benzo[g,h,i]perylene, Benzo[k]fluoranthene, 4-Bromophenyl phenyl ether, 1-Chloronaphthalene, Chrysene, Dibenzofuran, Dibenz[a,h]anthracene, Dibenzothiophene, Fluoranthene, Fluorene, Hexachlorobenzene, Indeno(1,2,3-cd)pyrene, Naphthalene, Phenanthrene, Pyrene, 1,2,4-Trichlorobenzene, 2-Chlorobiphenyl, 3,3'-Dichlorobiphenyl, 2,2',5-Trichlorobiphenyl, 2,3',5-Trichlorobiphenyl, 2,4',5-Trichlorobiphenyl, 2,2',5,5'-Tetrachlorobiphenyl, 2,2',4,5'-Tetrachlorobiphenyl, 2,2',3,5'-Tetrachlorobiphenyl, 2,3',4,4'-Tetrachlorobiphenyl, 2,2',4,5,5'-Pentachlorobiphenyl, 2,3',4,4',5-Pentachlorobiphenyl, 2,2',3,4,4',5'-Hexachlorobiphenyl, 2,2',3,4',5,5',6-Heptachlorobiphenyl, 2,2',3,3',4,4'-Hexachlorobiphenyl, 2,2',3,4,4',5,5'-Heptachlorobiphenyl, 2,2',3,3',4,4',5-Heptachlorobiphenyl, 2,2',3,3',4,4',5,5'-Octachlorobiphenyl, 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl, 2,2',3,3',4,4',5,5',6,6'-Decachlorobiphenyl | 83-32-9, 208-96-8, 120-12-7, 56-55-3, 50-32-8, 205-99-2, 191-24-2, 207-08-9, 101-55-3, 90-13-1, 218-01-9, 132-64-9, 53-70-3, 132-65-0, 206-44-0, 86-73-7, 118-74-1, 193-39-5, 91-20-3, 85-01-8, 129-00-0, 120-82-1, 2051-60-7, 2050-67-1, 37680-65-2, 3844-81-4, 16606-02-3, 35693-99-3, 41464-40-8, 41464-39-5, 32598-10-0, 37680-73-2, 31508-00-6, 35065-28-2, 52663-68-0, 38380-07-3, 35065-29-3, 35065-30-6, 35694-08-7, 40186-72-9, 2051-24-3 | Thermal Extraction, Gas Chromatography/ Mass Spectrometry (TE/GC/MS) | soil, sludges, solid waste | Dec. 1996 |
8276 | Toxaphene and Toxaphene Congeners by Gas Chromatorgraphy/Negative Ion Chemical Ionization Mass Spectrometry (GC-NICI/MS) | Determinative | Toxaphene, 2-exo,3-endo,6-exo,8,9,10-Hexachlorobornane (Hx-Sed), 2-endo,3-exo,5-endo,6-exo,8,9,10-Heptachlorobornane (Hp-Sed), 2-endo,3-exo,5-endo,6-exo,8,8,10,10-Octachlorobornane (P26), 2-endo,3-exo,5-endo,6-exo,8,9,10,10-Octachlorobornane (P40), 2-exo,3-endo,5-exo,8,9,9,10,10-Octachlorobornane (P41) , 2-exo,5,5,8,9,9,10,10-Octachlorobornane (P44) , 2-endo,3-exo,5-endo,6-exo,8,8,9,10,10-Nonachlorobornane (P50), 2,2,5,5,8,9,9,10,10-Nonachlorobornane (P62) | 8001-35-2, Hx-Sed: 57981-29-0, Hp-Sed: 70649-42-2, P26: 142534-71-2, P40: 166021-27-8, P41: 165820-16-6, P44: 165820-17-7, P50: 6680-80-8, P62: 154159-06-5 | Gas Chromatorgraphy/Negative Ion Chemical Ionization Mass Spectrometry (GC-NICI/MS) | solid & liquid matrices | July 2014 |
8280B | Polychlorinated Dibenzo-p-Dioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS) | Determinative | Polychlorinated Dibenzo-p-Dioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs): 2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD), 1,2,3,7,8-Pentachlorodibenzo-p-dioxin (PeCDD), 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (HpCDD), 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD), 2,3,7,8-Tetrachlorodibenzofuran (TCDF), 1,2,3,7,8-Pentachlorodibenzofuran (PeCDF), 2,3,4,7,8-Pentachlorodibenzofuran (PeCDF), 1,2,3,4,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,6,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,7,8,9-Hexachlorodibenzofuran (HxCDF), 2,3,4,6,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,4,6,7,8-Heptachlorodibenzofuran (HpCDF), 1,2,3,4,7,8,9-Heptachlorodibenzofuran (HpCDF), 1,2,3,4,5,6,7,8-Octachlorodibenzofuran (OCDF), Total Tetrachlorodibenzo-p-dioxin (TCDD), Total Pentachlorodibenzo-p-dioxin (PeCDD), Total Hexachlorodibenzo-p-dioxin (HxCDD), Total Heptachlorodibenzo-p-dioxin (HpCDD), Total Tetrachlorodibenzofuran (TCDF), Total Pentachlorodibenzofuran (PeCDF), Total Hexachlorodibenzofuran (HxCDF), Total Heptachlorodibenzofuran (HpCDF) | 1746-01-6, 40321-76-4, 39227-28-6, 57653-85-7, 19408-74-3, 35822-46-9, 3268-87-9, 51207-31-9, 57117-41-6, 57117-31-4, 70648-26-9, 57117-44-9, 72918-21-9, 60851-34-5, 67562-39-4, 55673-89-7, 39001-02-0, 41903-57-5, 36088-22-9, 34465-46-8, 37871-00-4, 55722-27-5, 30402-15-4, 55684-94-1, 38998-75-3 | High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS) | water, soil, fly ash, chemical waste samples, fuel oil, sludge | Feb. 2007 |
8290A | Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS) | Determinative | Polychlorinated Dibenzo-p-Dioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs): 2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD), 1,2,3,7,8-Pentachlorodibenzo-p-dioxin (PeCDD), 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (HpCDD), 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD), 2,3,7,8-Tetrachlorodibenzofuran (TCDF), 1,2,3,7,8-Pentachlorodibenzofuran (PeCDF), 2,3,4,7,8-Pentachlorodibenzofuran (PeCDF), 1,2,3,4,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,6,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,7,8,9-Hexachlorodibenzofuran (HxCDF), 2,3,4,6,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,4,6,7,8-Heptachlorodibenzofuran (HpCDF), 1,2,3,4,7,8,9-Heptachlorodibenzofuran (HpCDF), 1,2,3,4,5,6,7,8-Octachlorodibenzofuran (OCDF), Total Tetrachlorodibenzo-p-dioxin (TCDD), Total Pentachlorodibenzo-p-dioxin (PeCDD), Total Hexachlorodibenzo-p-dioxin (HxCDD), Total Heptachlorodibenzo-p-dioxin (HpCDD), Total Tetrachlorodibenzofuran (TCDF), Total Pentachlorodibenzofuran (PeCDF), Total Hexachlorodibenzofuran (HxCDF), Total Heptachlorodibenzofuran (HpCDF) | 1746-01-6, 40321-76-4, 39227-28-6, 57653-85-7, 19408-74-3, 35822-46-9, 3268-87-9, 51207-31-9, 57117-41-6, 57117-31-4, 70648-26-9, 57117-44-9, 72918-21-9, 60851-34-5, 67562-39-4, 55673-89-7, 39001-02-0, 41903-57-5, 36088-22-9, 34465-46-8, 37871-00-4, 55722-27-5, 30402-15-4, 55684-94-1, 38998-75-3 | High-Resolution Gas Chromatography, High-Resolution Mass Spectrometry (HRGC/HRMS) | soil, sediment, fly ash, tissue, sample extracts | Feb. 2007 |
8310 | Polynuclear Aromatic Hydrocarbons | Determinative | Polynuclear Aromatic Hydrocarbons (PAHs): Acenaphthene, Acenaphthylene, Anthracene, Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(g,h,i)perylene, Benzo(k)fluoranthene, Chrysene, Dibenzo(a,h)anthracene, Fluoranthene, Fluorene, Indeno(1,2,3-cd)pyrene, Naphthalene, Phenanthrene, Pyrene | 83-32-9, 208-96-8, 120-12-7, 56-55-3, 50-32-8, 205-99-2, 191-24-2, 207-08-9, 218-01-9, 53-70-3, 206-44-0, 86-73-7, 193-39-5, 91-20-3, 85-01-8, 129-00-0 | High Performance Liquid Chromatograph (HPLC) | groundwater, wastes | Sept. 1986 |
8315A | Determination of Carbonyl Compounds by High Performance Liquid Chromatography (HPLC) | determinative | carbonyls: Acetaldehyde, Acetone, Acrolein, Benzaldehyde, Butanal (Butyraldehyde), Crotonaldehyde, Cyclohexanone, Decanal, 2,5-Dimethylbenzaldehyde, Formaldehyde, Heptanal, Hexanal (Hexaldehyde), Isovaleraldehyde, Nonanal, Octanal, Pentanal (Valeraldehyde), Propanal (Propionaldehyde), m-Tolualdehyde, o-Tolualdehyde, p-Tolualdehyde | 75-07-0, 67-64-1, 107-02-8, 100-52-7, 123-72-8, 123-73-9, 108-94-1, 112-31-2, 5779-94-2, 50-00-0, 111-71-7, 66-25-1, 590-86-3, 124-19-6, 124-13-0, 110-62-3, 123-38-6, 620-23-5, 529-20-4, 104-87-0 | High Performance Liquid Chromatograph (HPLC) | aqueous samples, soils, waste samples, stack samples | Dec. 1996 |
8316 | Acrylamide, Acrylonitrile and Acrolein by High Performance Liquid Chromatography (HPLC) | Determinative | acrylamide, acrylonitrile, acrolein | 79-06-1, 107-13-1, 107-02-8 | High Performance Liquid Chromatograph (HPLC) | water | Sept. 1994 |
8318A | N-Methylcarbamates by High Performance Liquid Chromatography (HPLC) | Determinative | n-methylcarbamates: Aldicarb (Temik), Aldicarb sulfone, Bendiocarb, Carbaryl (Sevin), Carbofuran (Furadan), m-Cumenyl methylcarbamate, Dioxacarb, Formetanate hydrochloride, 3-Hydroxycarbofuran, Methiocarb (Mesurol), Methomyl (Lannate), Metolcarb, Mexacarbate, Oxamyl, Promecarb, Propoxur (Baygon), Thiodicarb | 116-06-3, 1646-88-4, 22781-23-3, 63-25-2, 1563-66-2,64-00-6, 6988-21-2, 23422-53-9, 16655-82-6, 2032-65-7, 16752-77-5, 1129-41-5, 315-18-4, 23135-22-0, 2631-37-0, 114-26-1, 59669-26-0 | High Performance Liquid Chromatograph (HPLC) | water, aqueous samples, soils, sludges, solids, oily wastes | Feb. 2007 |
8321B | Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet(HPLC/TS/MS)Detection | Determinative | nonvolatiles: Disperse Red 1, Disperse Red 5, Disperse Red 13, Disperse Yellow 5, Disperse Orange 3, Disperse Orange 30, Disperse Brown 1, Solvent Red 3, Solvent Red 23, Disperse Blue 3, Disperse Blue 14, Disperse Red 60, Methomyl, Thiofanox, Famphur, Asulam, Dichlorvos (DDVP), Dimethoate, Disulfoton, Fensulfothion, Merphos, Parathion methyl, Monocrotophos, Naled, Phorate, Trichlorfon, Tris (2,3-dibromopropyl) phosphate (Tris-BP), Dalapon, Dicamba, 2,4-D, MCPA, MCPP, Dichlorprop, 2,4,5-T, Silvex (2,4,5-TP), Dinoseb, 2,4-DB, 2,4-D, butoxyethanol ester, 2,4-D, ethylhexyl ester, 2,4,5-T, butyl ester, 2,4,5-T, butoxyethanol ester, Aldicarb, Aldicarb sulfone, Aldicarb sulfoxide, Aminocarb, Barban, Benomyl, Bendiocarb, Bromacil, Butylate, Carbaryl, Carbendazim, Carbofuran, Carbosulfan, Chloropropham, Chloroxuron, m-Cumenyl methyl carbamate, Diuron, EPTC, Fenuron, Fluometuron, Formetanate hydrochloride, 3-Hydroxycarbofuran, Linuron, Methiocarb, Methomyl, Metolcarb, Mexacarbate, Molinate, Monuron, Neburon, Oxamyl, Pebulate, o-Phenylenediamine, Physostigmine, Physostigmine salicylate, Promecarb, Propham, Propoxur, Prosulfocarb, Siduron, Tebuthiuron | 2872-52-8, 3769-57-1, 126038-78-6, 6439-53-8, 730-40-5, 5261-31-4, 17464-91-4, 6535-42-8, 85-86-9, 2475-46-9, 2475-44-7, 17418-58-5, 16752-77-5, 39196-18-4, 52-85-7, 3337-71-1, 62-73-7, 60-51-5, 298-04-4, 115-90-2, 150-50-5, 298-00-0, 6923-22-4, 300-76-5, 298-02-2, 52-68-6, 126-72-7, 75-99-0, 1918-00-9, 94-75-7, 94-74-6, 7085-19-0, 120-36-5, 93-76-5, 93-72-1, 88-85-7, 94-82-6, 1929-73-3, 1928-43-4, 93-79-8, 2545-59-7, 116-06-3, 1646-88-4, 1646-87-3, 2032-59-9, 101-27-9, 17804-35-2, 22781-23-3, 314-40-9, 2008-41-5, 63-25-2, 10605-21-7, 1563-66-2, 55285-14-8, 101-21-3, 1982-47-4, 64-00-6, 330-54-1, 759-94-4, 101-42-8, 2164-17-2, 23422-53-9, 16655-82-6, 330-55-2, 2032-65-7, 16752-77-5, 1129-41-5, 315-18-4, 2212-67-1, 150-68-5, 555-37-3, 23135-22-0, 1114-71-2, 95-54-5, 57-47-6, 57-64-7, 2631-37-0, 122-42-9, 114-26-1, 52888-80-9, 1982-49-6, 34014-18-1 | High Performance Liquid Chromatography/Thermospray/ Mass Spectrometry (HPLC/TS/MS), ultraviolet (UV)detection | dyes, solid and aqueous matrices, fly ash | Feb. 2007 |
8325 | Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Particle Beam/Mass Spectrometry (HPLC/PB/MS) | Determinative | nonvolatiles: Benzidine, Benzoylprop ethyl, Carbaryl, o-Chlorophenyl thiourea, 3,3'-Dichlorobenzidine, 3,3'-Dimethoxybenzidine, 3,3'-Dimethoxybenzidine, Diuron, Linuron (Lorox), Monuron, Rotenone, Siduron | 92-87-5, 33878-50-1, 63-25-2, 5344-82-1, 91-94-1, 119-90-4, 612-82-8, 330-54-1, 330-55-2, 150-68-5, 83-79-4, 1982-49-6 | High Performance Liquid Chromatography, Particle Beam, Mass Spectrometry (HPLC/PB/MS) | water, wastewater | Dec. 1996 |
8330A | Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC) | Determinative | explosives: nitroaromatics, nitramines: Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX), 1,3,5-Trinitrobenzene (1,3,5-TNB), 1,3-Dinitrobenzene (1,3-DNB), Methyl-2,4,6-trinitrophenylnitramine (Tetryl), Nitrobenzene (NB), 2,4,6-Trinitrotoluene (2,4,6-TNT), 4-Amino-2,6-dinitrotoluene (4-Am-DNT), 2-Amino-4,6-dinitrotoluene (2-Am-DNT), 2,4-Dinitrotoluene (2,4-DNT), 2,6-Dinitrotoluene (2,6-DNT), 2-Nitrotoluene (2-NT), 3-Nitrotoluene (3-NT), 4-Nitrotoluene (4-NT) | HMX: 2691-41-0, RDX: 121-82-4, 1,3,5-TNB: 99-35-4, 1,3-DNB: 99-65-0, Tetryl: 479-45-8, NB: 98-95-3, 2,4,6-TNT: 118-96-7, 4-Am-DNT: 19406-51-0, 2-Am-DNT: 35572-78-2, 2,4-DNT: 121-14-2, 2,6-DNT: 606-20-2, 2-NT: 88-72-2, 3-NT: 99-08-1, 4-NT: 99-99-0 | High Performance Liquid Chromatograph (HPLC) | soil, water, sediment | Feb. 2007 |
8331 | Tetrazene by Reverse Phase High Performance Liquid Chromatography (HPLC) | Determinative | tetrazene | 31330-63-9 | Reverse Phase High Performance Liquid Chromatography (HPLC) | soil, water | Sept. 1994 |
8332 | Nitroglycerine by High Performance Liquid Chromatography | Determinative | nitrogylcerine | 55-63-0 | High Performance Liquid Chromatograph (HPLC) | waste water, ground water, surface water | Dec. 1996 |
8410 | Gas Chromatography/Fourier Transform Infrared (GC/FT-IR) Spectrometry for Semivolatile Organics: Capillary Column | Determinative | semivolatile organics: Acenaphthene, Acenaphthylene, Anthracene, Benzo(a)anthracene, Benzo(a)pyrene, Benzoic acid, Bis(2-chloroethoxy)methane, Bis(2-chloroethyl) ether, Bis(2-chloro-1-methylethyl)ether, Bis(2-ethylhexyl) phthalate, 4-Bromophenyl phenyl ether, Butyl benzyl phthalate, 4-Chloroaniline, 4-Chloro-3-methylphenol, 2-Chloronaphthalene, 2-Chlorophenol, 4-Chlorophenol, 4-Chlorophenyl phenyl ether, Chrysene, Dibenzofuran, Di-n-butyl phthalate, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 2,4-Dichlorophenol, Dimethyl phthalate, Diethyl phthalate, 4,6-Dinitro-2-methylphenol, 2,4-Dinitrophenol, 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, Di-n-octyl phthalate, Di-n-propyl phthalate, Fluoranthene, Fluorene, Hexachlorobenzene, 1,3-Hexachlorobutadiene, Hexachlorocyclopentadiene, Hexachloroethane, Isophorone, 2-Methylnaphthalene, 2-Methylphenol, 4-Methylphenol, Naphthalene, 2-Nitroaniline, 3-Nitroaniline, 4-Nitroaniline, Nitrobenzene, 2-Nitrophenol, 4-Nitrophenol, N-Nitrosodimethylamine, N-Nitrosodiphenylamine, N-Nitroso-di-n-propylamine, Pentachlorophenol, Phenanthrene, Phenol, Pyrene, 1,2,4-Trichlorobenzene, 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol | 83-32-9, 208-96-8, 120-12-7, 56-55-3, 50-32-8, 65-85-0, 111-91-1, 111-44-4, 39638-32-9, 117-81-7, 101-55-3, 85-68-7, 106-47-8, 59-50-7, 91-58-7, 95-57-8, 106-48-9, 7005-72-3, 218-01-9, 132-64-9, 84-74-2, 95-50-1, 541-73-1, 106-46-7, 120-83-2, 131-11-3, 84-66-2, 534-52-1, 51-28-5, 121-14-2, 606-20-2, 117-84-0, 131-16-8, 206-44-0, 86-73-7, 118-74-1, 87-68-3, 77-47-4, 67-72-1, 78-59-1, 95-48-7, 106-44-5, 91-20-3, 88-74-4, 99-09-2, 100-01-6, 98-95-3, l 88-75-5, 100-02-7, 62-75-9, 86-30-9, 621-64-7, 87-86-5, 85-01-8, 108-95-2, 129-00-0, 120-82-1,l 95-95-4,88-06-2 | Gas Chromatography, Fourier Transform Infrared (GC/FT-IR) Spectrometry | wastewater, soils, sediments, solid wastes | July 2014 |
8430 | Analysis of Bis(2-chloroethyl) Ether and Hydrolysis Products by Direct Aqueous Injection Gas Chromatography/Fourier Transform-Infrared (GC/FT-IR) | Determinative | bis(2-chloroethyl)ether (BCEE), 2-Chloroethanol (CE), 2-(2-Chloroethoxy)ethanol (2CEE), Diethylene glycol (DEG), Ethylene glycol (EG) | BCEE: 111-44-4, CE: 107-07-3, 2CEE: 628-89-7, DEG: 111-46-6, EG: 107-21-1 | Gas Chromatography, Fourier Transform Infrared (GC/FT-IR) Spectrometry | aqueous matrices | July 2014 |
8440 | Total Recoverable Petroleum Hydrocarbons by Infrared Spectrophotometry | Determinative | total recoverable petroleum hydrocarbons (TRPHs) | NA | Infrared Spectrophotometry (IR) | sediment, soils, sludges | Dec. 1996 |
8510 | Colorimetric Screening Procedure for RDX and HMX in Soil | Screening | Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX), Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) | 121-82-4, 2691-41-0 | Colorimetric Screening | soil | Feb. 2007 |
8515 | Colorimetric Screening Method for Trinitrotoluene (TNT) in Soil | screening | 2,4,5-Trinitrotoluene (TNT) | 118-96-7 | Colorimetric Screening | soil | Dec. 1996 |
8520 | Continuous Measurement of Formaldehyde in Ambient Air | Determinative | formaldehyde | 50-00-0 | colorimetric analyzer | ambient air | Dec. 1996 |
8535 | Screening Procedure for Total Volatile Organic Halides in Water | determinative | volatile organic halides (VOX): Trichloroethylene (TCE), Perchloroethylene (Tetrachloroethene) (PCE), Carbon tetrachloride, Trihalomethanes (THMs) | TCE: 79-01-6, PCE: 127-18-4, 56-23-5 | Colorimetric Screening | water | Feb. 2007 |
8540 | Pentachlorophenol by UV-Induced Colorimetry | Determinative | pentachlorophenol (PCP) | 87-86-5 | Ultraviolet (UV)-Induced Colorimetry | soil | Feb. 2007 |
9000 | Determination of Water in Waste Materials by Karl Fischer Titration | determinative | Water (H2O) | NA | Karl Fischer Titration | waste | Feb. 2007 |
9001 | Determination of Water in Waste Materials by Quantitative Calcium Hydride Reaction | determinative | Water (H2O) | NA | quantitative calcium hydride reaction | liquids, solids, oils, paints, soils, water/alcohol mixtures | Feb. 2007 |
9010C | Total and Amenable Cyanide: Distillation | determinative | Cyanide | 57-12-5 | reflux distillation | wastes, leachates | Nov. 2004 |
9012B | Total and Amenable Cyanide (Automated Colorimetric, with Off-Line Distillation) | Determinative | Inorganic Cyanide | 57-12-5 | colorimetry | wastes, leachates | Nov. 2004 |
9013A | Cyanide Extraction Procedure for Solids and Oils | sample preparation | soluble Cyanide | 57-12-5 | Extraction | solids, oils, multiphase wastes | July 2014 |
9014 | Cyanide in Waters and Extracts Using Titrimetric and Manual Spectophotometric Procedures | determinative | non-complexed Cyanide | 57-12-5 | titration, colormetric | drinking water, natural surface waters, domestic and industrial wastewaters, soil | July 2014 |
9015 | Metal Cyanide Complexes in Waters and Waste Extracts Using Anion Exchange Chromatography and UV Detection | determinative | metal cyanide complexes: Dicyanoargentate(I) ([Ag(CN)2]-), Dicyanoaurate(I) ([Au(CN)2]-), Hexacyanocolbaltate(III) ([Co(CN)6]3-), Tricyanocuprate(I) ([Cu(CN)3]2-), Hexacyanoferrate(III) ([Fe(CN)6]3-), Hexacyanoferrate(II) ([Fe(CN)6]4-), Tetracyanonickelate(II) ([Ni(CN)4]2-) | With potassium as cation: 506-61-6, 554-07-4, 13963-58-1, 14264-30-3, 13746-66-2, 13943-58-3, 14220-17-8 | Anion Exchange Chromatography, UV Detection | water, waste | July 2014 |
9020B | Total Organic Halides (TOX) | Determinative | Total Organic Halides (TOX) | NA | microcoulometric titration | drinking water, ground water | Sept. 1994 |
9021 | Purgeable Organic Halides (POX) | screening | Purgeable Organic Halides (POX) | NA | microcoulometric titration | drinking water, ground water | July 1992 |
9022 | Total Organic Halides (TOX) by Neutron Activation Analysis | Determinative | Total Organic Halides (TOX) | NA | netron activation analysis | aqueous samples | Sept. 1986 |
9023 | Extractable Organic Halides (EOX) in Solids | Determinative | Extractable Organic Halides (EOX) | NA | pyrolysis/ microcoulometry | solid wastes, soils, suspended solids from industrial wastewater | Dec. 1996 |
9030B | Acid-Soluble and Acid-Insoluble Sulfides: Distillation | sample preparation | Sulfides | 7704-34-9 | distillation | aqueous materials, solid waste, effluents | Dec. 1996 |
9031 | Extractable Sulfides | sample preparation | Sulfides | 7704-34-9 | extraction | oil, solid matrices, multiphastic waste | July 1992 |
9034 | Titrimetric Procedure for Acid-Soluble and Acid-Insoluble Sulfides | Determinative | Sulfides | 7704-34-9 | titration | sample extracts | Dec. 1996 |
9035 | Sulfate (Colorimetric, Automated, Chloranilate) | Determinative | Sulfate | 14808-79-8 | colorimetry | ground water, drinking water, surface water, domestic waste, industrial waste | Sept. 1986 |
9036 | Sulfate (Colorimetric, Automated, Methylthymol Blue, AA II) | Determinative | Sulfate | 14808-79-8 | colorimetry | ground water, drinking water, surface water, domestic waste, industrial waste | Sept. 1986 |
9038 | Sulfate (Turbidimetric) | Determinative | Sulfate | 14808-79-8 | turbidity | ground water, drinking water, surface water, domestic waste, industrial waste | Sept. 1986 |
9040C | pH Electrometric Measurement | Determinative | pH | NA | electrometric pH | aqueous, multiphasic waste | Nov. 2004 |
9041A | pH Paper Method | Determinative | pH | NA | litmus paper | waste | July 1992 |
9045D | Soil and Waste pH | Determinative | pH | NA | electrometric pH | soils, solid wastes, sludges, non-aqueous liquids | Nov. 2004 |
9050A | Specific Conductance | determinative | conductivity | NA | conductivity meter | drinking water, ground water, surface water, saline waters, aqueous waste | Dec. 1996 |
9056A | Determination of Inorganic Anions by Ion Chromatography | determinative | inorganic anions: chloride (Cl-), fluoride (F-), bromide (Br-), nitrate (NO3-), nitrite (NO2-), phosphate (PO43-), sulfate (SO42-) | 16887-00-6, 16984-48-8, 7726-95-6, 84145-82-4, 14797-65-0, 98059-61-6, 18785-72-3 | ion chromatography | drinking water, wastewater, aqueous extracts of solids, collection solutions from bomb combustion of solid waste | Feb. 2007 |
9057 | Determination of Chloride from HCl/Cl2 Emission Sampling Train (Methods 0050 and 0051) by Anion Chromatography | determinative | chloride (Cl-) | 16887-00-6 | ion chromatography | stack gas emission samples | Dec. 1996 |
9060A | Total Organic Carbon | Determinative | Total Organic Carbon (TOC) | NA | carbonaceous analyzer | ground water, surface water, saline waters, domestic waste, industrial waste | Nov. 2004 |
9065 | Phenolics (Spectrophotometric, Manual 4-AAP with Distillation) | Determinative | phenolics | NA | colorimetry | ground water, surface water, saline waters, domestic waste, industrial waste | Sept. 1986 |
9066 | Phenolics (Colorimetric, Automated 4-AAP with Distillation) | Determinative | phenolics | NA | colorimetry | ground water, drinking water, surface water, saline waters | Sept. 1986 |
9067 | Phenolics (Spectrophotometric, MBTH with Distillation) | Determinative | phenolics | NA | colorimetry | drinking water, ground water, surface water, saline waters, domestic waste, industrial waste | Sept. 1986 |
9070A | N-Hexane Extractable Material (HEM; Oil and Grease) and Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material) By Extraction and Gravimetry | Determinative | N-Hexane Extractable Material (HEM) | extraction and gravimetry | surface water, saline waters, industrial aqueous waste, domestic aqueous waste | Nov. 2004 | |
9071B | n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples | Determinative | oil and grease | NA | Soxhlet extraction | sludge, sediment, solids | Apr. 1998 |
9074 | Turbidimetric Screening Method for Total Recoverable Petroleum Hydrocarbons in Soil | screening | petroleum hydrocarbons | NA | Turbidity | soil | Feb. 2007 |
9075 | Test Method for Total Chlorine in New and Used Petroleum Products by X-Ray Fluorescence Spectrometry (XRF) | Determinative | chlorine (Cl2) | 16887-00-6 | X-Ray Fluorescence Spectrometry (XRF) | new & used oils, fuels, crankcase oil, hydraulic oil, diesel oil, lubricating oil, fuel oils, kerosene | Sept. 1994 |
9076 | Test Method for Total Chlorine in New and Used Petroleum Products by Oxidative Combustion and Microcoulometry | Determinative | chlorine (Cl2) | 16887-00-6 | oxidative combustion and microcoulometry | new & used oils, fuels, crankcase oil, hydraulic oil, diesel oil, lubricating oil, fuel oils, kerosene | Sept. 1994 |
9077 | Test Methods for Total Chlorine in New and Used Petroleum Products (Field Test Kit Methods) | Determinative | chlorine (Cl2) | 16887-00-6 | field kit | new or used petroleum products | Sept. 1994 |
9078 | Screening Test Method for Polychlorinated Biphenyls in Soil | screening | Polychlorinated Biphenyls (PCBs) | 1336-36-3 | field kit | soil, sand, gravel, loam, clay, sediment | Dec. 1996 |
9079 | Screening Test Method for Polychlorinated Biphenyls in Transformer Oil | Screening | Polychlorinated Biphenyls (PCBs) | 1336-36-3 | field kit | transformer oil, electrical insulating fluids | Dec. 1996 |
9080 | Cation-Exchange Capacity of Soils (Ammonium Acetate) | Determinative | cation-exchange capacity (CEC) | NA | Ammonium Acetate exchange | soil | Sept. 1986 |
9081 | Cation-Exchange Capacity of Soils (Sodium Acetate) | Determinative | cation-exchange capacity (CEC) | NA | sodium actetate exchange | soil | Sept. 1986 |
9090A | Compatibility Test for Wastes and Membrane Liners | Determinative | compatibility with membrane liners | NA | long-term immersion | waste destined for surface impoundment, waste pile, or landfill | July 1992 |
9095B | Paint Filter Liquids Test | Determinative | free liquids | NA | filtration | waste | Nov. 2004 |
9096 | Liquid Release Test (LRT) Procedure | Determinative | liquid release | NA | overburden pressure test | waste destined for landfill | Sept. 1994 |
9100 | Saturated Hydraulic Conductivity, Saturated Leachate Conductivity, and Intrinsic Permeability | determinative | conductivity, permeability | NA | constant head methods, falling head methods, modified compaction permeameter method, triaxial cell method, pressure-chamber permeameter method, single bore hole methods, piezometer methods | earth materials, leachate, soil liners | Sept. 1986 |
9131 | Total Coliform: Multiple Tube Fermentation Technique | determinative | total Coliform | NA | multiple tube fermentation | ground water, surface water | Sept. 1986 |
9132 | Total Coliform: Membrane-Filter Technique | determinative | total Coliform | NA | membrane-filter | wastewater, ground water | Sept. 1986 |
9210A | Potentiometric Determination of Nitrate in Aqueous Samples with Ion-Selective Electrode | determinative | Nitrate (NO3-) | 14797-55-8 | ion-selective electrode | drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts, aqueous extracts | Feb. 2007 |
9211 | Potentiometric Determination of Bromide in Aqueous Samples with Ion-Selective Electrode | determinative | Bromide (Br-) | 7726-95-6 | ion-selective electrode | drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts | Dec. 1996 |
9212 | Potentiometric Determination of Chloride in Aqueous Samples with Ion-Selective Electrode | determinative | Chloride (Cl-) | 16887-00-6 | ion-selective electrode | drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts | Dec. 1996 |
9213 | Potentiometric Determination of Cyanide in Aqueous Samples and Distillates with Ion-Selective Electrode | determinative | Cyanide (CN-) | 57-12-5 | ion-selective electrode | drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts | Dec. 1996 |
9214 | Potentiometric Determination of Fluoride in Aqueous Samples with Ion-Selective Electrode | determinative | Fluoride (F-) | 16984-48-8 | ion-selective electrode | drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts | Dec. 1996 |
9215 | Potentiometric Determination of Sulfide in Aqueous Samples and Distillates with Ion-Selective Electrode | determinative | Sulfide (S2-) | 18496-25-8 | ion-selective electrode | distilled samples | Dec. 1996 |
9216 | Potentiometric Determination of Nitrite in Aqueous Samples with Ion-Selective Electrode | determinative | Nitrite (NO2-) | 14797-65-0 | ion-selective electrode | drinking water, wastewater, reagent waters | Feb. 2007 |
9250 | Chloride (Colorimetric, Automated Ferricyanide AAI) | determinative | Chloride (Cl-) | 16887-00-6 | Colorimetric | ground water, drinking water, surface water, saline waters | Sept. 1986 |
9251 | Chloride (Colorimetric, Automated Ferricyanide AAII) | determinative | Chloride (Cl-) | 16887-00-6 | Colorimetric | ground water, drinking water, surface water, saline waters, domestic & industrial waste | Sept. 1986 |
9253 | Chloride (Titrimetric, Silver Nitrate) | determinative | Chloride (Cl-) | 16887-00-6 | Titrimetric | oxygen bomb combustates, water | Sept. 1994 |
9310 | Gross Alpha and Gross Beta | sampling | gross alpha, gross beta | NA | particle activity measurement | surface water, ground waters | Sept. 1986 |
9315 | Alpha-Emitting Radium Isotopes | sampling | radium-223, radium-224, radium-226 | 444811-40-9, 13233-32-4,, 7440-14-4 | coprecipitation | surface water, ground water | Sept. 1986 |
9320 | Radium-228 | determinative | radium-228, radium-226 | 15262-20-1, 7440-14-4 | Coprecipitation | groundwater | July 2014 |